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To our knowledge, reverse phase of high performance liquid chromatography was firstly developed to analyze the metabolites of 7-tocopherol with ideal results. Meanwhile, Gas chromatography/Mass chromatography were used to analyze the structures of unknown metabolites of 7-tocopherol and a main unknown metabolite was identified as a side chain ω- hydroxylate of 7-tocopherol.The kinetic results of of 7-tocopherol reacted in the S9 of male SD-rat liver showed that the optimal time was 45 min; the optimal concentration of S9 5 mg/ml; the optimal concentration of NADPH 1 mM; and the optimal concentration of 7-tocopherol 8 μg/ml. The result of γ-tocopherol metabolized in the S9 of male SD-rat was the best; male Brazil turtle better; and male cobia worst.

本试验首次确立了γ-生育酚代谢物的RP-HPLC分析方法,结果理想且重现性好;用GC/MS对γ-生育酚的未知代谢物结构进行分析,判断其中一种主要的代谢物为γ-生育酚侧链初级羟基化代谢物;γ-生育酚在雄性SD-大鼠肝S9的代谢动力学表明,本实验条件下代谢反应的最佳时间为45min,S9浓度为5mg/ml,NADPH浓度为1mM,γ-生育酚浓度为8μg/ml;发现γ-生育酚在雄性SD-大鼠肝S9中代谢最高,雄性巴西龟次之,雄性军曹鱼最低。

Results Totally 550 eyes' the best corrected visual acuity was more than 0.51-3 months after surgery, accounting for 94.83%; 30 eyes (5.17%) had iris prolapse and intraoperative complications; 4 eyes (0.69%) had iridodialysis; 6 eyes 1.03% had posterior capsule rupture; 30 eyes (5.17%) had hyphema; 30 eyes had (5.17%); 109 eyes (18.79%) had postoperative complications, including corneal edema in 50 eyes (8.62%, of which endothelial-like opacity in 40 eyes); 40 eyes (6.90%) had inflammation of anterior chamber; 10 eyes (1.72%) had transient high intraocular hypertension; 5 eyes (0.86%) had hyphema, 4 eyes had pupillary capture.

结果 术后1~3月最佳矫正视力大于等于0.5的有550只眼(94.83%),术中并发症,虹膜脱出30只眼(5.17%),虹膜根部离断4只眼(0.69%),晶状体后囊破裂6只眼(1.03%),前房出血30只眼(5.17%),后弹力层脱离30只眼(5.17%)。术后并发症109只眼(18.79%)包括角膜水肿50只眼(8.62%,其中内皮条样混浊40只眼),前房纤维渗出40只眼(6.90%),短暂性高眼压10只眼(1.72%),前房积血5只眼(0.86%)瞳孔夹持4只眼(0.70%)。

The results show that the optimal value of CoCl2 concentration is 0.2 mol/L and the maximum adsorbed amount is 19.674 mg/g onto this adsorbent. The adsorption capacity of phosphine onto CoCl2-modified ACF decreases with the increase of temperatures. The maximum absorbed amounts are 19.674 mg/g at 298 K, 13.537 mg/g at 313 K and 11.087 mg/g at 328 K, respectively. It is found that the Freundlich equation is more suitable for the description of phosphine adsorption process than the Langmuir equation. The isosteric heat of adsorption decreases with the increase of the surface loading on CoCl2-modified ACF, which means that CoCl2-modified ACF adsorbent has an energetically heterogeneous surface. Meanwhile, adsorptive phosphine removal performance may be a dominant of physical adsorption when the heat of adsorption is 16-24 kJ/mol, the CoCl2-modified ACF adsorbent will be one of the candidates for tail gas purification of airtight calcium-carbide furnace and recycle of phosphine.

研究结果表明:浸渍液浓度最佳值为0.2 mol/L,此改性ACF对PH3的饱和吸附量为19.674 mg/g;PH3在CoCl2改性ACF上的吸附量随温度升高而迅速降低,在298,313和328 K时PH3的饱和吸附量分别为19.674,13.537和11.087 mg/g;Freundlich吸附等温方程较好地模拟了PH3在改性ACF上的等温吸附;PH3气体在改性ACF上的等量吸附热随吸附量的增大而减小,表明改性ACF吸附剂表面能量的不均匀性;吸附热在16~24 kJ/mol范围内,过程为物理吸附,有利于密闭电石炉尾气的净化。

The effects of Konjak glucomannan on the quality of lotus having been dried in microwave were investigated for the purpose of making lotus tea .

本实验是以生产荷花茶为目的,来研究魔芋精粉的赋形性及其成膜的保鲜作用对微波干制后易折皱、破碎荷花品质的影响,得最佳魔芋精粉的浓度为 0 。1

It applies single factorial experiment and orthogonal test to confirm the best technological parameter,and thus obtain solid and white semitransparent konjak granulated gel

运用了单因素试验和正交试验确定了制粒的最佳工艺参数,并且获得了坚实有弹性,复原性好,口感细腻,碱味淡的半透明状洁白魔芋凝胶颗粒

It applies single factorial experiment and orthogonal test to confirm the best technological parameter,and thus obtain solid and white semitransparent konjak granulated gel

运用了单因素试验和正交试验确定了制粒的最佳工艺参数,并签ゑ得了坚实有弹性,复原性好,口感细腻,碱味淡的半透明状洁白魔芋凝胶颗粒

On the basis of the avidity of lesional macrophages for polysaccharide-containing supramolecular structures such as nanoparticles, we have developed a new positron emission tomography agent with optimized pharmacokinetics to allow in vivo imaging at tracer concentrations.

在伤害性巨噬细胞对含多糖的超分子结构如纳米粒子的亲和力的基础之上,我们开发了一种新的正电子发射断层成像剂,该成像剂在示踪物浓度水平进行体内成像方面具有最佳药代动力学特征。

First, this research developed a set of simple and effective technologies for preparative extraction and separation of flavonoid and phloridzin from Lithocarpus polystachyus, which includes:(1) Microwave-assisted extraction of flavonoid f...

本研究首先研发出一套简单、有效的制备性提取分离多穗柯黄酮类及其根皮苷工艺,这套工艺包括:(1)微波辅助氢氧化钙水溶液提取多穗柯黄酮,最佳工艺条件为用1.2 %氢氧化钙水溶液为提取液,料液比1:12,预煮时间5min,微波功率800W处理25min。

First, this research developed a set of simple and effective technologies for preparative extraction and separation of flavonoid and phloridzin from Lithocarpus polystachyus, which includes:(1) Microwave-assisted extraction of flavonoid from tender leaves of Lithocarpus polystachyus Rehd. The extraction conditions are as the follows, 1.2 % of Ca2 water solution, solid-liquid ratio of 1:12, pre-boiling for 5 min, 800 W of microwave treating for 25 min.

本研究首先研发出一套简单、有效的制备性提取分离多穗柯黄酮类及其根皮苷工艺,这套工艺包括:(1)微波辅助氢氧化钙水溶液提取多穗柯黄酮,最佳工艺条件为用1.2 %氢氧化钙水溶液为提取液,料液比1:12,预煮时间5min,微波功率800W处理25min。

ObjectiveTo study the optimal technology of supercritical- CO2 fluid extraction(SFE-CO2) for Litsea cubeba Lour.

目的筛选超临界CO2 流体萃取荜澄茄挥发性成分的最佳工艺,并研究萃取物的药效。

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In the negative and interrogative forms, of course, this is identical to the non-emphatic forms.

。但是,在否定句或疑问句里,这种带有"do"的方法表达的效果却没有什么强调的意思。

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