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The effects of FPL andits three ingredients on growth of ovary,on micro-and ultra-structure andAlkaline phosphatase activity of endometrium,on structure andkeratinization rate of exfoliated cells in vaginal epithelium in mice,onmicrocirculation in rat and on uterine kinesis in rabbit were respectivelyobserved by the techniques of light and electron microscopes,histochemistry,microcirculation and organ cinetography.The results have confirmed themechanism of FPL for the sterility caused by ovary standstill and persistentcorpus luteum to be as follows:(1) a weak estrogen-like role which canprompt development of ovary,proliferation and secretion of endometrium andvaginal epithelium and cornification of exfoliated cells in vaginal epithelium;(2)enhancing AKP's activity of endometrium;(3)improving microcirculation;(4) exciting uterus.

分别采用光学显微镜和电子显微镜技术、组织化学技术、微循环技术和器官运动描记等现代医学实验技术,观察了促孕液对小白鼠的卵巢发育、子宫内膜的显微和超微结构和碱性磷酸酶活性、阴道上皮结构和脱落细胞的角化率、对大白鼠的微循环和对家兔的子宫运动的影响,结果证实了促孕液治疗卵巢静止、持久黄体的机理:(1)微弱的雌激素样作用,能刺激卵泡发育,促进子宫内膜和阴道上皮增生、分泌和阴道上皮脱落细胞角化;(2)提高子宫内膜碱性磷酸酶的活性;(3)改善微循环;(4)促进子宫运动。

Microscope and image analysis technique are adopted in 《JB/T 7990-1998》. The "grain size" tested by microscope is expressed by the "largest breadth" of the grain image. When the grain size is tested by image analysis instrument, the grain size is expressed by the diameter of a circle whose area equals the grain image's.

JB/T7990-1998》规定用图像分析仪或显微镜测量粒度,显微镜法测量的"粒度"是以颗粒投影的"最大宽度"来表征的,而用图像分析仪测量的"粒度"指的是"等面积圆直径",即,用与颗粒投影面积相等的圆的直径表征颗粒粒度。

Selected the best cultivate condition by cultivated on four different media under different conditions; Observated morphology perperties; Studied on biology perperties by germ tube testing, Carbohydrate fermentation testing, Tween testing and Esculin dissociation; lysis testing.

选择四种不同的培养基分别在不同温度条件下培养,选出最优培养条件;通过光学显微镜、电子显微镜观察菌落及菌体的形态学特点;通过芽管试验、碳水化合物发酵试验、碳水化合物同化试验、沙堡培养基生长试验、过氧化氢酶试验、七叶苷分解试验、吐温试验研究该菌的生理、生化学特征;应用PCR技术通过特异性的引物扩增得到菌属特异性的片段,最后测定扩增片段的核苷酸序列,从而进行菌种的分析、鉴定。

Results:Whith the time and doses of ART incubation extended, ART significantly inhibited the proliferation of SGC-7901 cells and the inhibited effect shows dose-and -time-dependent. Obvious changes of apoptotic morphology were observed by invert microscope, fluorescence microscope, scanning electron microscope and transmission electron microscope, they showed that cells had marked nuclear condensation or the fragmentation of chromation as well as apoptotic , mitochondrial edema and vesicle , with the time of incubation extended , the proliferation rate become slow and the volume became small and transformed. FCM assay indicated that most of the cells were arrested in Go/Gi and the apoptotic peak appeared. During the prolong of incubation time, the apoptosis rate was increased. At the same time, the number of S and G2/M phase cells were decreased. The result of TUNEL indicant that there are apoptosis and necrosis.

结果:随着药物浓度的增加和作用时间的延长,蒿甲醚对胃癌SGC-7901细胞的抑制作用呈时间和浓度依赖关系:在倒置显微镜、荧光显微镜、扫描电镜和透射电镜下可观察到典型的凋亡细胞的形态改变,表现为:核固缩或染色质边聚或凝聚成大块状,可见凋亡小体,线粒体肿胀增殖,严重的空泡化,随作用时间的延长,细胞增殖速度减慢,细胞体积缩小变形;流式细胞术显示胃癌SGC-7901细胞出现明显的凋亡峰,随着作用时间的延长,其凋亡率逐渐升高,细胞周期阻滞在G_0/G_1期,S及G_2/M期细胞数大量减少;流式细胞术TUNEL检测结果显示细胞凋亡和坏死同时存在。

The method is :there are two perpendicular axes whose distance are controlled ,one is the axis of work table, the other is fixed with a microscope for aiming.

该测量方法是:两个相互垂直且间距可调的数控回转轴,一轴与工件的回转中心重合,另一轴上固定可移动的瞄准显微镜,当显微镜瞄准被测孔时,两轴的转角由各自的圆光栅测出,两轴之间的角度位置确定曲面壳体零件上小孔的孔位置,同时采用CCD摄像头,利用图象处理技术实现小孔的尺寸测量。

In addition, molecular orientation behaviors induced by shearing, electric field and magnetic field were investigated. The space group of the monomers A3EO7 and A9EO7 were determined as P2〓2〓2 and P112/m by means of electron diffraction and X-ray diffraction. Liquid crystalline properties of the monomer and the polymer were studied using DSC, variable X-ray diffraction, TEM and polarized optical microscope. Both monomers exhibit monotropic liquid crystalline behavior, and they also give a metastable phase on the cooling process. The polymer PA9EO7 shows enantiotropic liquid crystalline properties. Thus the rigid polymer backbone is not a fatal defect that completely distorts the packing arrangement of the mesogenic moiety in the side chain liquid crystalline polyacetylene.

结合电子衍射倾转方法和粉末X射线衍射技术,确定了两个液晶小分子A3EO7和A9EO7的晶胞参数和空间群,采用Cerius〓模拟软件,运用分子模拟的方法给出了小分子在晶胞中的排列方式;利用DSC、变温X射线衍射技术和透射电子显微镜研究了小分子和聚合物的液晶态,单体A3EO7和A9EO7表现出单向液晶性质,并且在降温过程中都表现出一个亚稳液晶相或亚稳结晶相,聚合物PA9EO7具有双向液晶性;采用偏光显微镜和X射线平板照相技术,研究了剪切和电场对聚合物分子取向的影响,在不同的液晶态,剪切作用对聚合物PA9EO7具有不同的诱导取向结果,直流电场可以诱导聚合物联苯液晶基元沿施加电场方向取向。

By dehydrochlorination reaction the poly[(2-methoxyl-5-octyloxy)phenylene vinylene] is synthesized and the material"s structure is characterized by nuclear magnetic resonance spectroscopy, infrared absorption spectrum, ultraviolet and visible spectrophotometry. At the meantime, the fluorescence spectrum is measured and the mechanism of fluorescence occurring is analyzed. Thermal Gravimetric Analyzer"s results show that the MO-PPV"s thermal stability is fine. Also the experiment of resolvable property indicates that the MO-PPV can well dissolve in chloroform. Through analyzing the film"s surface by Metaloscope and Atomic Force Microscope, the good filming is found.

通过脱氯缩合法合成了聚(2-甲氧基-5-辛氧基)对苯乙炔,并分别用核磁共振波谱法、红外吸收光谱法、紫外-可见分光光度法等对其进行了结构表征;测量了样品的荧光光谱,分析了荧光产生的机理;热失重仪分析了材料的热稳定性,研究表明MO-PPV材料具有良好的热稳定性;溶解性实验发现材料在氯仿中溶解性较好;金相显微镜和原子力显微镜研究了薄膜的表面形貌,发现该材料的成膜性良好;材料的导电性研究表明,固体材料在掺杂下才可以表现出导电特性,而配成溶液的材料导电性因溶剂的不同而不同,并随溶解时间的长短发生变化。

Pristine Li-Al LDHs are synthesized by hydrothermal process in different reaction conditions by varying the aging time for 1 and 24 hours. Both the Li-Al layered double hydroxides (abbreviated as Li-Al LDH1 and Li-Al LDH24 for aging time 1 hour and 24 hours, respectively) were modified by using sulphanilic acid sodium salt hydrate, modified agent to form modified Li-Al LDH1-SAS and Li-Al LDH24-SAS. The morphology of the pristine layered double hydroxides are investigated by using wide angle X-rays diffraction, scanning electron microscopy and particle size analyzer which indicates that the crystallinity and aspect ratio is increased with increasing the aging time from 1 hour to 24 hours. The particle size of Li-Al LDH24 and Li-Al LDH1 are found to be ~1000 nm and ~250 nm, respectively. Both the pristine and modified LDHs are characterized by XRD, FTIR spectra and thermogravimetric analysis.

本研究目的在於改变长晶时间的长短,合成出同径大小的Li-Al LDHs,再经由改质剂sulphanilic acid sodium salt hydrate将Li-Al LDHs无机层材表面有机官能化制备出改质型Li-Al LDHs-SAS,於是进一步藉由扫描式电子显微镜、射径仪和穿透式电子显微镜等仪器分别观察LDHs改质前和改质后其主层结构型态上的变化;从中可以发现Li-Al LDHs随著长晶时间的增加其径有随之增大的趋势,但经有机化改质后其径会由於改质环境的影响明显低许多,针对此现象本实验将未改质和改质后之Li-Al人工无机层材制备成复材进一步探讨其在热性质和难燃特性上的为表现。

Its rule of change was obtained. On the basis of other studies, the flocculation kinetics and flocs structure was studied. By making some assumptions, collision frequency were presented. Then the the flocculation kinetics model was established through population balance equation. Comparison of experimental data and modeling results indicate that there are the same trend between the two. So the model can predict flocs number and size during flocculation of Yellow River's loess particles without using empirical parameters. The TEM and SEM were used to obsever flocs in the study of floc structure. The flocculation was divided as flocculi, floc and floc aggregate. The flocs structure model was established by assumption that particles position in floc accords with tetrahedron. The fractal dimension of model and experimental flocs was found to be coincident. So the model can reflect the structure of flocs formed in flocculation of Yellow River's loess particles by macromolecule flocculant at a certain extent.

最后,本文还对絮凝动力学和絮体结构进行了研究,在前人研究的基础上,针对高分子絮凝黄河泥沙,对絮凝过程作了一些符合试验条件的假设,建立了颗粒碰撞频率表达式,应用了颗粒数量平衡方程,从而建立了絮凝过程的动力学生长模型,模型计算结果与试验数据对比表明,二者趋势一致,在没有使用经验参数的情况下基本上能够描述黄河泥沙絮凝过程中絮体数量和尺寸分布的变化过程;对絮体结构的研究中,应用扫描电子显微镜和透射电子显微镜对絮体进行了观察,将絮体分为絮粒、絮团和絮网三个不同的生长阶段,通过假设颗粒结合位置符合正四面体,建立了絮体结构模型,计算得到的模型絮体分形维数基本与试验中的实际絮体相符,在一定程度上能眵反映高分子絮凝黄河泥沙生成的絮体结构。

The polyurea coating was tested with Taber tribomachine and the highp ressure water jet erosion tester for studying the wear behavior of polyure coating under conditions of dry friction and highspeed water jet contained sand. The morphology of the coating was observed with SEM and Chromatic confocal 3D Profiler. The surface component of test samp les was measured by FT2IR Spectrometer and Electron Energy Disperse Spectroscopy. The p roperties of polyurea coating under two testing conditionswas analyzed.

为研究聚脲涂层在干摩擦条件下和高速含砂水流冲蚀条件下的性能变化情况,用 Taber 磨损试验机和高速含沙水射冲蚀磨损试验机测试了聚脲涂层的磨损性能,用扫描电子显微镜和白光共焦三维轮廓仪观测涂层的磨损表面形貌,用表面红外光谱和电子显微镜能谱元素分析了涂层表面试验前后的组分变化,分析了涂层在2种摩擦条件下的磨损情况。

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