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晶体衍射

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The structure of AlPO4-5 single crystal has been refined by the SMART 1000 single crystal diffractometer.

用扫描电镜观察晶体的形貌;AlPO4-5分子筛晶体结构通过SMART 1000单晶衍射仪鉴定。

The results show that the particles character as the growth of anion coordination tetrahedron during solvent thermal treatment, where blende-type ZnS particle is in the shape of double cone or tetrahedron, blend-type CdS appears as the tetrahedron, but wurtzite-type CdS is in the shape of cone. In addition, the particles with the better crystallinity are obtained with the increase of solvent thermal treatment temperature and time.

结果表明:采用溶剂热处理,粉末形状呈现负离子配位多面体生长特征,闪锌矿型ZnS粉末由球形变为双锥状或四面体状,颗粒上有明显的电子衍射花纹;闪锌矿型CdS晶体粉末主要呈四面体形状,而纤锌矿型CdS晶体粉末则以锥状为主,并且粉末的晶型随溶剂热处理温度的升高和时间的延长更趋于完整。

In this paper,the affecting rules of micronization on the properties of crystal type of acorn starches were studied by applying RINT2000 vertical goniometer to measurethem.

利用RINT2000 vertical goniometer型X-衍射仪测定经超微粉碎橡实淀粉的晶体特性,研究了超微粉碎对橡实淀粉晶体特性的影响规律。

The electrochromic reaction of this coating in theliquid electrolyte is reversible.X-ray diffraction was used to analyse the coating,and the result shows that the original WO_3 film is triclinic WO_3 while the colouredlayer is orthorhomic H_...

X 光衍射实验发现,变色后的涂层由原来的三斜 WO_3晶体变成了 H_(0.1)WO_3斜方晶体。本文还用扫描电子显微镜对热处理前后涂层的表面形貌进行了分析。

Caprolactam grafted carbon fibre could improve the initial crystallization temperature and the crystallization rate more obviously than ungrafted carbon fibre. The crystallization of nylon 6 was determined by nucleation. The nonisothermal crystallization dynamics was well coincident with the rule of both of Jeziorny and Liu equation. isothermal crystallization dynamics fitted to Avrami equation.

用广角X射线衍射法对晶型结构进行研究,表明碳纤维使原生态的样品中α晶型的含量降低,结晶度下降,其中接枝聚己内酰胺链段的碳纤维/MC尼龙6原位复合材料中α晶型的含量比未接枝的碳纤维/Me尼龙6原位复合材料的多,结晶度也较大:样品淬火时,碳纤维有利于基体尼龙6结晶时形成γ型晶体,接枝聚己内酰胺链段的碳纤维更有利于基体尼龙6结晶时形成γ型晶体;淬火后的样品在200℃下退火2个小时后γ晶型完全转变为α晶型。

The presence of boron was primarily ascertained by the color of crystal, X-ray diffraction and Raman spectrum.

通过晶体的颜色、X射线衍射以及Raman光谱可以初步断定合成出的金刚石晶体中确实含有硼元素。

On the basis of developing a new technology to synthesize sodium diacetate successfully without any pollution,the culture of bigger crystal in perfect shape and single crystal of small dimension suitable for X-ray diffraction was attained.

在研究成功双乙酸钠零污染合成工艺的基础上,培养成功了晶型完美的大尺寸晶体和适宜进行X光结构分析的小尺寸单晶,并进一步应用四圆衍射仪测得其晶体结构。

The crystal monochromator is a key device of the X-ray beamline. It uses crystals as dispersive elements to diffract and separate the synchrotron radiation, and provide X-ray monochmmatic light with a given energy bandwidth.

晶体单色仪是X射线光束线上的关键设备,它用晶体作为色散元件,衍射、分离具有连续光谱的同步辐射,向用户提供一定带宽的X射线单色光。

The morphology of calcium carbonate scale withthe presence of the PAA is not in order any more, but can be still observed the shapeof cubic structure. The crystal morphology of calcium carbonate scale with addingP is completely destroyed, and XRD spectrums show the quantity ofcalcite reduces, so the scales become loose, spongy, floccular and amorphous.

添加PAA后尽管表面不再平整但仍能观察到比较规整的四面体晶体结构;而添加P后晶体形状被彻底破坏,垢样成为疏松、多孔、絮状的无定形聚集体。X衍射谱图也表明,添加P后垢样中方解石含量减少甚多,垢样变得疏松。

The amorphous gelatin was heated by self-combustion in microwave oven. The burning process of amorphous gelatin was studied by TG-DTG. The products were detected by X-Ray and TEM.

利用热分析研究了干凝胶自燃烧过程,并且利用X衍射、透射电子显微镜研究了pH值、温度、成胶时间以及燃烧温度对MnZn铁氧体的晶体结构、晶体组成和粒径大小的关系。

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