时基

The rate of c-kit+ cells in the heart increased gradually from E10 with the highest level of 12.6±3.2% at E11, which was nearly similar to the fetal liver, except for E12 when the c-kit+ cells was 3.4±1.2% in the heart compared to the fetal liver with 11.6±4.1% c-kit+ cells. The rate of c-kit cells in the suspension cells from the heart at E11 maintained stable after 24h culture based in the stromal cells of the heart and AGM region with the same conceptus age, but the rate of c-kit cells obviously decreased in the condition of the stromal cells from the fetal liver. The c-kit cells of the three conditions were all at low level at 48h without significant difference.

通过流式检测c-kit+细胞我们发现，胚胎期心脏和胎肝c-kit+细胞比率几乎一致，E11时c-kit+细胞明显增多，分别高达(12.6±3.2)%和(9.6±2.8)%，但E12时心脏中c-kit+细胞明显减少，仅为(3.4±1.2)%，此时胎肝中c-kit+细胞为(11.6±4.1)%。E11的悬浮细胞与心脏内皮细胞和AGM区基质共培养24h时，c-kit+细胞数量保持稳定，但在胎肝基质细胞中c-kit+细胞数量明显减少，在共培养48h，三组中的c-kit+细胞均呈较低水平，组间没有显著性差异。

Both of them showed no toxic effect on mice at the testing dose of 10 mg/kg. The 2,2-diphenyl-1-picrylhydrazyl free radical scavenging test showed that both of the formicary extracts were potent radical scavengers and their scavenging activities were dose-dependent. Furthermore, at higher concentrations (5～10 mg/ml) both of them exhibited significantly higher DPPH scavenging activity than butylated hydroxytoluene.

二苯基三硝基肼(1，1-diphenyl-2-picrylhydrazyl ，DPPH)自由基的清除能力的检测表明：两种蚂蚁窝甲醇提取物都具有显著的自由基清除能力，并呈现出剂量依赖性，而且，在高浓度时(5～10 mg·mL-1)，它们的自由基清除能力甚至显著地高于二丁基羟基甲苯(butylated hydroxyl toluene，BHT)。

Using solution culture experiment, discussed the influnce of nitrobenzene to the germinationrates and seedling growth of ten leguminous crops, and results showed that, when the nitrobenzeneconcentration was 1～100mg·L~(-1), it had little influnce to germination rates of leguminous crops,with the increasing of nitrobenzene concentration, emergence rates of leguminous crops decreased,but no significance compared with control, and found that the toxicity of nitrobenzene toleguminous related with the concentration, the thresholds of nitrobenzene toxicity to differentleguminous crops were different, under the test conditions, the inhibition of root was larger thanhypocotyl, according to the relationship between the inhition rates of root and hypocotyl length andthe nitrobenzene concentration, the sensitive order of the ten leguminous crops to nitrobenzenewas:small-seedsoybean＞kidneybean＞Dongnong42＞brownbean＞Dongnong49＞Dongnong46＞ormosia＞french bean＞black bean＞mung bean.

本研究探索了硝基苯对十种豆类作物的发芽率及幼苗生长的影响，结果表明：硝基苯浓度为1～100mg·L~(-1)时，对豆类作物发芽率影响不大，随着硝基苯浓度的增加，豆类作物出苗率有所降低，但与对照差异不显著，研究发现硝基苯对豆类作物的生物学毒性同浓度有关，硝基苯对不同的豆类作物的毒害阈值不同。

Caprolactam grafted carbon fibre could improve the initial crystallization temperature and the crystallization rate more obviously than ungrafted carbon fibre. The crystallization of nylon 6 was determined by nucleation. The nonisothermal crystallization dynamics was well coincident with the rule of both of Jeziorny and Liu equation. isothermal crystallization dynamics fitted to Avrami equation.

用广角X射线衍射法对晶型结构进行研究，表明碳纤维使原生态的样品中α晶型的含量降低，结晶度下降，其中接枝聚己内酰胺链段的碳纤维／MC尼龙6原位复合材料中α晶型的含量比未接枝的碳纤维／Me尼龙6原位复合材料的多，结晶度也较大：样品淬火时，碳纤维有利于基体尼龙6结晶时形成γ型晶体，接枝聚己内酰胺链段的碳纤维更有利于基体尼龙6结晶时形成γ型晶体；淬火后的样品在200℃下退火2个小时后γ晶型完全转变为α晶型。

In this thesis, investigations focused on heteropoly acids-catalyzed C-C and C-N bond formation reactions and the synthesis of xanthenediones and acridinediones under thermal conditions are described.1.12-Phosphotungstic acid has been used as an efficient,eco-friendly,and air- and moisture-stable catalyst to promote the direct dehydrative substitution of the hydroxy group of benzylic and allylic alcohols with variousβ-dicarbonyl compounds.

本篇论文主要描述了杂多酸催化下的C-C和C-N键的生成，以及无溶剂直接加热下合成十氢氧杂蒽二酮和9-芳基十氢吖啶二酮。主要内容如下：1。在磷钨酸催化下，1，3-二羰基化合物与醇能够顺利偶合，脱除一分子的水，生成烷基化的1，3-二羰基化合物。反应在甲苯中进行时，二芳基甲醇能与各类1，3-二羰基化合物反应，成率很高；但对于1-苯乙醇，只能得到很低的产率。

The results show that the introducing of multivinyl monomer and CaCO3 can slow down polymerization rate to different extent.Using 1％～5％ trimethylolpropane trimetbacrylateor divinyl benzene,tight encapsulation of CaCO3 can be realized and beyond 94％PS cannot be extracted. The amount of crosslinker or emulsifier should be accommodated when the load amount of CaCO3 is increased.CaCO3 content in the product increases consequently with the increase of the loaded amount of CaCO3,which can be known from FT-IR and TGA.TEM observations reveal that when the load amount of CaCO3 is 14.8％,most CaCO3 particles are encapsulated and each latex particle contains one CaCO3 particle.Composite particles have well-defined core—shell structure and the thickness of polymer shells is around 10 nm.However,the thickness of polymer shell decreases and many free CaCO3 particles appear when the load amount of CaCO3 reaches 29.3％and 58.7％,respectively.

结果表明，多乙烯基单体以及碳酸钙的引入会使聚合反应速率有不同程度的降低；使用1%～5%的TMPTMA或DVB，可实现PS对碳酸钙颗粒的牢固包覆，不可抽提的PS达94%以上；当碳酸钙用量改变时，需要适当调整乳化剂和多乙烯基单体的用量；IR和TGA的结果表明，随着碳酸钙用量增加，产物中的碳酸钙含量也相应增加；TEM照片和计算结果显示，当碳酸钙用量为14.8%时，绝大部分碳酸钙颗粒被包覆，且基本上每个乳胶粒中包覆一个碳酸钙颗粒，复合粒子具有清晰的核壳结构，壳层厚度约为10 nm，而当碳酸钙用量增加到29.3%和58.7%时，壳层厚度减小，并且出现较多裸露的碳酸钙颗粒。

Furthermore, influences of different phosphate salts at various concentrations on the ionization efficiency of phosphopeptide were investigated systematically, finding that the signal intensity for phosphopeptide 48FQEEQQQTEDELQDK63 digested from β-casein were 5 to 8 times increased in an optimized condition with 10 mmol/L ammonium monobasic phosphate or 3 to 4 times increased with 10 mmol/L ammonium dibasic phosphate as additive to matrix 2,5-dihydroxybenzoic acid, respectively.

考察了两种适合于磷酸化肽离子化的基质类型2，5-二羟基苯甲酸和2，4，6-三羟基苯乙酮。用2，5-二羟基苯甲酸作为基质时，当加入10 mM 磷酸氢二铵时，磷酸化蛋白质β-casein的磷酸肽 48FQEEQQQTEDELQDK63的离子化效率可以增强5-8倍，当加入10 mM磷酸二氢胺时，磷酸肽的离子化效率可以增强3-4倍。

Rodriguez isn't the only Yankee who needs a good October. When he looks around the clubhouse, he sees more teammates who have never won a title in New York than those who have. And thanks to the Rangers' picking up $67 million of the money left on his contract when he was traded to New York, Rodriguez can find three players in the same room to whom the Yankees are paying more this year -- Jeter ($21 million), Giambi ($19 million) and righthander Mike Mussina ($19 million)-- and a fourth, lefthander Randy Johnson, to whom they pay an equal amount ($16 million). Next year the Yankees will pay outfielder Bobby Abreu ($17.5 million) more than Rodriguez, making A-Rod a veritable bargain. I point out all of this to Rodriguez early this month as we walk underneath the first base stands at Yankee Stadium toward the indoor batting cage.

A-Rod并非洋基阵中唯一需要藉由季后赛杰出表现来证明自己价值的球员，环顾球员休息室，尚未为洋基拿到冠军戒指的队友甚至多过曾经办到的人，感谢游骑兵队愿意分担他天价合约中的六千七百万美元额度，在洋基阵中有三位球员从洋基老板的口袋中拿到比A-Rod更多的薪水– Jeter， Giambi，以及Mussina，另外还有和A-Rod并驾齐驱的Randy Johnson，下个球季洋基要付给Bobby Abreu的薪水也将超越A-Rod，这让A-Rod的交易看起来简直划算到不行，本月初，在一次和A-Rod一同走向洋基球场中的室内打击练习场时的谈话中，我向他提及这些数据

The following main results are obtained: The TiO_2 photocatalyst with small crystallite size, high surface area, narrow and uniform pore size distribution, and microporous frameworks could be prepared out by applying MW radiation in the preparation process. The microwave-induced fluorescence technique verified for the first time that microwave enhanced the formation rate of hydroxyl radical, leading to the increase in the photocatalytic efficiency. Compared with the conventional catalyst, TiO_2 prepared by MW dielectric heating owns a higher UV absorption ability, and its optical absorption edge and photovoltaic response are shifted toward the short wavelength region, resulting in increase of photooxidation efficiency. The photocatalytic conversion and the mineralization ratio of acetaldehyde are increased respectively by 30% and 40% over the TiO2 prepared by MW radiation when compared to the TiO2 prepared by the conventional heating. For the MW-assisted photocatalytic reaction over the MW-prepared TiO2, production of hydroxyl radicals is enhanced by 22.5%, and the photocatalytic conversion is accordingly increased by 20%. Similarlly, applying MW also increased the photocatalytic conversion and the mineralization ratio of acetaldehyde over TiO2/Al2O3 sample.

论文得到如下主要结果和结论：(1)微波介电加热TiO_2 溶胶可得到晶粒度小、光催化活性高、比表面积大和孔径分布窄而均一，且微孔发达的TiO_2光催化剂；在溶胶干燥处理过程中微波可使催化剂表面缺陷增加，进而导致光催化反应过程有更多的活性羟基自由基产生；(2)微波制备能显著增强TiO_2 样品的紫外光吸收率，并使其光吸收和光伏响应阈值发生蓝移，从而提高TiO_2的氧化还原能力；(3)与常规加热法所制TiO_2比较，微波法制备的TiO_2对乙醛的光催化降解转化率提高30%，CO_2生成率提高40%以上；(4)与未加微波辐射时相比，发现在光催化反应过程中施加微波，TiO_2 的羟基自由基生成速率提高了22.5%，相应CH_3CHO 光催化降解转化率提高了20%；对Al_2O_3/TiO_2催化剂，CH_3CHO 光催化降解转化率甚至提高了33%，同时CO_2 的生成率也都大幅度提高；(5)微波辐射可改变光催化降解乙醛的产物分布，推断施加微波时乙醛光催化降解按照羟基自由基引发的链式反应机理进行，微波&非热效应&起主要作用。

The corresponding relations between the strain of the static state and dynamic cycle load and the volume resistance of the short chopped carbon fibers, short chopped carbon mat, unidirectional carbon fibers reinforced vinyl resin composites is existed. The physical modes of these kinds of composites are also designed based on the experiment data. The resistance and strain of the short chopped fibers reinforced vinyl composites satisfy the equation of y =A + Bx + Cx~2 in the static strain test method and the short chopped mat reinforced vinyl composites is y = A + Bx.

短切碳纤维、短切碳纤维毡、单向碳纤维增强乙烯基酯树脂复合材料在静态和动态循环载荷下，应变与电阻之间有较好的对应性，同时根据实验数据，建立了不同条件下该复合材料应变和电阻变化规律的物理模型，短切碳纤维增强乙烯基酯树脂复合材料在静态拉伸时电阻与应变之间满足：y=A+Bχ+Cχ~2；碳纤维毡增强乙烯基酯树脂复合材料在静态拉伸破坏时电阻与应变之间满足：y=A+Bχ。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。