无水乙醇

Finally, promising application fields and expected development are predicted, some suggestions for research and development of anhydrous ethanol in China are also put forward.

最后，展望了无水乙醇制备的发展前景，同时对我国无水乙醇研究与开发提出了一些建议。

Eight hydrazone Schiff bases have been synthesized by the reaction of salicylaldehyde, o–vanillin, 2-hydroxy-1-naphthaldehyde with nicotinic or isonicotinoyl hydrazide in anhydrous ethanol respectively; Three thiosemicarbazone Schiff bases have been synthesized by the reaction of salicylaldehyde, o–vanillin, o–hydroxyacetophenon with thiosemicarbazide in hydrous-ethanol respectively.

主要包括以下五部分的工作： 1、以水杨醛、邻香草醛、邻羟基萘甲醛、邻羟基苯乙酮分别与烟酰肼和异烟酰肼按1：1的比例在无水乙醇中反应，制备了八种酰腙类Schiff碱；以水杨醛、邻香草醛、邻羟基苯乙酮与氨基硫脲在水-乙醇混合溶剂中反应，合成了三种Schiff碱配体，并对Schiff碱配体的结构进行了表征。

The following dehydration techniques of ethanol: distillation ,molecular sieve separation,membrane separation and corn adsorption are mainly concerned.

介绍了采用精馏法、分子筛分离法、膜分离法和作物吸附法制备无水乙醇的方法及其近年来无水乙醇制备的新进展。

The results showed: at the reaction temperature of 25～30 ℃,hydrogen pressure of 1.0～1.5 MPa,Vethanol∶Vcyclopentadiene of 5～6∶1,the catalyst dosage of 4 %～5 % and stirring rate of 800 r/min.The conversion of cyclopentadiene was above 98% and the selec...

结果表明，在反应温度25-30℃，氢气分压为1.0-1.5 MPa，无水乙醇作为溶剂，V无水乙醇∶V环戊二烯为5-6∶1，催化剂用量为4%-5%，搅拌速度为800 r/min条件下，反应时间2~3 h，环戊二烯的转化率大于98%，环戊烯的选择性大于95%。

Through designing of composition and structure of the bioactive graded coating,innerstress and its distribution in the coating were analyzed and calculated, the resultsshowed that when composition distribution coefficient n was 1.5, a reasonable stressdistribution could be got, that was at the beginning of deposition the suspension containingrichly BG granules was used so that a rich BG granules layer, a good transitional layerbetween BG layer at the bottom and the coating could be obtained at the titanium alloy side,the bottom of the coating; the stress value near the interface and surface and its character,pressure stress or tensile stress, were decided by the character of its composition itself.Changing composition distribution coefficient n could only change the variation tendency ofstress in the coating, but did not change the stress distribution rule in the coating. Thethinner the coating is, the sharper stress variation in the coating is, which does not mean thatthicker coating is better because the thicker the coating is, the little the permitteddeformation of coating is, so the coating thickness should be thinner, for example, about50μm for bending applications, but for applications only bearing pure shear stress, such asroot of tooth implant, the coating can be thicker little, for instance, about 80～100μm. The study on electrification characteristic and electrophoresis deposition of HAand BG granules in aqueous and non-aqueous solution system found that EPD almost didn'toccur in aqueous solution system. However, because HA granules take position charges inabsolute alcohol, a homogeneous EPD be carried out on the cathode titanium alloy slice, but taking negative charge in absolute alcohol the BG granules not be deposited on the cathode. A guided HA crystallizing, 100～300nm, on surface of the BG granules be realized by metathetical reaction, which cover BG granules with HA microcrystals and make the covered BG granules taking position charges in absolute alcohol, sequentially realize the EPCD of the BG and HA granules on the cathode, so it is feasible to make a titanium alloy/BG/HA bioactive graded coating by making use of EPCD technology. The corrosion experiment of rich boron bioglass coating and plasma spray coating showed that split phase, rich boron and rich silicon phase, occurred during its preparation. In basic medium the corrosion behavior of 〓 BG coating showed uniformity corrosion, the corrosion mostly occurred at rich boron phase area, therefore batch formula design of BGshould avoid the occurring of split phase. The corrosion appearance of plasma spray coatingappeared a non-uniform corrosion, mostly occurred at the edge of the laminated HA moltendrops, and emerged an accelerated corrosion tendency, which will easyly lead to corrosioncrackles extending to the interface and the happening of osmotic interfacial corrosion, thatmay be one of the major reasons leading to the coating cracking-off in the later period. Thetesting results of thermal expansion coefficient of 〓 and 〓BG showed the thermalexpansion coefficient of 〓 BG matched with that of titanium alloy better, and 〓 BG couldsinter with titanium alloy into densification enamel layer at low temperature (720℃).

将Ti6Al4V合金在1000℃下进行真空热处理会降低其力学性能，且合金内的V元素会向表面富集，因此，钛合金真空热处理和表面涂层的烧结温度不能过高，即应低于其相转变点；通过对生物活性梯度涂层的组成和结构的设计，分析和计算了梯度涂层内的应力大小和分布，结果表明：对于本研究，当成分分布系数n=1.5时，可以获得较合理的涂层力学性能，即在沉积开始时，采用富含BG颗粒的悬浮液，以便在钛合金侧获得同底层BG有良好过渡的富BG涂层；梯度涂层界面和表面的应力大小、性质由材料组成本身的性质决定，改变成分分布系数，只能改变涂层内应力变化的趋势；涂层的厚薄不影响涂层内的应力分布规律，但涂层越薄，涂层内的应力变化越快，但这并不意味着涂层越厚越好，因为涂层越厚，涂层允许的变形越小，对于应用于弯曲受力部位的涂层而言，涂层应薄一点为好(50μm)；而对于仅纯受剪切应力的部位，如牙根种植体，涂层可适当加厚(80～100μm)；通过对HA和BG颗粒在水溶液体系和非水溶液体系中的带电特性和电泳沉积的研究发现，它们在水溶液体系中很难发生电沉积；在无水乙醇溶液中，HA颗粒带正电，可在阴极钛合金片上发生均匀的电泳沉积，而BG颗粒则带负电荷；利用复分解反应法，可以制得100～300nm的HA，通过诱导HA在BG颗粒表面结晶，可对BG颗粒进行表面包覆，获得了被HA包覆的BG颗粒，改变了BG颗粒表面的带电特性，使BG和HA颗粒在无水乙醇中均带上正电荷，从而实现了HA和BG颗粒在阴极上的共沉积。

A set of apparatus for determining solid-liquid equilibrium data at atmospheric pressure has been established. The solubility of sebacic acid in water, 20% ethanol aqueous solution, 50% ethanol aqueous solution, 80% ethanol aqueous solution and ethanol were determined. Wilson equation, ideal thermodynamics equation and λh equation were applied to describe solid liquid equilibria data.

建立了一套常压固液平衡测定装置，测定了癸二酸在水、20％乙醇-水溶液、50％乙醇-水溶液、80％乙醇-水溶液、无水乙醇体系中的溶解度，并用Wilson方程、热力学简化方程和λh方程模型对实验数据进行关联。

Results showed that the optimum extraction conditions are that extract with ethanol for four hours, soak the remains with boiled water for 40min, repeat 3 times, sedimentate with 2 times volume ethanol; the content of tea polysaccharides is increasing with the fermentation time in different piles of Yunnan Pu-erh tea, 0.45% tea polysaccharides obtained in the first pile, and 1.68% in the forth pile.

试验证明：最佳提取工艺为无水乙醇浸提4h，取茶渣，沸水提取40min，重复3次，2倍体积无水乙醇沉淀；&涯堆&是普洱茶制作过程中的一道特殊工序，是形成普洱茶品质特征最关键的一步，翻堆样中茶叶渥堆时间越长，茶多糖含量越高，一翻堆含量仅0.45%，到四翻堆上升到1.68%，以上均为干物质计。

The liposolubility is the major component in the extractum,and therefore,dehydrated alcohol and acetone may be used as the dewaxing solvent for the extractum.

无水乙醇和丙酮是理想的浸膏后处理和脱蜡溶剂。结论：该浸膏含较多的脂溶性成分，采用无水乙醇和丙酮作为浸膏的脱蜡溶剂是可行的。

The methods of ultrasonic decolor ization for corn gluten meal and low velocity electric distilling extraction were studied in the tests.

研究超声波处理法对玉米蛋白粉进行脱色的工艺条件和电动搅拌方式提取玉米醇溶蛋白的最佳提取条件，确定最佳脱色条件是：以无水乙醇为溶剂，萃取温度50℃，料液比1：12，超声波处理25min；最佳提取条件是：料液比1：8，50℃水浴加热，低速搅拌提取3h，乙醇的浓度是75%。

Absolute ethanol and a mixed solution of ethanol and benzene with the volume ratio of 1:1 are used as the solvents, and carbon disulfide and sulfur powders as the sulfur ions source, respectively.

分别以无水乙醇及体积比为1：1的无水乙醇与苯的混合溶液为溶剂，以二硫化碳和单质硫为硫源。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。