晶体衍射

The platform of diffraction data collection and analysis for protein crystalAccording to the characteristics of Hefei Light Source,based on the XRDS Station in NSRL at USTC,the experiment platform was set up for measuring sulfur anomalous scattering signal with long-wavelength X-ray.

蛋白质晶体衍射数据采集及数据分析的平台根据合肥光源的特点，依托中国科学技术大学国家同步辐射实验室X射线衍射与散射实验站，搭建了适于测量硫元素反常散射信号的长波长X射线衍射实验平台。

In the same time, we synthesized a ketone containing iodine and determined its crystal structure by X-ray diffraction.

同时，我们通过Heck反应，合成了一个含碘不饱和酮，通过X-晶体衍射对该单晶化合物进行了晶体结构测定。

All the compounds are characterized by IR and elemental analysis.we design and prepare a bipyridinium supramolecular compound and six coordination compounds, which are also characterized by IR, elemental analysis and X-ray structure analysis. According to X-ray structure analysis, hydrogen bonds and n-n stocking interactions participate in the architecture of three-dimensional framework [H2L1 (NO3)2 (H2O)2]n; one-dimensional zigzag coordination polymer [Hgl21.5CH3OH]n; binuclear metallamacrocycle (HgI2L2)2 3H2O; helical double-stranded one-dimensional coordination polymer [Co2(L2)2-2CH3OH]n; double-stranded one-dimensional coordination polymer [Co2(L3)2-CH3OH-CH3CN]n; and three-dimensional compound [Cu(C5H4NCOO)2(H2O)2]-H2O with hydrogen bonds, three-dimensional coordination polymer {[Cd(C5H6NCOO)2H2O]-DMF}n, which are indirectly obtained from the precursor ligand L3 through metal ion induced the hydrolysis of diamide and self-assembled with the hydrolyzate.

我们首次合成了一个双吡啶鎓超分子化合物和六个过渡金属配合物，并通过IR谱，元素分析和X-ray晶体衍射分析对它们进行了表征。X-ray晶体结构分析表明：超分子化合物[H_2L1·(NO_3)_2·(H_2O)_2]_n是由多种氢键和芳香环间的π-π堆积作用构建的三维无限结构；[HgI_2(L1)·1.5CH_3OH]_n是一维锯齿状配位聚合物；(HgI_2L2)_2·3H_2O是双核金属大环化合物；[Co_2(L2)_2·2CH_3OH]_n是具有一维双螺旋结构的配位聚合物；[Co_2(L3)_2·CH_3OH·CH_3CN]_n为一维双链结构的配位聚合物；以及由非直线形配体L3在金属离子Cu和Cd的诱导作用下发生水解，并且金属离子与水解产物——异烟酸根离子自组装，形成了三维氢键超分子化合物[Cu(C_5H_4NCOO)_2(H_2O)_2]·H_2O和三维配位聚合物{[Cd(C_5H_6NCOO)_2H_2O]·DMF}_n。

The construction of branched-chain sugar was carried out by hydroboration-oxidation of a double bond in the corresponding hexose.

通过相应的烯糖9的硼氢化-氧化反应构建了支链糖11，同时分离到一系列还原的副产物7c-e，通过X-射线晶体衍射确定了7c和7e新的手性中心的构型。

And then, a window-type novel x-ray crystal spectrometer was put forward based on the elliptically curved crystal analyzer. It was coupled to an x-ray CCD camera, and a set of system had been designed and constructed. The spectrograph is useful in the experiments of x-ray diagnostics, for example in x-ray lasers, inertial confinement fusion, laser-matter interaction, and so on.

本论文从X射线晶体衍射和椭圆自聚焦几何光学原理出发，剖析追究了椭圆型弯曲X射线晶体谱仪在实际应用中产生问题的根源，率先从技术上提出解决目前椭圆型弯曲X射线晶体谱仪存在问题的思路，论证了其相应实施方案的可行性。

The inperfect crystal structure and its analysis for materials, is an elective course for the master graduate student, which include the crystallology principle, development of crystal diffraction, crystal determination and computer simulation of new phase, analysis of solid solution and superstructure, correction of crystal structure and bondvalent theory, analysis of inperfect crystal structure, analysis of amorphous structure and so on.

材料不完整晶体结构及其分析方法，为材料科学及工程等专业硕士研究生的选修课，内容包括晶体学基础、晶体衍射技术最新进展、新相晶体结构测定与数值模拟、固溶体与超结构分析、晶体结构修正与价键理论、不完整晶体结构分析、非晶结构分析等。

The patterns of Reflection high energy electron diffraction from the epitaxial growth of Si-Ge crystal are interpreted basing on the kinetical diffraction theory of crystal.

在晶体衍射理论基础上，利用运动学理论解释了反射式高能电子衍射（reflection high energy electron diffraction， RHEED）在Si-Ge晶体外延生长过程中不同阶段出现的花样。

The structure characters of this kind of molecules were discussed. The results show that the phenyl group located in the 4- or 5- position of pyrryl ring are not coplanar with the pyrryl ring.

对这类吡咯环上4或5-位有芳环取代基时化合物的晶体结构特征进行了扼要讨论，晶体衍射实验结果表明，4， 5-位上的芳环与吡咯环本身处于非共平面结构。

The proper alkaline content was in favor of compressive strength. The chemically combined water of paste without activator decreases with the increase of fly ash content, the content of Ca2 decreases after 28d. The increase extent of chemically combined water of pastes with NaOH is higher than that of without activator, and the paste with Ca2 is the same. The XRD peak of Ca2 of paste without activator is high at early age, and the peak of mullite and quartz has less change along with age. When NaOH is added, the peak of quartz of fly ash has clear drop. The surfaces of fly ash activated has eroded trace at 7 d.

研究结果表明：适量碱的掺入对强度有利；未掺激发剂浆体的化学结合水量随着粉煤灰掺量的增加而减少，Ca2含量在28d后开始下降；掺NaOH浆体的结合水量随龄期增长的幅度比未掺激发剂的浆体的大，而掺Ca：试样变化较小；未掺激发剂的水泥－粉煤灰体系在早期Ca2的峰值较大，且粉煤灰中的莫来石和石英晶体的衍射峰随龄期变化不大；NaOH掺入后，28d时，粉煤灰中的石英晶体衍射峰明显下降；时于掺激发别的试样，在7d时粉煤灰颗粒表面已被腐蚀。

After obtaining highly active purified, Arabidopsis thaliana AHAS, the crystallization of AHAS-monosulfuron had been tried.

通过X-射线衍射实验，经过对全部衍射图像的整合、分析，最终得到了分辨率为2.9〓的晶体衍射数据。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。