晶体衍射

Deoxy-hemoglobin of Bar-Headed Goose was prepared with Na2S2O4 as reducing agent.The single crystals were obtained from polyethylene glycol solution 6000 at pH 7.2, 0.05mool/L phosphate buffer, protein 20mg/ml. Using the hanging drop methed.

报导了以Na2S2O4为还原剂制备脱氧血红蛋白，并以聚乙二醇溶液为沉淀剂，在pH7.2，蛋白浓度20mg／ml条件下培养出适合于X射线分析用的斑头雁脱氧血红蛋白晶体，经X射线平面探测仪收集衍射强度数据和处理。

The compositions of complexes were determined as, by chemical and elemental analyses, Mn2CI2, Mn2Cl2, Cu2Cl2-2H2O, Cu(NO3)2-H2O, Cu(CH3COO)2, Zn2Cl2, Zn2(NO3)2-4H2O,ZnSO4 and Zn4(NO3)2, respectively. These complexes were characterized by IR,'H NMR and XPS. The crystal structures of these complexes were determined by single crystal X-ray diffraction techniques. The thermstability of the complexes was investigated by TG-DTG and the processes of their thermal decomposition were speculated. The constant-volume combustion energies of complexes, cU, were determined by a precision rotating bomb calorimeter at 298.15 K. Their standard enthalpies of formation, Hm, were calculated respectively. Finally, their biological activity was researched after the bactericidal activity was determined by selection of 1-2 bacteria.

通过化学分析、元素分析确定化合物分子组成分别为Mn_2Cl_2，Mn_2Cl_2，Cu_2Cl_2·2H_2O，Cu(NO_3)_2·H_2O，Cu(CH_3COO)_2，Zn_2Cl_2，Zn_2(NO_3)_2·4H_2O，ZnSO_4和Zn_4(NO_3)_2；借助IR、~1H NMR和XPS对化合物的键型特征进行了表征，运用X-射线单晶衍射分析法测定了个别化合物的晶体结构；以TG-DTG技术研究了化合物的热稳定性，阐明了它们的热分解机理；用精密转动弹热量计测定了化合物在298.15 K的恒容燃烧能，并计算了它们的标准燃烧焓和标准生成焓；选取1～2种病菌，初步测定了化合物的杀菌活性，进而研究了它们的生物活性。

In this paper several technologies, such as Fourier transform infrared spectroscopy, elemental analyzer, wide angle X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy and high resolution transmission electron microscopy were used to systemically investigate the evolution of crystal structure, chemical structure, microstructure and properties of wet-spinning and dry-jet wet-spinning PAN precursor fibers during proxidation and carbonization process, analysis the structural change of carbon fibers during graphitization, and discuss the correlation between the structure and properties.

本文采用傅里叶变换红外光谱、元素分析仪、X射线衍射仪、场发射扫描电镜、透射电镜以及高分辨透射电镜等测试技术，分别系统研究了湿纺原丝和干喷湿纺原丝在预氧化和碳化过程中纤维晶体结构、化学结构、微观结构和力学性能的演变规律，分析了碳纤维在石墨化过程中的结构转变，并对碳纤维结构与性能的相关性问题作了探讨。

Calcium carbonate crystal form was characterized by microscope and electron-scanning microscope,XRD and FTIR analysis was employed to investigate the morphology of calcium carbonate whiskers.

论文摘要以工业废弃磷石膏为原料制备碳酸钙晶须，利用显微镜和扫描电镜观察晶体形貌，晶须样品的晶型用X衍射和红外光谱进行了表征。

Calcium carbonate whiskers were synthesized by using industrial waste phosphogypsum as raw materials.Calcium carbonate crystal form was characterized by microscope and electron-scanning microscope,XRD and FTIR analysis was employed to investigate the morphology of calcium carbonate whiskers.

论文摘要以工业废弃磷石膏为原料制备碳酸钙晶须，利用显微镜和扫描电镜观察晶体形貌，晶须样品的晶型用X衍射和红外光谱进行了表征。

Calcium carbonate whiskers were synthesized by using industrial waste phosphogypsum as raw materials.Calcium carbonate crystal form was characterized by microscope and electron-scanning microscope,XRD and FTIR analysis was employed to investigate the morphology of calcium carbonate whiskers.

论文摘要以废弃磷石膏为原料制备碳酸钙晶须，利用显微镜和扫描电镜观察晶体形貌，晶须样品的晶型用X衍射和红外光谱进行了表征。

By means of modern analysis and testing tools such as X-ray diffraction and flurescence spectrum research the crystal constitution and luminescence performance of materials.

结合X射线衍射仪、荧光分光光度计等现代分析测试手段，研究了其晶体结构和发光性能。

The second-harmonic generation theory of phase aberrated laser beam in uniaxial crystals is discussed, in cluding the effects of diffraction and transverse walkoff.

理论上研究了单轴晶体Ⅰ类匹配时相位畸变光束二次谐波的转换，其中考虑了衍射、离散效应，给出了相位畸变小信号解。

Guangzhou 510650, P.R.China）Abstract: A new type of photoelectrode was innovated by anodising titanium mesh in H2SO4 solution and named Ti/TiO2 mesh electrode.

摘 要：采用电解氧化金属钛网的方法制备新型光电极Ti/TiO2，采用X射线衍射仪、激光拉曼光谱仪与扫描电镜测试电极的表面晶体结构与表面形态。

A chiral phase transfer catalyst, N-benzyl quinine bromide, was synthesized from natural chiral compound. And 2,5-bimethyl-4-(3-nitrobenzene)-1,4-bihydrogenation pyridine-3--4-methyl formate (viz. nitrendipine) was synthesized by this chiral phase transfer catalysis, and characterized by elemental analysis, infrared spectrum,1H nuclear magnetic resornace, and X-ray single-crystal diffraction.Key words: ammonium; chiral phase transfer catalyser; crystal structure

通过对天然手性物质进行修饰合成手性相转移催化剂N-苄基溴化奎宁，并对目标分子2，5-二甲基-4-(3-硝基苯)-1，4-二氢吡啶-3-甲酸乙酯-5-甲酸甲酯进行不对称催化合成，并通过红外光谱和核磁共振氢谱对化合物进行了表征，用X射线单晶衍射法测定了该化合物的晶体结构。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。