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The fabrication of fibers was attempted. The copolymers, the copolymers containing MOCT and the copolymer films containing MOCT were characterized by using Fourier Transform Infrared Spectroscopy, Scanning Electron Microscopy, Differential Scanning Calorimetry, Thermogravimetric Analyzer and X-ray Diffraction etc. The conclusions were summarized as following,1. The AN/MMA copolymers were testified that copolymerization of most AN and MMA occurred and the ratio of AN and MMA in copolymer was less than the ratio of monomers. With the increase of the contents of MMA, the viscosity of copolymer solution, molecular weight and decomposition temperature of copolymers increase.

通过傅立叶变换红外光谱、扫描电子显微镜、差示扫描量热分析、热重分析、X-射线衍射分析等测试方法对得到的AN/MMA共聚物、含有正十八烷微胶囊的共聚物以及共聚物膜等进行了测试和分析,得到如下的研究结论: 1、丙烯腈—甲基丙烯酸甲酯之间发生了聚合反应,共聚物的组成比略小于投料比;共聚物的粘度和分子量随着第二单体MMA加入量的增加有增大的趋势;第二单体加入量的增大使得共聚物的分解温度升高,通过热重分析证实当AN/MMA摩尔比为85/15时,共聚物的耐热稳定性较高。

The matrix composites for diamond tools were tested with such modern testing instruments and equipments as DTA-7 differential thermal analyzer, JCXA-733 electronic probe and scanning electron microscope, JEM 2000 FX Ⅱ transmission electron microscope, eXL energy spectrometer, and humidity test instrument. The analysis, comparison, and induction of the testing results prove the enhancing effects of the rare earth on the matrix composites: degeneration, micro-alloying, purification, and catalytic activation. The comprehensive function of these effects leads to the decrease in the porosity of the matrix composites and to the increase in such actual indexes as the flexural strength, hardness, and impact ductility of the whole rare earth Fe-based diamond tool materials.

由DTA-7型差热分析仪、JCXA-733型电子探针及扫描电镜、JEM2000FXⅡ型透射电镜、eXL能谱仪以及莱茨2AP高温显微镜材料润湿性测试仪等现代测试仪器设备对金刚石工具材料进行了测试实验,对测试实验的结果进行了分析、比较和归纳,证实了稀土对胎体材料具有变性、微合金化、纯化和催化活化等四大强化作用机理,这些机理的综合作用导致了胎体材料孔隙率的降低和整个稀土Fe基金刚石工具材料抗弯强度、硬度及冲击韧性等实际使用性能的上升。

A Fourier transform infrared spectrophotometer, a solid state Si-NMR, a scanning electron microscope, an X-ray diffractometer, a thermogravimetric analyzer and a differential calorimeter were used to measure the structural and thermal properties of the WPU/silica hybrids.

研究中使用粒径分析仪、黏度仪与界面电位分析仪分析复合物乳液特性,利用傅立叶转换红外线光谱仪、固态核磁共振光谱仪、表面扫描电子显微镜、X-ray绕射光谱、热重量分析仪、示差扫描热卡计探讨混成复合物的结构、热性质与结晶情形,同时也利用万能拉力机、动态机械热分析仪探讨混成复合物的机械性质。

The crystallization of the blends were investigated by wide angle X-ray diffraction and polar light microscope . The results show that PPEKK in the blends deforms the crystallization of PPS but don't change its crystal structure.

用广角X射线衍射和偏光显微镜对共混物的结晶性能进行了研究,结果表明PPEKK对共混物中PPS的结晶作用有阻碍作用,但没有改变PPS的晶相结构。

The structure and morphology of the composites were investigated by X-ray diffraction and scanning electron microscopy.

利用X射线衍射和电子扫描显微镜对共聚物复合材料的结构和形貌进行了分析和表征。

The surface morphology and microstructure of products was characterized by scanning electron microscope and X-ray diffraction.

利用扫描电子显微镜和X射线衍射对样品的表面形貌和微结构进行了分析表征。

The phase compositions and the microstructures of the samples were investigated by an X-ray diffractometer and a scanning electron microscope, respectively.

利用X射线衍射仪和扫描电子显微镜分别对试样的相组成和显微结构进行分析。

MAIN OUTCOME MEASURES: At 1, 3, 5, 7, 14 days following immersion, microstructure of the sample surface was observed using scanning electron microscope. The structure of composite was analyzed utilizing X-ray diffractometer.

主要观察指标:于浸泡1,3,5,7,14 d后采用扫描电子显微镜观察样品表面形貌的显微结构,复合材料的结构采用X射线衍射仪进行表征。

The resultant particles were characterized by X-ray diffractometer and scanning electron microscope.

用X射线衍射仪测定出产物的相结构,用扫描电子显微镜观察产物的微观结构。

The optics microscope, X-ray diffractometer and different...

利用光学显微镜、X射线衍射仪和差热分析仪对不同金刚石的晶形、晶体结构和抗氧化性能进行了研究,并与同样工艺条件下合成的不含硼金刚石进行对比,对某些实验现象做了讨论。

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