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Preparation of dehydrated gypsum phases of β-series in forms of hemihydrates, anhydrite and anhydrite in laboratory is presented in the paper.

本文介绍了β系列三种石膏脱水相——半水石膏、无水石膏和无水石膏的试验室制备条件。

The traditional methods to produce anhydrous ethanol were introduced briefly in this paper.

简要介绍了传统制取无水乙醇的方法,重点介绍了生物质吸附法制取无水乙醇的方法及国内外的进展情况,并对无水乙醇的制取方法进行了展望。

The bane argues to know data Endanger an effect healthily:NONE The environment influence:NONE The physics and chemistry bane:NONE Special bane:The AZO-FREE passes the ICP method analysis test to have no related of lead over 100 ppms, Ge over 5 ppms 9.5 a fires and the explosion danger The order:Obsolescent Combustible extreme limit(the air lie quality:Vol%):non-combustible product Apply to extinguish fire:The water,water sprays fog,carbon dioxide,the stem powder to extinguish fire a ,foam to extinguish fire The special sex protection equipments of the fire fighter:Need to go together with to take the goggle and anti-virus mask Very the rules a fire and the explosion danger:When the temperature hoick, the product meeting because of hot bulge cold but cause to open 9.6 Respond sex Stability:Under the normal regulations condition stability Environment should avert from:The water immerse,affect by damp and cold,clear fire perhaps the temperature is high in 500 ℃s Incompatibility:Have no Dangerous of decline a solution an outcome:Have no Dangerous polymer reaction:Will not take place 9.7 health dangers Dangerous way:Inhale, take, the skin and eyes get in touch with solid perhaps dust-The physics contact may result in allergic sex respond.

危害辩识资料健康危害效应:NONE 环境影响:NONE 物理性及化学性危害:NONE 特殊危害:AZO-FREE 通过ICP方法分析测试无相关之铅超过100ppm,镉超过5ppm 9.5火灾和爆炸危险闪点:不适用可燃极限:不燃物品适用灭火剂:水、水喷雾、二氧化碳、干粉灭火剂、泡沫灭火剂消防人员之特别性防护设备:需配带护目镜和防毒面具非常规火灾和爆炸危险:当温度急剧上升时,产品会由于热胀冷缩而导致开裂 9.6 反应性稳定性:在常规条件下稳定应避开的环境:水浸、受潮、明火或者温度高于500℃不相容性:无危险的降解产物:无危险的聚合物反应:不会发生 9.7健康危险危险方式:吸入,摄取,皮肤和眼睛接触固体或者灰尘----物理接触可能造成过敏性反应。

Due to the ability of the bivalent magnesium cation to form stable chelate complexes with carbonyl compounds,magnesium methylate for example is used as a selective carbonyl condensing agent. Three synthesis routes was proposed based on literatures and comprehensive comparison with other ways. First,Magnesium methylate is prepared by reacting magnesium metal with dry methanol.The magnesium salts of"higher"primary alcohols,i.e.alcohols with ≥ 2 carbon atoms,do not react directly with pure alcohols under normal conditions.In fact catalysts are required to set the reaction in motion and the preparation is performed under pressure at the higher temperatures.

一、直接合成法:本文将镁与无水甲醇直接反应制得甲醇镁;"更高级"的醇(比如C≥ 2的醇)在无催化剂的条件下无法直接和镁进行反应,本文以CCl4为催化剂将无水乙醇与镁直接反应制得乙醇镁,但是以原甲酸三乙酯为催化剂无水乙醇与镁无法反应;不论是以CCl4为催化剂还是以原甲酸三乙酯为催化剂,丙醇均无法与镁直接反应。

Due to the ability of the bivalent magnesium cation to form stable chelate complexes with carbonyl compounds,magnesium methylate for example is used as a selective carbonyl condensing agent.Three synthesis routes was proposed based on literatures and comprehensive comparison with other ways.First,Magnesium methylate is prepared by reacting magnesium metal with dry methanol.The magnesium salts of higherprimary alcohols,i.e.alcohols with ≥ 2 carbon atoms,do not react directly with pure alcohols under normal conditions.In fact catalysts are required to set the reaction in motion and the preparation is performed under pressure at the higher temperatures.

一、直接合成法:本文将镁与无水甲醇直接反应制得甲醇镁;"更高级"的醇(比如C≥2的醇)在无催化剂的条件下无法直接和镁进行反应,本文以CCl_4为催化剂将无水乙醇与镁直接反应制得乙醇镁,但是以原甲酸三乙酯为催化剂无水乙醇与镁无法反应;不论是以CCl_4为催化剂还是以原甲酸三乙酯为催化剂,丙醇均无法与镁直接反应。

Approach is to dip cotton balls ethanol scrub, scrub the parts, including LED, lens and mirrors, photosensitive surface, it is necessary to pay attention to ethanol must be pure, or else they will become more dirty washing, but also can use water After ethanol washing, the lens at the lens and reflectors Oh breath and then gently wipe clean swab until unabated until smooth.

处理方法是用棉球沾无水乙醇擦洗,擦洗的部件包括发光管、透镜及反光镜、光敏管表面,要注意无水乙醇一定要纯,否则会越清洗越脏,也可以在用无水乙醇清洗后,对准透镜及反光镜片呵一口气,然后再用干净的棉棒轻轻擦拭,直到光洁如初为止。

Approach is to dip cotton balls scrub ethanol, scrub the parts, including LED, lens and mirrors, photosensitive surface, it is necessary to pay attention to ethanol must be pure, or else they will become more dirty washing, but also can use water After ethanol washing, the lens at the lens and reflectors Oh breath and then gently wipe clean swab until unabated until smooth.

处理方法是用棉球沾无水乙醇擦洗,擦洗的部件包括发光管、透镜及反光镜、光敏管表面,要注意无水乙醇一定要纯,否则会越清洗越脏,也可以在用无水乙醇清洗后,对准透镜及反光镜片呵一口气,然后再用干净的棉棒轻轻擦拭,直到光洁如初为止。

The invention relates to a fabric nanometer following cleaning agent for obtaining TiO2/ZnO composite hydrosol, and relative production and cleaning method, wherein it uses butyl titanate and zinc acetate as predecessor, uses glacial acetic acid as catalyst and peptizer, uses water as solvent, uses absolute ethyl alcohol as the solvent of butyl titanate, and uses ethanolamine as deposit agent and supplies OH-, to be hydrolysed and polycondensated to form TiO2/ZnO composite hydrosol. And its components and mass percents are: butyl titanate at 1-15%; zinc diethyl at 1-12%; absolute ethyl alcohol at 1-20%; glacial acetic acid at 5-15%; and aminoethyl alcohol at 0.1-5%, and the left is water. The invention has lower cost and simple process.

本发明涉及一种可以得到TiO 2 /ZnO复合水溶胶的纺织品纳米后整理试剂及其制备工艺及对织物的整理方法,以钛酸丁酯和乙酸锌为前驱物,冰乙酸为催化剂和胶溶剂,水为溶剂,无水乙醇为钛酸丁酯的溶剂,乙醇胺为沉淀剂并提供OH -,经过水解、缩聚反应形成的TiO 2 /ZnO纳米溶胶整理剂,其组分和重量百分比含量如下:钛酸丁酯占1~15%;二水乙酸锌占1~12%;无水乙醇占1%~20%;冰乙酸占5%~15%;乙醇胺占0.1%~5%;水余量,具有耐洗性、无毒、无刺激、成本低廉、制作工艺简单可靠的优点,可实现对对织物的抗紫外、抗菌、抗静电功能整理。

The petrography and mineral chemistry characteristics of the two spinel-rich spherules show features of crystallization from liquids and their alteration taken place under non-oxidized surrounding.

岩石学和矿物化学特征表明,GRV 020025-3RI8和GRV 021579-3RI5都经历过熔融结晶过程,它们的蚀变均发生在非氧化的含水或无水的环境中。

In this paper, as a typical lewis acid, anhydrous aluminum (AlCl_3) was used as the catalyst to get PP/PS blends compatibilized by in-situ Fridel-Crafts alkylation. The effects on PP and PS components of AlCl_3 were investigated first, mainly by rheology, including steady rheology method and dynamic rheology method. Then the in-situ reactions in PP/PS alloys under different conditions were executed and studied in detail by selective Soxhlet solvent extraction. And at the same time, the evolutions of phase structures of PP/PS and the resulted PP/PS/AlCl_3 alloys were investigated by SEM and SALS. The steady and dynamic rheological behaviors of in-situ compatibilized PP/PS alloys were obtained systematically.

本文选用典型路易斯酸无水氯化铝(AlCl_3)作为催化剂,利用烷基化反应机理,对PP/PS合金直接进行原位催化反应增容,以流变学方法(包括静态流变和动态流变学方法)为主,详细探讨无水AlCl_3对PP/PS合金体系中PP和PS两组分的影响,并在此基础上进一步系统研究无水AlCl_3原位催化增容PP/PS合金的相结构演变及增容反应特征,然后对不同原位催化增容条件下获得增容合金材料的流变行为特征作了深入探讨。

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