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无水乙醇

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Chloro-2-hydroxypropyl trimethylammonium chloride was synthesized by using trimethylamine hydrochloride and epichlorohydrin as the raw materials and anhydrous as solvent.

无水乙醇作溶剂、三甲胺盐酸盐和环氧氯丙烷为原料合成了3-氯-2-羟丙基三甲基氯化铵,探索出最佳合成条件为:n∶n为0.95∶1,反应温度为40~50℃,反应时间为30m in,所得产品质量分数大于98%,收率达90%。

It is shown that polystyrene has been grafted on the surface of nmSiO2 particles and the grafting ratio is about 40%. The surface of nmSiO2 could be treated effectively by KH570in absolute ethanol at 25℃, 48h. The nmSiO2-g-PSt unpurified by toluene appear microsphere in which nmSiO2 particles are contained, whereas the purified one appear internet formed by many pieces. The grafting ratio of PSt on nmSiO2 surface could be influenced obviously by dispersion agents content and agitation speed, whereas the morphology of nmSiO2-g-PSt purified is rarely changed.

结果表明:常温下在无水乙醇介质中处理48h以上可获得良好的硅烷处理效果;PSt已接枝包覆于nmSiO2表面,接枝率约40%;经甲苯洗涤前nmSiO2-g-PSt呈多粒子包覆微球状,洗涤后呈单粒子包覆网状结构;分散剂用量、搅拌速度改变对接枝率有影响,但对包覆形态影响不大。

The specific properties of materials, such as the palate adhesion, dynamic cruor, anti-bacterial and the degradability of lysozyme, were studied, which provide valuable data for further application. The main creative ideas are listed as follows:(1) The water-retention chitosan/poly vinyl alcohol blend fiber was obtained by coagulating in 10% NaOH/ethanol solution, and the blend and crosslink due to GA can enhance the mechanical properties of fiber;(2) The controlled degradable chitosan/gelatin blend fiber was obtained by solution filature, and the mechanical properties were improved;(3) The N-acylchitosan with the different degree of substitution were successfully prepared, and the relationship between structure and properties was estabilished;(4) By a new solvent system of 6% NaOH/4% urea for cellulose, the blood anti-coagulant function films were prepared by blending cellulose with chitin;(5) In the same solvent system above mentioned, the anti-bacterial blend films based on cellulose and carboxymethyl-chitosan were prepared, and the relationship of DS and the anti-bacterial property was concluded;(6) The controlled degradable chitosan films was obtained by the chemical crosslink.

本论文的主要创新点:(1)以NaOH水溶液/无水乙醇为凝固液,采用溶液纺丝法制备出保水性壳聚糖/聚乙烯醇纤维,共混和戊二醛交联极大提高了壳聚糖纤维力学性能;(2)用壳聚糖和明胶共混,以溶液纺丝法制备出可控降解的壳聚糖/明胶纤维,并大幅度提高了壳聚糖共混纤维的干、湿态抗张强度;(3)确立了不同取代度N-酰基壳聚糖的合成方法及其膜的结构与性能的关系;(4)利用纤维素新溶剂6%NaOH/4%尿素制备出抗凝血性纤维素/甲壳素共混膜;(5)利用上述纤维素新溶剂制备出抗菌性纤维素/羧甲基壳聚糖共混膜,揭示了羧甲基壳聚糖取代度与抗菌性能的关系;(6)制备出可控降解壳聚糖交联膜。

The calcium was determined by xylenol orange-CTMAB-absolute ethyl alcohol complexation color in the gelatin.

以二甲酚橙—十六烷基三甲基溴化胺—无水乙醇络合显色体系测定了明胶中的钙。

Anhydrous alcohol and glacial acetic acid were used as component solvent, which the volume ratio was 2:1, zinc dust as reductant, reaction temperature was 25~35℃, reaction time was 2 h, the yield was 81%.

在还原反应中采用无水乙醇和冰醋酸的混和溶剂,两种溶剂的体积比为2:1,以锌粉为还原剂,反应温度为25~35℃,反应时间为2h,产率为81%。

FLD at high dose appears to be better than cimetidine for hydrochloric acid- induced model and ab-solute ethvl alco- hol- induced model.

茯苓饮500,1000,2000mg/Kg灌胃,对大鼠胃粘膜损伤有良好的保护作用,其中对盐酸和无水乙醇模型,茯苓饮高剂量优于cimetidine(P<0.05,或P<0.01)。

Methods 122 cases of ovarian cysts at ultrasound-guided puncture,took the allantoic fluid,ethanol inactivated cyst wall after normal saline washed cysts.

对122例卵巢囊肿在超声引导下穿刺,抽出囊液,生理盐水冲洗囊腔后无水乙醇灭活囊肿壁。

The main points included:the selection of the best level, the puncture point, angle and depth of needle; exhaustedthe allantoic fluid, pumped into pure ethanol and exhausted it after 5~10 minusts.

要点包括选择最佳层面,穿刺点、进针角度及深度;抽净囊液,注入纯无水乙醇保留5~10 min抽净。

Its absolute ethanol extracts had no obvious antioxygenation on oil.

无水乙醇作萃取溶剂对油脂的抗氧化效果不明显。

Using modified apple fruit RNA extraction method based on CTAB by adding a step of using KAc and absolute ethanol to precipitate pectin, high-quality total RNA was extracted from the leaf and the inflorescence of jackfruit (Artocarpus heterophyllus Lam.). The yields of total RNA were 74.7 μg/g FW for the leaf and 31.6 μg/g FW for the inflorescence.

以菠萝蜜的叶片和花序为材料,采用改良的十六烷基三甲基溴化胺法(在原来的提取方法基础上,使用乙酸钾和无水乙醇预先沉淀果胶),成功提取菠萝蜜叶和花序的总RNA,平均产率分别为74.7μg/gFW和31.6μg/gFW。

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