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And the PLA/Chitosan/ACP barriers with additional 2 wt% chitosan still maintain 56.58 % antibacterial ability after eightieth day. The different composition of PLA/Chitosan/ACP composites was prepared by water washing solidification from NMP/water/lactic acid consolvent. After storing at room temperature for 48 hours and taking it out to obtain a shapable composites. To investigate the influence of ratio of composition with the shapable property of composites, it was analyzed by Rheometer, TGA, AFM, XRD. The result of the different APC content had different effect both water content and yield stress of composite materials. The yield stress decreased with ACP content while increases. It was derived that ions, released from ACP interact with amide groups of chitosan to form water-absorbing ionic clusters through chelating or electrostatic attraction.

另外,以聚乳酸/几丁聚醣作为基材并添加不同比例的非晶型磷酸钙,经过水洗固化后可得白色片状沉淀物,於室温下静置48小时后,复合材之体积呈现膨胀且具有可塑形之特性,以热重分析仪与流变仪分析样品之含水率与屈伏应力,结果显示不同ACP含量对复合材含水率与屈伏应力具有消长变化,而PLA/Chitosan/ACP之可塑程度与其所吸收之水份多寡有关,推测可能机制为ACP磷酸钙盐解离后之金属离子与几丁聚醣之胺基透过螯合作用或静电吸引之交互作用,形成具吸水性之离子团簇分散於疏水性之聚乳酸基材中。

It is suggested that the intrinsic chirality of the material structure played a role in the band formation. The spherulitic morphology of PHA had considerable effect on the mechanical properties.

对PHA环带的形成机理进行了分析,推测结构上的手性是片晶取向变化的原因。

The results show that a sound bonded interface is obtained without sheet inclusion, pore and unbinding. The microstructure consists of bulk α-Mg phase and needle compound in the weld metal, element Al diffuses along the grain boundary of the substrate into the welding line. A little Y diffuses into the base metal. A little Mn and Cu segregate and element Ni distributes homogeneously and no segregation appears in weld area.

结果表明:界面接合良好,未观察到片状夹杂物、气孔及未焊合等缺陷;焊缝区由块状α-Mg相和针状化合物组成,基体中的Al元素通过晶界扩散偏聚到焊缝中,微量Y元素扩散到基体中,有少量的Mn和Cu元素发生偏聚,Ni元素分布均匀,没有发生偏聚现象。

A snowflake consists of up to 100 snow crystals clumped together.

一片雪花包含将近一百粒结合在一起的雪晶。

The influence of induction heating for PCD compacts determines the quality of the welded tools.

感应加热过程对聚晶金刚石复合片的影响,决定了焊后刀具的质量。

The performances of polycrystalline diamond compacts which includes impact resistance, heat stability and wear resistance are introduced.

介绍了聚晶金刚石复合片的主要性能,即抗冲击性能、热稳定性及耐磨性。

Through a variety of resin filter, adsorption and elution conditions for the optimization, as well as decolorization, crystallization methods of research, this article eventually determine the strong acid cation resin HZ-001 which is at pH 3, 3BV / h, having the largest adsorption to the tryptophan; the fermentation broth were centrifuged to remove sediment,then treated with activated carbon to be decolored and then treated with strong acid cation resin HZ-001. After that,2mol/l amino acid were passed through the HZ-001 ion exchanging column,kept almost constants when the flow rate stayed 6 BV / h. At 60℃,it was condensed into the saturated state and then added Ethanol until its percentage reaching 30%. At 4 ℃ under 100rpm placed in the shaker 20h, the collection of L-tryptophan was dried up in vacuo.

本文通过对种树脂的筛选、吸附和洗脱条件的优化,以及对脱色、结晶方法的研究与摸索,最终确定强酸型阳离子树脂HZ-001在pH=3,3倍床体积流速,温度室温,对色氨酸有最大的吸附作用;将发酵液离心去沉淀并用活性炭脱色后通过HZ-001强酸型阳离子交换树脂柱,再用2mol/L的氨水6倍床体积流速在室温下进行洗脱,收集洗脱液,60℃浓缩为过饱和状态后加入30%无水乙醇,4℃下100rpm摇起晶20h,过滤搜集结晶并真空干燥得白色粉片状L-色氨酸晶体。

The intercrossing angle of the two kinds of epitaxial lamellae is about ±45℃,while the contact planes should be (010) of IPP and (100) of LLDPE.

两种片晶的c轴成45°交角,附生结晶的接触面为LLDPE的(100)和IPP的(010)。

Different from previous works, it was found that the lamellae is not extended but twisted or double-oriented.

与前人工作不同之点是,HEPP纤维中的片晶不是伸展的,而是扭曲或双重取向的。

When the annealing time increases, the twisted lamellae extend gradually.

当退火时间增加,扭曲的片晶逐渐伸展。

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The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0,0.4,0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗,测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

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