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To be different from the already chloromethylation catalyst, it has a certain amount of moisture wet, which will not produce huge amounts of doughtic cancerogenic chloromethyl methyl ether during and after the reaction.4,4\'-bisbiphenyl, 1,4-bisbenzene, 1,4-bis(chloro- methyl)-2,5-dimethylbenzene, 1,5-bis-2,4-dimethylbenzene, 4-(chlor- omethyl)-1,2-dimethylbenzene, 1,2-bis-4,5-dimethylbenzene, 5,8-bis-1,2,3,4-tetrahydronaphthalene, 3,3\',5-tris-4,4\'-bisbiphenyl and 3,3\', 5,5\'-tetrakis-4,4\'-bisbiphenyl were synth- esized by using this new catalyst. Results indicated that when the reaction temperature was 55~60℃, the reaction time was 12h, the catalyst which consists of the concentration of 80%H_2SO_4, HAc and Lewis acid, the amount of Lewis acid 0.15 mol(nLewis:nbiphenyl=1.5:1), yield of biphenyl chloromethylation product 4,4\'-bis(chrolomethylbiphenyl can reach a maximum 85%.

采用这种催化体系完成了4,4′-二氯甲基联苯、对二氯甲基苯、1,4-二氯甲基-2,5-二甲基苯、1,5-二氯甲基-2,4-二甲基苯、4-氯甲基-1,2-二甲基苯、1,2-二氯甲基-4,5-二甲基苯、5,8-二氯甲基-四氢萘、3,3',5-三氯甲基-4,4'-二甲基苯和3,3',5,5'-四氯甲基-4,4'-二甲基苯的合成,结果表明:在反应条件为:反应温度55~60℃,反应时间12h,选择80%H_2SO_4、冰醋酸和Lewis酸为催化剂,反应最佳反应Lewis酸用量是0.15mol(和原料比为1.5:1),反应效果最好,联苯氯甲基化产物(4,4′-二氯甲基联苯)收率为85%;在反应条件为:反应温度70℃,反应时间8h,80%H_2SO_4、冰醋酸和Lewis酸为催化剂,反应最佳反应Lewis酸用量是0.1mol(和原料比为1:1)时,反应效果最好,苯的氯甲基化产物收(来源:ABd0C论文eded网www.abclunwen.com)率为75%;在反应条件为:在反应条件为:反应温度40℃,反应时间10h,60%H_2SO_4和Lewis酸为催化剂,反应最佳反应Lewis酸用量是0.1mol(和原料比为1:1)时,反应效果最好,对二甲苯氯甲基化产物(1,4-二氯甲基-2,5-二甲基苯)收率为78.5%;在反应条件为:反应温度35℃,反应时间10h,60%H_2SO_4、冰醋酸和Lewis酸为催化剂,反应最佳反应Lewis酸用量是0.1mol(和原料比为1:1)时,反应效果最好,间二甲苯氯甲基化产物(1,5-二氯甲基-2,4-二甲基苯)收率为81.5%。

Gotham Central's debut yielded Eisner Award nominations in 2003 for Best New Series, Best Writer-Rucka, Best Writer-Brubaker, and Best Penciller/Inker-Lark

世界街头中央的首张2003年取得了艾斯纳奖最佳新产品系列,最佳作家,鲁茨卡,最佳编剧兼布鲁巴科,提名和最佳Penciller /墨轮,百灵

The essential effect of feature selection is to improve the accuracy and speed of classification systems. Niched Pareto Genetic Algorithm is a powerful method to solve optimization problems with multiple objectives.

利基柏拉图基因演算法是一种针对多目标最佳化问题所发展出来的工具,可找到多个目标之间的折衷最佳解,以供分析人员选择,而这些折衷最佳解所形成之理想曲线,称为柏拉图最佳边际。

Kobe received nearly every national honor (USA Today Player of the Year, Naismith POY, Gatorade POY and McDonald's All-American) and subsequently dominated the summer camp circuit, earning MVP honors at the 1995 Adidas ABCD Summer Camp and the Beach Ball Classic in South Carolina.

科比几乎拿到了全国所有的荣耀(《今日美国》年度最佳球员,奈史密斯年度最佳球员,佳得乐年度最佳球员和麦当劳全美最佳阵容),并且主导了随后的夏季训练营,获得了1995 ADIDAS ABCD 夏季训练营和南卡罗来纳 Beach Ball Classic 两个MVP。

With the dazzling splendor that director George Cukor offers: the designer's eye for detail, the painter's flair for color, the artist's imagination, and the delicacy of handling, the film garnered no less than twelve Oscar nominations, and took home eight statuettes including Best Picture of the year, Best Actor- Harrison, Best Director- Cukor, as well as Best Art Decoration, Sound, Scoring, Costume Design, and color Cinematography...

随着令人眼花缭乱的绚丽导演乔治丘克提供:设计者对细节的眼睛,画家对颜色天赋,艺术家的想象力,处理细腻,电影积累不低于12次奥斯卡提名,并捧回了8个小雕像,包括最佳影片今年,最佳男主角,哈里森,最佳导演,楚科尔,以及最佳艺术装饰,音响,配乐,服装设计,摄影和彩色。。。

The optimum conditions were as follows: 1 Fe3+/Fe2+ was 1.70-1.75;2 the precipitant,25% ammonia water was used 20%-30%,under 35℃,pH10-11 and with a stirrer speed of 3000 r/min for 1 h;3 in the first package process with gelatin and agar,the optimum amounts was 0.050-0.060g/150mL at the temperature of 55-60℃ and pH of 9-11;In the f...

最佳工艺条件为:(1)Fe3+/Fe2+之比在1.70~1.75;(2)沉淀剂25%NH3.H2O过量20%~30%,温度35℃,pH值11,反应时间为1h;(3)琼脂的最佳用量为0.050~0.060g/150mL;包覆的最佳温度为50~60℃,pH值为9~11;聚乙二醇作为第二次包裹剂时,最佳温度为55℃,反应时间是1h,pH值为4~5;并用透射电镜、分光光度计、古埃磁天平等进行了初步表征。

The constraint conditions of quasi optimal and strict optimal OOCs constructed by recursive method are theoretic analyzed. Based on these constraint conditions, as the initial conditions of OOCs obtained by direct construction, some quasi optimal and strict optimal OOCs with larger code length and sizes are obtained by recursive method.

2理论研究了基于递归法构造准最佳和严格最佳光正交码的约束条件,在此基础上,以直接构造法得到的光正交码为初始条件,利用递归法构造了一些具有相同相关特性的码长更长、容量更大的准最佳和严格最佳光正交码。

And another construction methods for perfect and quasi-perfect binary array pairs are presented with the help of the relationships among the perfect, quasi-perfect and double quasi-perfect binary array pairs. On the other hand, a new kind of discrete signal is presented in this paper, which is the punctured binary sequence pair and the punctured binary array pair.

另一方面,本文提出了一种新的离散信号,即屏蔽二进序列偶和阵列偶,建立了完整的屏蔽二进序列偶和阵列偶的理论体系,它包括最佳屏蔽二进序列偶理论、最佳屏蔽二进阵列偶理论、准最佳和双准最佳屏蔽二进阵列偶理论,以及屏蔽二元互补序列偶理论。

The relationships among perfect punctured binary array pair, quasi-perfect and double quasi-perfect punctured binary array pair is presented. Specially, when first and second dimension period of the punctured binary array pair are odd, the perfect punctured binary array pair, quasi-perfect and double quasi-perfect punctured binary array are able to change each other.

定义了准最佳屏蔽二进阵列偶和双准最佳屏蔽二进阵列偶,研究了它们的变换性质和频谱特性,给出了它们存在的组合允许条件,利用这些组合允许条件,有效地搜索出若干准最佳屏蔽二进阵列偶和双准最佳屏蔽二进阵列偶。

The entire theory systems of the punctured binary sequence pair and the punctured binary array pair are built, which include the perfect punctured binary sequence pair theory, the perfect punctured binary array pair theory, the quasi-perfect and double quasi-perfect binary array pair theory, and the punctured binary complementary sequence pair theory.

定义了屏蔽二进序列偶、最佳屏蔽二进序列偶和奇周期最佳屏蔽二进序列偶,研究了它们的变换性质和存在的组合允许条件,并用这些性质和条件,搜索出若干最佳屏蔽二进序列偶和奇周期最佳屏蔽二进序列偶。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。