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无水乙醇

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The result indicated that KH-570 and the xylene modified nanometer silicon dioxide has the good dispersivity and the stability in the water and the absolute ethyl alcohol resolver.

结果表明KH-570和二甲苯改性的纳米TiO2在水和无水乙醇溶剂中有较好的分散性和稳定性。

However, the gelation tune was decreased with the increase of water amount and increased with the increase of ethanol amount.

在类似"两步法"中,通过同时使用的氢氟酸和氨水,凝胶化时间更短,其最佳条件是无水乙醇和水与正硅酸四乙酯的体积比各自是4和0.6,同时加入氢氟酸和氨水的体积比为1:1时,获得的比表面积最大。

Objective To validate the therapeutic effect of CT-guided percutaneous ethanol injection for the treatment of nonfunctional accident adrenal tumor.

目的探讨CT引导下经皮无水乙醇消融术对无功能性肾上腺偶发瘤的治疗价值。

The results revealed that the motor nerves and parasympathetic system would be blocked predicatively by epidural injection with alcohol or phenol glycerin .

硬膜外腔注射无水乙醇和酚甘油进行化学性神经根毁损对实验兔运动神经和植物神经的阻滞效果显著,三月后再次硬膜外腔置管无显著的出血禁忌。

In the course of the condensation of 2, 4, 6-triamino quinazoline with substituted benaldehyde, the solvent DMF was replaced by absolute ethanol and the dried 3A clathrates was used as the dehydrating agent in order to improve the yield.

在2,4,6-三氨基喹唑啉与取代苯甲醛的缩合过程中,用无水乙醇代替DMF作溶剂,并用干燥过的分子筛吸收反应过程中生成的水,从而简化了后处理的步骤,并提高了产率。

It includes the following steps: extract trivalent iron ion and divalent iron ion in water phase through organic extractant, get predecessor of; absterge it with secondary distilled water for2-3 times and get pure load metal predecessor of organic phase; mix organic phase of Mg2 and Fe3 with mol rate of 1:2 and introduce them into autoclave, add distilled water according to the rate of 3:1 or 4:1 of organic phase and water phase and airproof it, and then mix it fiercely, stripping with hydrothermal method at temperature between 200 degree C and 300 degree C and make them react for 2.5 hours; cool it to the room temperature under natural condition, separate liquid and centrifugalize it, absterge it with absolute alcohol for 2-3 times and dry it at temperature of 50 degree C for 30-180 minutes, then get product of magnesium ferrite.

包括如下步骤:通过有机萃取剂来萃取水相中的三价铁离子和二价镁离子,制得有机相前驱物;用二次蒸馏水洗涤2-3次,获得纯净的负载金属有机相前驱物;按照Mg 2 和Fe 3 摩尔比1∶2将有机相混合均匀后引入高压釜中,按照有机相与水相的比例为3∶1或4∶1加入蒸馏水,密封后,对溶液进行强力搅拌,水热反萃的温度在200-300℃之间反应2.5小时;自然冷却至室温,分液,离心分离,用无水乙醇洗涤2-3次,在50℃下干燥30-180分钟,得铁酸镁产品。

TiO2 powder was prepared from TiCl4 with addition of aqueous ammonia by changing Ti4 hydrogel into its corresponding alcogel followed by ethanol-thermal ,dryness and calcination.

用四氯化钛为原料,经氨水沉淀、水洗、无水乙醇洗涤得到Ti4醇凝胶,对Ti4醇凝胶进行乙醇热处理、干燥、焙烧制得了TiO2粉体。

From the azeotropic mixture from the top of the tower the absolute ethanol is prepared and returned to the oxidation and carbonylation system.

塔顶出来的共沸混合物按照工业乙醇脱水方法制备的无水乙醇返回氧化羰化合成系统。

The invention relates to a synthesis method of N-acetylaminoglucose, which comprises dissolving D-glucosamine hydrochlorate and alcohol at the mass ratio of 2-2.5:100, adjusting the pH value of the solution to 9-10, filtering, taking the filter liquor, mixing and adding acetic anhydride at the 50-60wt% amount of D-glucosamine hydrochlorate, mixing and reacting for 2h, using absolute ethyl alcohol to recrystallizing, filtering and recrystallizing via water, to obtain rod-shape food grade N-acetylaminoglucose.

本发明涉及一种N-乙酰氨基葡萄糖的合成方法。该方法的具体步骤为:将D-葡萄糖胺盐酸盐和乙醇按2~2.5∶100的质量比溶于水中,调节该溶液的pH值为9~10;过滤,取滤液,搅拌下加入乙酸酐,其加入量为原料D-葡萄糖胺盐酸盐量的50~60wt%;搅拌反应2小时后,用无水乙醇进行重结晶;过滤,晶体再用水重结晶,得棒状食品级N-乙酰氨基葡萄糖。

Study on treatment of coal tar waste water by chlorine dioxide;2. Determination of naphthalene in coal tar by capillary pillar gas chromatography

白色易挥发晶体,有温和芳香气味,粗萘有煤焦油臭味;蒸汽压 0.13kPa/52.6℃闪点:80℃;熔点 80.1℃沸点217.9℃;不溶于水,溶于无水乙醇、醚、苯,相对密度(水=1)1.16;相对密度(空气=1)4.42;稳定性:稳定;危险标记:8;主要用途:用于制造染料中间体、樟脑丸、皮革、木材保护剂等

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