最佳化的

The conditions for HPLC to detect endogenous polyamines were optimized, that is, benzoylation for 30min at 37℃, detection wave length at 230nm, elution speed at 0.7ml·min〓 Using the above method, endogenous polyamines of calli in Citrus were analyzed.

优化了植物多胺的HPLC测定条件，确定在37℃苯甲酰化反应30min，检测波长230nm，流速0.7ml·min〓效果最佳。

Results showed that chloroacetic acid was the best reagent for esterification and the catalyst had satisfactory catalytic activity and selectivity.

实验结果表明，氯乙酸是最佳酯化剂，催化剂具有较强的活性及选择性。

The experiment confirmed the kind of catalyst and the best technical condition.The result shows,731 strong acidity ion exchange resin is the best catalyze and high selection,it can be used serval times,esterify rate in 80.2%.

考察了催化剂种类、用量、原料配比、反应时间、阻聚剂用量以及催化剂使用次数等因素对酯化率的影响，确定了催化剂种类和最佳工艺条件。

The optimal conditions for the target product were obtained: reaction temperature 110 ℃, reaction time 1.5 h, NaOH dosage 1.2 g,molar ratio 3:1(disproportionated rosin glycide ester: the hydroxyl group per D-glucose unit), microwave power 700 W.

目标产物的最佳合成条件：反应温度110℃，反应时间1.5 h，NaOH用量1.2 g，摩尔比3：1（歧化松香缩水甘油酯：葡萄糖单元中羟基数）及微波功率700 W。

2The choosen 16mg/ml percolation filtration of Hirudo and 0.02 ug/ml PDGF were used to incubate RPE cells for 15 minutes with three different modes.

结果(1)0.02μg/mlPDGF促RPE细胞增殖作用最佳(p.05)；(2)16mg/ml水蛭渗滤液在3种加药方式下均能不同程度抑制细胞内PTK活性，降低转录因子STAT3的磷酸化水平。

Taking refined konjak powder as raw material, taking the mixture of NaH2PO4 and Na2HPO4 as phosphate esterification reagent, the konjac glucomannan phosphate ester was prepared under the dry condition, and the optimal process of konjac glucomannan phosphate ester was optimized by orthogonal test method.

方法］以细化的魔芋粉为原料，以NaH2PO4和Na2HPO4混合物为磷酸酯化试剂，在干法条件下，制备魔芋葡甘聚糖磷酸酯，并采用正交试验法优化魔芋葡甘聚糖磷酸酯最佳工艺。

In the present work, the synthesis of phytosterol laurate was studied, which was esterified directly by using sodium dodecyl sulfate as catalyst. And the optimal conditions were obtained by single-factor and orthogonal experiment.

研究使用十二烷基硫酸钠为催化剂，通过羧酸直接酯化，合成植物甾醇月桂酸酯的工艺，利用单因素试验和正交试验确定最佳工艺条件。

The results showed high class PbSt2 could be synthesized by this new saponifying process.Compared with metathetical process,the reaction time shortened,liquid-solid ratio and moisture content of filter cake decreased.Powder product could be prepared by one-step process,and particle product by two-step process.For the optimum processing conditions,the reaction temperature and time for one-step process were 65℃ and 10min,the amount of alkali added in the first step was 50%;reaction temperture and time were 65℃ and 10min for the two-step process.

结果表明，用皂化法工艺可得到优等品PbSt2，较复分解工艺，反应时间缩短、液-固比降低、滤饼湿含量比减小，一步式工艺得到粉状产品，二步式工艺得到颗粒状产品；最佳工艺条件为：一步式工艺反应温度65℃，反应时间10min；二步式工艺第一步的加碱量比50%，反应温度65℃，反应时间10min。

1M of iodide was optimized parameter of electrolyte in this research. Furthermore, the TiO2 film gave a higher conversion efficiency than the TiO2 film nontreated by 4-tertbutylpyridine, which increased 13% by surface treatment with 4-tertbutylpyridine.

在碘浓度为0.1M时为此实验电解液之最佳参数，另外TiO2薄膜电极通过4-叔丁基吡啶的处理，染料敏化太阳能电池之转换效率较未处理电极高出了13%。

The stability of immobilized ECE on pH, temperature and operation were improved.

固定化酯酶的最佳pH值和温度分别为10.5和50℃。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。