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The preparation method comprises monomer synthesis and polymer synthesis. The polymer synthesis is that cyclopentadienyl sodium monomer is added into metallic cobalt complex-triphenyl phosphorus cobalt chloride under strict oxygen-free and water-free conditions, and then double inner alkyne or outer alkyne conjugate monomer is added in, and after reaction, the precipitation, filtering, abstersion and vacuum-drying are carried out, the large molecules polymer containing cyclopentadienyl cobaltocenium organometallic cobalt is obtained.

制备方法,包括单体合成和聚合物的合成,聚合物的合成是在严格无氧无水条件下,在金属钴配合物三-三苯基磷氯化钴,加入环戊二烯钠单体,随后加入双内炔或双外炔共轭单体,反应后沉淀,过滤,洗涤,真空干燥,得到含环戊二烯茂钴有机金属钴的大分子聚合物。

Eight hydrazone Schiff bases have been synthesized by the reaction of salicylaldehyde, o–vanillin, 2-hydroxy-1-naphthaldehyde with nicotinic or isonicotinoyl hydrazide in anhydrous ethanol respectively; Three thiosemicarbazone Schiff bases have been synthesized by the reaction of salicylaldehyde, o–vanillin, o–hydroxyacetophenon with thiosemicarbazide in hydrous-ethanol respectively.

主要包括以下五部分的工作: 1、以水杨醛、邻香草醛、邻羟基萘甲醛、邻羟基苯乙酮分别与烟酰肼和异烟酰肼按1:1的比例在无水乙醇中反应,制备了八种酰腙类Schiff碱;以水杨醛、邻香草醛、邻羟基苯乙酮与氨基硫脲在水-乙醇混合溶剂中反应,合成了三种Schiff碱配体,并对Schiff碱配体的结构进行了表征。

II: ① take a thin wire, one end with sand paper wipe, and then lightson alcohol to non-yellow flame ignition,② wire with the end of the water dip, and then dip a number of sodium chloride or anhydrous sodium carbonate powder,③ ignited a new spirit lamp (lamp wick is clean, pure ethanol),④ the stained sodium salt powder on the wire on the ignitiontip, when there is a sharpsmall yellow flame, which is sodium flame.

方法二:①取一条细铁丝,一端用砂纸擦净,再在酒精灯外焰上灼烧至无黄色火焰,②用该端铁丝沾一下水,再沾一些氯化钠或无水碳酸钠粉末,③点燃一盏新的酒精灯,④把沾有钠盐粉末的铁丝放在外焰尖上灼烧,这时外焰尖上有一个小的黄色火焰,那就是钠焰。

All experiments were carried out under the dry and oxygen-free argon atmosphere by using standard Schlenk techniques.

在无水无氧和纯的氩气保护下,使用Schlenk技术,用2-(C1CH2) C5H4N·HC1与2当量的C9H7Li在THF中冰水浴反应,以73%的产率得到3-(2-C5H4NCH2)C9H7(1)。

Four kinds of systematic solvents: hexamethylene, chloroform, alcohol and water were applied to extract the different components orderly from Maca, and the finger print spectra of the components were measured and analyzed by virtue of the two indexes.

测定了内蒙、甘肃、新疆的十种甘草的系统三溶剂氯仿、无水乙醇和水提取物的三维紫外指纹图谱、HPLC指纹图谱、红外指纹图谱,进行了共有峰率和变异峰率分析。

The methods of ultrasonic decolor ization for corn gluten meal and low velocity electric distilling extraction were studied in the tests.

研究超声波处理法对玉米蛋白粉进行脱色的工艺条件和电动搅拌方式提取玉米醇溶蛋白的最佳提取条件,确定最佳脱色条件是:以无水乙醇为溶剂,萃取温度50℃,料液比1:12,超声波处理25min;最佳提取条件是:料液比1:8,50℃水浴加热,低速搅拌提取3h,乙醇的浓度是75%。

In order to develop a highly- effective antitumor drug of retinoic acid,a new complex of nickel with all-trans retinoic acid has been synthesized in absolute ethanol,without oxygen in darkness and characterized by elemental analysis,molar conductance,IR,UV,and HNMR spectrometry. Its formula is best described as Ni2 .3H2O.

为了开发一种新型高效的维甲类抗癌新药,在无水、无氧、避光条件下合成了维甲酸镍的配合物,通过元素分析、摩尔电导、红外光谱、紫外光谱、差热及核磁共振氢谱测定了配合物的组成、结构和性质,其分子式为Ni2 。3H2O。

Physical technology can improve the dyeing ability of wool fiber and dyeing system, increase the wool quality.

物理技术可改善羊毛纤维或染色体系的染色性能,提高羊毛的加工质量;减少染整污水的排放,实现无水或非水染色,节约能源,有利于环保。

Because of advantages such as containing metal-free, so the organocatalyst has not the potential risk of leaching of toxic metal ion to the environment; generally has good catalytic activity, some might exhibit peculiar character and catalytic mechanism as enzyme; easily handled, can be performed in solution or air without the necessity of severe conditions like water-free a...

因为其不含金属离子,不存在有毒金属离子泄漏而造成环境污染;一般具有较高的催化活性,有些显示出类似酶的特性和催化机理;反应容易操作,可在溶液或空气中进行,不需要无水无氧等苛刻条件;价格一般比较便宜,易于制备、修饰和改性,可调控性大;易于与产物分离及从反应体系中回收等一系列&绿色&的优点。

Chaper 3: Aldol condensations of aromatic aldehydes with ketones under solvent-free condition to synthesize α,β-unsaturated ketones in good to excellent yields using PEG400 and powdered anhydrous K2CO3 as catalysts at 90℃or 120℃were described.

第三章:在无溶剂条件下,由PEG400 和无水K2CO3催化芳香醛与酮的Aldol 缩合反应合成α,β?不饱和酮,得到较高的收率。

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