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无水乙醇

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Sample of plant leaf was pulverized with absolute alcohol in a mortar to extract chlorophyll from the leaf.

将植物叶试样置于研钵中用无水乙醇研磨,使植物叶中叶绿素溶入乙醇中。

Put 3g chitosan into 50mL 1% CH3COOH solution, after dissolved completely, added 9mL H2O2 into this solution and the reaction took place at temperature of 80℃ for 3 hours. Filtrated the hydrolysate and then concentrated liquid to 20mL, neutralized liquid with 1% NaOH, added 200mL ethanol to extract hydrolyte, 3000r/min eccentricity, and then we could got all water-soluble canary yellow chitosan by vacuum-freeze drying.

称取3g壳聚糖,于50mL1%冰乙酸溶液中充分溶解,加入9mL过氧化氢,在80℃条件下水浴反应3h,水解液抽滤,滤液在60℃浓缩至20mL左右,1%NaOH中和后,加入体积比为10:1左右的无水乙醇,沉淀水溶性壳聚糖,3000r/min离心,将糖液真空冷冻干燥后可得淡黄色完全水溶性壳聚糖。

Methods Benzhydrylpiperazine was synthesized by condensation of chlorodiphenylmethane and anhydrous piperazine in absolute ethanol.

以二苯甲基氯和无水哌嗪为原料,无水乙醇做溶剂,两者经缩合制得二苯甲基哌嗪。

The other for: safrole, sassafras oil, safrole different 82 yuan / kg; 1 - phenyl -2 - propanone 2,500 yuan / kg; 3.4 dioxane methylene diphenyl -2 - propanone 7200 yuan / ton; Piperonal 1,000 yuan / kg; N-acetyl-o-amino benzoic acid 11500 yuan / ton; anthranilic acid 15,500 yuan / ton; Phenylacetate 15,000 yuan / ton; acetic anhydride 9900 yuan / ton; trichloromethane 4100 yuan / ton ; anhydrous ether 8500 yuan / ton; piperidine 58000 yuan / ton; methyl ethyl ketone 10,000 won / ton; sulfate 1,200 yuan / ton; hydrochloride 400 yuan / ton; ethanol 4200 yuan / ton.

另供:黄樟素、黄樟油、异黄樟素82元/公斤;1-苯基-2-丙酮2500元/公斤;3.4 亚甲基二氧苯基-2-丙酮7200元/吨;胡椒醛1000元/公斤;N-乙酰邻氨基苯酸11500元/吨;邻氨基苯甲酸15500元/吨;苯乙酸15000元/吨;醋酸酐9900元/吨;三氯甲烷4100元/吨;无水乙醚8500元/吨;哌啶58000元/吨;甲基乙基酮10000元/吨;硫酸1200元/吨;盐酸400元/吨;无水乙醇4200元/吨。

The other for: safrole, sassafras oil, safrole different 82 yuan / kg; 1 - phenyl -2 - propanone 2,500 yuan / kg; 3.4 dioxane methylene diphenyl -2 - propanone 7200 yuan / ton; Piperonal 1,000 yuan / kg; N-acetyl-o-amino benzoic acid 11500 yuan / ton; anthranilic acid 15,500 yuan / ton; Phenylacetate 15,000 yuan / ton; acetic anhydride 9900 yuan / ton; trichloromethane 4100 yuan / ton ; anhydrous ether 8500 yuan / ton; piperidine 58000 yuan / ton; toluene 5200 yuan / ton; methyl ethyl ketone 10,000 won / ton; sulfate 1,200 yuan / ton; hydrochloride 400 yuan / ton; anhydrous Ethanol 4200 yuan / ton.

另供:黄樟素、黄樟油、异黄樟素82元/公斤;1-苯基-2-丙酮2500元/公斤;3.4 亚甲基二氧苯基-2-丙酮7200元/吨;胡椒醛1000元/公斤;N-乙酰邻氨基苯酸11500元/吨;邻氨基苯甲酸15500元/吨;苯乙酸15000元/吨;醋酸酐9900元/吨;三氯甲烷4100元/吨;无水乙醚8500元/吨;哌啶58000元/吨;甲苯5200元/吨;甲基乙基酮10000元/吨;硫酸1200元/吨;盐酸400元/吨;无水乙醇4200元/吨。

Said preparation method includes: dissolving curcumin and polyvinyl pyrrolidone according to mass ratio of 1:4-1:15 in organic solvent (for example absolute ethyl alcohol, propyl alcohol, isopropyl alcohol and ethyl acetate), making reduced pressure distillation at 55-95deg.C to remove most of ethyl alcohol to obtain paste material, quickly pouring the paste material into a stainless steel disk, vacuum drying at 60-90deg.C in drying oven and pulverizing.

本发明将姜黄素和聚乙烯吡咯烷酮按质量比1∶4~1∶15溶于有机溶剂(如无水乙醇、丙醇、异丙醇、乙酸乙酯等),于减压蒸馏55-95℃下除去大部分乙醇至成糊状,迅速倒入不锈钢盘中,在60-90℃下真空烘箱烘干,用粉碎机粉碎,得到姜黄素固体分散体。

The effects of molar ratio of linoleic acid and ethanol, temperature , and amount of ionic liquid on esterification reaction were studied and the optimal reaction conditions were obtained, that is, n :n = 4:1 , at refluence temperature, with the amount of ionic liquid equaling 42wt.

研究了环境友好的BF4离子液体催化亚油酸等高碳脂肪酸与无水乙醇酯化反应,考察了亚油酸与乙醇的摩尔比、反应温度、离子液体用量等条件对亚油酸酯化反应结果的影响,优化了反应的工艺条件。

Anhydrous ethanol ; glacial aletic acid ; anhydrous aluminium ; ethyl acetate ; catalyzed esterize

无水乙醇;冰乙酸;无水三氯化铝;乙酸乙酯;催化酯化

The results show that the resulting product can be separated by the mixture of petroleum ether, aether and acetic acid (10:10:1, V/V). Among them, the oleic acid component can be eluted by the mixed solvent of ethanol and carbon tetrachloride (35:15, V/V), and then productivity of sodium oleoyl sarcosine can be obtained.

结果表明:用石油醚:无水乙醚:冰乙酸=10:10:1分离产物中的组分,再用无水乙醇:四氯化碳=35:15混合溶剂洗脱制备油酸组分,进而计算油酰肌氨酸钠的产率是可行的。

The fixative mixture was replaced by washing the specimens in precooled (-20℃) 100% methanol followed by washing with absolute ethanol.

先用-20℃预冷的无水甲醇洗固定好的样品,然后用-20℃预冷的无水乙醇洗。

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