时时地

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现；3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布；4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒；5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明：1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致；2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响；3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现； 3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布； 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒； 5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明： 1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致； 2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响； 3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

What he wanted for Sydney was the effect he had noticed when tacking round the promontory at Elsinore, of the castle's piled-up turrets against the piled-up clouds and his own billowing white sails; the liberation he had felt on the great platforms of the Mayan temples in Mexico, of being lifted above the dark jungle into another world of light; the height and presence of Gothic cathedrals, whose ogival shape was to show in the cross-sections of the Sydney roof-shells; and the curved, three-dimensional rib-work of boat-building , as he had watched his own father doing it at Aalborg.

当他在艾尔西诺海岬旁作之字形航行时，天边积云朵朵，海水蓝天融为一色，海风一过，巨大的白帆随之鼓起，城堡上层叠而立的塔楼在一片湛蓝中像条游龙飘忽不定。如此景致早已收藏于心。他所向往的悉尼巨作不正是这幅美景的再现么？当他伫立于墨西哥玛雅寺庙辽阔的平台之上时，那份无拘无束的洒脱正从昏暗的丛林中抽身而出，徐徐升腾，遁入另一个光的世界。这不羁的心不正是他想施予悉尼的么？还有那直插云霄的哥特式大教堂，它们的伟岸和雍容时时撞击着他，剖开未来悉尼歌剧院的扇形穹顶吧，横截面上所展示的不正是带着尖顶拱的外形么？当他在奥尔堡傻傻地看着父亲建造船坞时，那有着优美弧线的三维肋拱结构不也是激活他未来创作的源泉么？

So as technology hurtles forward, we must think back to that legacy.

因此，在技术不断地前进的同时，我们必须时时牢记这个光辉传统。

He's just as miffed as you the racer is at having to drive fifty-five miles per hour when the speedometer on the car clearly reads one hundred and fifty.

他的，正如miffed作为你赛车是在无需驱动器五十五英里每小时时，车速对汽车清楚地写著150 。

To be entirely free, and at the same time entirely dominated by law, is the eternal paradox of human life that we realise at every moment; and this, I often think, is the only explanation possible of your nature, if indeed for the profound and terrible mysteries of a human soul there is any explanation at all, except one that makes the mystery more marvellous still[29b].

要全然的自由，同时又要全然地受制于律法，这是我们时时感受到的人生永恒的吊诡；而这一点，我常常想，只能是你性情的唯一可能的解释，如果说对人性那深邃可怕的神秘，除了越说越神之外，的确能有什么解释的话 [29b]。

While in eastern sociaties, genarally,with narrow minds, the regimes have strong desire to monopolize eternally the supreme social treasures and power,so autocracy is the ruling way ,accompanied with lying-politics to centrelize the the will of the pople,within which a super-stable sociaty is created by doing all the upmost, and all the time and everywhere is peaceful life with songs and dancings,but reasonable depression and complaints are deemed illegal,thus the instability of the countries with clusters of social problems are surely formed,the reason is that those who are spiritualy depressed ang melancholy are many,among them the majority the elites will always remain such a spiritual state.

而东方社会一般都是由于政权的领袖集团心胸狭小，希望长期且永远地垄断全社会的财富与权力，因而实行的是专制主义政权，并且长期以慌言政治作为统一人心的主要手段。在慌言政治下，还要竭力营造一个越稳定社会，在这个社会里，总是处处时时歌舞升平，不允许发泄不满情绪，这样就决定了社会的不稳定因素众多，因为心理苦闷者多，尤其社会精英中的大部份人会永远有这种心态。

Whilein eastern sociaties, genarally,with narrowminds, the regimes have strongdesire to monopolize eternally the supreme social treasures andpower,so autocracy is the ruling way ,accompanied with lying-politicsto centrelize the the will ofthe pople,within which a super-stable sociaty is created bydoing all the upmost, and all the time and everywhere is peacefullife with songs and dancings,but reasonable depression andcomplaints are deemed illegal,thus theinstability of the countrieswith clusters of social problems are surely formed,the reason isthat those who are spiritualy depressed ang melancholyare many,among them the majority the elites willalways remain such a spiritualstate.

而东方社会一般都是由于政权的领袖集团心胸狭小，希望长期且永远地垄断全社会的财富与权力，因而实行的是专制主义政权，并且长期以慌言政治作为统一人心的主要手段。在慌言政治下，还要竭力营造一个越稳定社会，在这个社会里，总是处处时时歌舞升平，不允许发泄不满情绪，这样就决定了社会的不稳定因素众多，因为心理苦闷者多，尤其社会精英中的大部份人会永远有这种心态。

That is how the spirit of Jesus works to this day, always surprising us with something new.

耶稣的神就是以这样的方式，一直工作到现在，时时让我们惊喜地看到新事物。

They have pure hearts and only do what artists should do. They refused to cater to fashionable trends or walk through to cater for the vulgars, they never give up their pursuit for art. They never think about becoming a giant in this era, but they always think about what they can do for this era. I shall cherish their names in my heart, and I shall take their behaviors for example by me all the time.

怀着一颗赤子之心，始终只做一个艺术家该做的事情，他们不投时好，不敷衍媚俗，一刻也没有放松对美的追求，他们没有去想成为这个时代的什么伟人，但他们一直想着为这个时代去做点什么，他们的名字是值得我深深地藏在心里，他们的行为是值得我时时予以仿效的。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。