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The histological sections, with HE and Masson's trichromic staining made, to evaluate the effectiveness of repair of bony defect. Results There existed new cartilage and new immature bone tissue in the bone substitute in 4 weeks after operation, as well as mass of cartilageous cells,osteoblasts, collagen tissue and more small vessels were seen.

方法高温法制备出磷酸四钙,然后在模拟体内环境下将其与无水磷酸氢钙发生水化固化反应,合成水泥型羟基磷灰石人工骨,将自制的CPC人工骨植入新西兰兔桡骨大段骨缺损模型中,术后4、8、12、16周取材,采用HE染色和Masson三色染色分析评价骨缺损修复效果。

Methods Tetra-calcium phosphate was prepared by high heating, than imitated the internal situation of humanbody, for hydrolization and solidation,to synthesize the hydroxy-calcium phosphate,as artificial bone in sement-type ,then im-planteted them into the large segmental defect of radius of New Silan rabbits model. The implanted materials were taken out at 4th, 8th, 12th, and 16th weeks after implantation. The histological sections, with HE and Masson's trichromic staining made, to evaluate the effectiveness of repair of bony defect.

方法高温法制备出磷酸四钙,然后在模拟体内环境下将其与无水磷酸氢钙发生水化固化反应,合成水泥型羟基磷灰石人工骨,将自制的CPC人工骨植入新西兰兔桡骨大段骨缺损模型中,术后4、8、12、16周取材,采用HE染色和Masson三色染色分析评价骨缺损修复效果。

Methods 100 mg of muscle of rat corpse was preprocessed before trimethylamine was extracted with anhydro-methylbenzene, then trinitrophenol was added into extracts, and yellow compounds emerged. The optical density was detected by spectrophotometer at 410 nm and the concentration of TMA-N was calculated using the standard curve. Results There was good linear correlation (R^2=0.9991, P.001) between OD and the concentration of TMA-N in the range of 1~10 mg/L.

大鼠肌肉组织样本100 mg经预处理后,将三甲胺抽提于无水甲苯中,与苦味酸作用,形成黄色的苦味酸三甲胺盐,用分光光度计在410 nm处检测吸光度,标准曲线法计算TMA-N含量。

The main factors that influence tablet hardness and disintegration time are wetting agent ethanol, agglutinating agent polyvinylpyrrolidone and tablet pressure.

确定了制片压力、润湿剂无水乙醇和粘合剂聚乙烯吡咯烷酮为影响崩解时间和片剂硬度的主要影响因素。

He thought his happiness was complete when, as he meandered aimlessly along, suddenly he stood by the edge of a full-fed river.

他漫无目的地东游西逛,突然在河边停住了脚步,一条盈满水的河。这时他觉得自己幸福到极点了。

Dimethyl carbonate was used as the methylating reagent, o-vanillin as the material and K2CO3 as the catalyzer to synthesize oV. The effect of material ratio, reaction time, reaction temperature and catalyzer dosage on its synthesis reaction was investigated.

方法]采用碳酸二甲酯作为甲基化试剂,以邻位香兰素为原料,无水碳酸钾为催化剂,合成邻藜芦醛,研究物料配比、反应时间、反应温度和催化剂量对反应的影响。

Part I, the Friedel-Crafts acylation on DAA and methyl dehydroabietic acid was carried out with acetyl chloride, benzoyl chloride or phthalic anhydride as acylating regents, anh- ydrous aluminum chloride as catalyst and with different solvents to compare with, we have got t- hree new compounds.

第一部分,分别以脱氢松香酸和脱氢松香酸甲酯为底物,乙酰氯、苯甲酰氯、邻苯二甲酸酐为酰化试剂,无水三氯化铝作催化剂,采用不同的溶剂及反应条件进行傅克酰基化反应,得到3个新化合物。

Bromo-2-sulfolene (2) reacted with substituted benzoic acid salt s 3a~3c or alizarin yellow (3d) to give four novel allylic substitution products 4a~4d by esterification reaction, respectively.

以3,4-二溴环戊砜(1)为原料,在无水吡啶作用下发生消除反应,得到反应中间体4-溴-2-环戊烯砜(2),再分别与一系列取代苯甲酸盐3a~3c以及茜素黄GG(3d)发生酯化反应,合成出4种新环戊烯砜衍生物4a~4d,并用IR,1HNMR,MS,元素分析等表征了它们的结构。

Coconut water is sterile until opened.

心 得鲜椰子水是无菌的,开盖后宜马上饮用。

A study has been made on Synthesis of poly with diphenyl ether and terephthaloyl chloride as reactants, 1,2 dichloroethane as solvent, and aluminum chloride as catalyst.

研究了以1,2-二氯乙烷为溶剂,以无水三氯化铝/DMF为复合催化剂体系,在温和条件下,以二苯醚和对苯二甲酰氯为原料合成高分子量聚醚酮酮的方法。

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