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X-ray diffraction is one of the most common and efficient ways to measure a superlattice structure. This dissertation displays the detail results for characterization of Ge〓Si〓/Si superlattices by x-ray diffraction (including x-ray small angle diffraction and double crystal diffraction). It was found, when the growth temperature is lower, the intensities of xray small angle diffraction peaks are modulated by a periodical function, which indicates that both sets of interfaces of the superlattice is highly flat; when the growth temperature is higher, the diffraction peak intensities are simply decay with the increase of diffraction vector, which indicates that one set of interfaces is highly flat but another is not; when the growth temperature is very high, the diffraction peaks are reduced more rapidly, which indicates that both sets of interfaces are not ideal.

本文详细介绍了用X-射线衍射(包括X-射线小角衍射和双晶衍射)方法对Ge〓Si〓/Si超晶格结构特性测试的结果,尤其是发现,当Ge〓Si〓/Si超晶格的生长温度较低时,X-射线小角衍射谱峰的强度随着衍射波矢的增加而周期性调制,表明超晶格的两套界面都十分平整;当生长温度较高时,Ge〓Si〓Si超晶格的X-射线小角衍射谱峰的强度随着衍射波矢呈简单的衰减变化,对应于超晶格内有一套界面不平整的情况;当生长温度进一步提高时,X-射线小角衍射峰明显减少,表明超晶格内两套界面都不理想。

The results show that the interplanar crystal spacing and lattice index of Al-rich α phase reduce gradually with increasing pressure. When the pressure reaches from common pressure to 5 GPa , Al-rich α phase lies on the (200) and (220) crystal faces, the interplanar crystal spacing are reduced by 1.07% and 1.15%. From common pressure to 3 GPa , the microstructure of ZA27 alloy changes from thick dendrites to fine dendrites, and finally to granular. According to the effect of solute diffusion coefficient under super high pressure and the calculation of Scherrer formula, it can be seen that the crystal organization is fine within the bounds of certain pressure. This conclusion is consistent with the experiment results.

结果表明:随着压力的增加,晶面间距和晶格常数都逐渐减小,当压力达到5 GPa时,富铝α相在(200)与(220)晶面处,晶面间距较常压力时的分别减小1.07%和1.15%;在常压至3 GPa范围内,晶粒由粗大的树枝晶→细小的树枝晶→粒状、椭球状枝晶转变的趋势,通过压力对合金凝固溶质扩散系数的影响结合Scherrer公式计算分析其组织变化原因,得出在一定的压力范围内,随着压力的增大,晶粒尺寸逐渐变小,这一结论与实验结果相符。

Thealmost single phase can be obtained in RFe1.95 under suitablegrowth conditions.Any deviation from these growth conditions andcomposition results in the apparence of intergrain rare earth phaseor intragrain RFe3 or WSP deposition.

工艺研究发现,在合适的提拉条件下,RFe1.95的成份可以得到近似单相的结构,成份的偏离将导致晶体中出现晶间稀土相或晶内的RFe3或WSP淀积。

The complex style of zoning texture in garnet is mainly originated by Fe-Mg exchange reaction on it s interface with Bt or other mafic minerals and intercrystal diffusion at the same time.

石榴石中复杂的环带结构样式主要通过它与黑云母等相邻矿物界面上发生的Fe-Mg交换反应和向晶内的扩散作用来实现。

At first, mineral composition and distributing of impurities in andalusite grains were studied by SEM and EDS. The results showed that main mineral impurities were biotite, ilmenite, clay species, the wall rock conglutinated at brim of andalusite and impurities in the chiastolitic cruciform pattern were easily removed, but the small impurities in andalusite grain were hardly removed.

首先,利用SEM和EDS分析了红柱石矿的矿物组成和杂质分布,结果显示这种红柱石矿所含的杂质矿物主要是黑云母、钛铁矿和黏土矿物等,其中分布在红柱石颗粒边缘的围岩和空晶石内的黑十字容易去除,而分布在晶内的细粒杂质则不易去除。

Results of EBSD show that most of the reversed austenite in the steel treated by QT distribute along the grain boundary, but in the steel treated by two--phase region heat treatment the austenites distribute uniformly along all kinds of boundaries, especially also along the lath martensite boundary in the grain, so the cryogenic toughness can be also improved even the amount of austenitic is lower than that in the steel treated by QT process.

EBSD结果则表明:经两相区处理,回转奥氏体不仅在晶界和板条束界形成,也在晶内的板条界上形成,因此即便在其含量低于淬火+回火处理的条件下, 9Ni钢的低温韧性也有明显提高,证明回转奥氏体的分布也是影响9Ni钢低温韧性的一个主要因素。

Grain boundary slidings happen in this alloy at the creep temperature of 200 ℃ and the deformation of this alloy is coordinated by intragranular slip and grain boundary sliding.

结果表明:在125~200 ℃蠕变温度下,当蠕变寿命接近100 h时,2024铝合金的蠕变应力随着温度的升高明显下降;与125 ℃相比,150 ℃时合金的蠕变应力下降9.3%,在175 ℃时合金的蠕变应力下降30.3%;当蠕变温度为200 ℃时,该合金的蠕变应力下降幅度达到45.8%;在125~175 ℃下,合金在蠕变过程中的变形机制主要为位错在晶内的滑移;在200℃时,合金晶界开始发生滑移,合金变形由晶界滑移与位错在晶内的滑移协调完成;在合金蠕变断面上存在大量微孔,随着蠕变温度的升高,微孔的尺寸明显变大,当微孔尺寸超过3 μm时,微孔对合金的断裂机制有显著影响;在125和150 ℃下,合金的蠕变断口呈现韧窝型穿晶断裂特征;在175和200 ℃下,合金的蠕变断口呈现沿晶断裂特征。

Refining grain behavior of the heat affected zone of E36 high strength low alloy steel was studied, when E36 steel was welded by three wires submerged arc welding with 110 kJ/cm large heat input .

大热输入焊接时,氧硫复合物诱导热影响区的晶内铁素体形核,并促进晶内铁素体的感生形核,晶内铁素体及其感生晶内铁素体使热影响区粗晶区的晶粒细化,确保焊接热影响区粗晶区的强度与韧性不降低。

The results show that the growth rate of tetrapod ZnO is controlled by spiral growth and its crystallization is via VLS model. The condensation of tiny zinc droplets in zinc vapor is the key factor of the formation of tetrapod ZnO. The growth steps are formed on the terminated faces as zinc diffuses outwards and the elongation of whiskers continues until zinc inside the droplets is depleted. VS crystallization, which has little effect on the elongation growth, takes place on side faces of the whiskers and consequently makes the whiskers radius increase.

结果表明: T-ZnO晶须的结晶作用是气-液-固方式,晶须生长受螺旋生长机理控制;锌蒸气中产生凝聚生长的锌液滴是制备T-ZnO晶须的关键,锌从液滴内向外扩散在晶须的端面产生生长台阶,随着液滴内的原子向外不断扩散,针体部分就不断地伸长生长,当液滴内的原子全部消耗尽时,晶须便不再发生轴向生长;气-固方式的作用主要是促进晶须棱面生长而使晶须变粗,对轴向生长几乎没有影响。

Microscopic characteristics of cladded crystal fiber are analyzed by X-ray diffraction, Laue X-ray diffraction and scanning electron microscopy, it is found that magnesium-ion indiffusion does not affect the single crystal structure and the domain structure of the magnesium diffused crystal fiber. It is found for the first time that MgO-rich layer in the magnesium diffused LiNbO〓 surface layer exhibits the crystal structure of an unknown compound from the Li-Mg-Nb-O ternary system and MgNb〓O〓. It is proposed for the first time that this unknown compound and MgNb〓O〓 in MgO-rich layer are the real sources of magnesium-ion indiffusion LiNbO〓. Their appearance indicate that MgNb〓O〓 is in the surface layer of MgO-rich layer, the unknown compound is in the subsurface layer and beneath where the MgNb〓O〓 is located, and these compounds have obviously preferred orientation.

通过镁离子内扩散法,首次在国内实现了具有阶跃和抛物折射率分布的c轴LiNbO〓单晶光纤和a轴Nd:MgO:LiNbO〓单晶光纤的芯—包层波导结构,为我国在该项目的研究填补了空白;建立了晶纤损耗的测量系统,提出了利用单模石英光纤作为晶纤入射光耦合器的思想;通过对晶纤损耗的测量,得到了包层晶纤比未包层晶纤损耗降低约14倍的好结果,并实现了低次模传输:对经镁离子内扩散实现包层后的晶纤的微观特性,利用X射线衍射,劳厄照相和扫描电镜表征发现,晶纤并不因镁离子的内扩散而影响其单晶结构和镁的扩散层畴的变化。

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Fancy gold-plated dangling earrings with facetted White Opal crystals.

花式镀金悬垂耳环与facetted白欧泊水晶。

This essay chooses the study aim from biology teachers in middle school in Shi Jiazhuang which tells us that most of the middle school biology teachers in Shi Jiazhuang have the"burnout", lower successfulness, individualize.

本文选取石家庄市初中生物教师作为研究对象,运用问卷调查的方法对石家庄市初中生物教师职业倦怠的现状进行调查,调查结果发现,石家庄市初中生物教师这一群体普遍存在职业倦怠,情感枯竭程度偏高,成就感偏低,去个性化程度最为严重。

In measurements of a day,generallyspeaking,the photosynthesis of birch in mesophytic habitat is better than that in xerophytichabitat(peak values are 12.8,10.33μmolCO2m-2s-1 respectively);that of sexual birch inmesophytic habitat is better than that of clone birch(peak values are 9.87,6.71μmolCO2m-2s-1respectively);that of young tree is better than that of seedling(peak values are12.37,10.05μmolCO2m-2s-1 respectively).

在一天中的各个时刻,总体说来,中生生境生长的白桦光合作用超过旱生生境生长的白桦光合作用(净光合速率峰值分别为12.8、10.33μmolCO2m-2s-1);白桦幼树的光合作用超过白桦幼苗(净光合速率峰值分别为12.37、10.05μmolCO2m-2s-1);中生生境有性白桦的光合作用超过无性白桦的光合作用(净光合速率峰值分别为9.87μmolCO2m-2s-1、6.71μmolCO2m-2s-1)。