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无水乙醇

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Major procurement of goods: a three-chlorosilanes, dichloromethane, AE activity ester, 3-iodine Silane, special acid, pentyl chloride, triethylamine, thiadiazole, tetrazolylazo acid, 2 - Acetamide, tetrahydrofuran, the four-guanidine, isopropanol, five phosphorus trichloride, sodium vary bitter, acid, sodium phenylacetate, 6-2 silicon n-amine, Ethylacetoacetate , Methyl isobutyl ketone, potassium dihydrogen phosphate, aluminium oxide, DL methionine, N, N-dimethylaniline, NN-diethyl aniline, 4 sodium EDTA, Anhydrous sodium sulfate, ammonium sulfate, potassium sulfate, sodium acetate, sodium carbonate, DMC, formic acid, sodium chloride medicinal, oxalate, protopine, acetone, alcohol, acetic acid, vinegar Ethyl, butyl acetate, methanol, ethanol (anhydrous, industrial, medicinal), formaldehyde, Ye Jian (30%), hydrochloride (industrial-grade, refined grade, reagent level), sulfate (98%), Ammonia, calcium carbonate, chlorine dioxide, 6 - APA ,7-ACA ,7-ADCA ,7-ANCA, sulbactam, ceftazidime activity ester, Deng salt (hydroxymethyl-K, acid precursors Potassium, sodium dihydrogen methyl), resin, the enzyme, water treatment agent, Xiao Mo agent, demulsifier, flocculants, activated carbon, all kinds of medicinal materials, All kinds of additives

三甲基一氯硅烷、二氯甲烷、AE活性酯、三甲基碘硅烷、特戊酸、特戊酰氯、三乙胺、噻二唑、四氮唑乙酸、二甲基乙酰胺、四氢呋喃、四甲基胍、异丙醇、五氯化磷、异辛酸钠、苯乙酸、苯乙酸钠、六甲基二硅胺烷、乙酰乙酸乙酯、甲基异丁酮、磷酸二氢钾、三氧化二铝、DL蛋氨酸、N,N-二甲基苯胺、NN-二乙基苯胺、乙二胺四乙酸四钠、无水硫酸钠、硫酸铵、硫酸钾、醋酸钠、碳酸钠、碳酸二甲酯、甲酸、药用氯化钠、草酸、片碱、丙酮、正丁醇、冰醋酸、醋酸乙酯、醋酸丁酯、甲醇、乙醇、甲醛、液碱(30%)、盐酸(工业级、精制级、试剂级)、硫酸(98%)、氨水、碳酸钙、二氧化氯、6-APA、7-ACA、7-ADCA 、7-ANCA、舒巴坦、头孢他啶活性酯、邓盐(羟甲基钾、前体酸钾、二氢甲基钠)、树脂、生物酶、水处理剂、消沫剂、破乳剂、絮凝剂、活性碳、各种药用辅料、各种添加剂

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现;3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布;4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒;5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明:1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致;2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响;3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。

In a large test tube, dissolve 0.5 g (4.5 mmole) of semicarbazide hydrochloride and 0.5 g of anhydrous sodium acetate (or 0.8 g of sodium acetate trihydrate) in 4 mL of distilled water and 7 mL of ethanol.

在一个大试管中,用4 mL蒸馏水和7 mL乙醇溶解 0.5 g (4.5 mmole)的胺基氢氯酸盐和0.5 g无水醋酸钠(或0.8 g的三水合醋酸钠)。

METHODS:Ceftizoxime acid was prepared with 7-Amino-3-norcephem-4-carboxylic acid(7-ANCA)and AE-ester ceftizoxime acid as raw material;then ceftizoxime sodium was obtained through the reaction between ceftizoxime acid and sodium carbonate.

以粗品7-氨基-3-烷基头孢烷酸和AE活性酯为原料合成头孢唑肟酸,再与无水碳酸钠反应制得头孢唑肟钠;同时研究反应时间、乙醇用量和滴加时间、无水碳酸钠的用量以及pH值对产品质量的影响。

Wedgeplug O-Seal plug valves with their positive, no-leak features are not only recommended as the best general purpose valves for handling hydrocarbons, vegetable oils, solvents, etc., but are ideal for such tough service as butane, propane, butadiene, acetone, ethyl alcohol, ammonia, anhydrous ammonia, benzene, vinyl chloride, dry chlorine, Dowtherm, ethane, ethylene, hydrogen chloride, napthalene, oxygen, hydrogen, phthalic anhydride, dry phosgene, phosphoric acid, potassium carbonate, styrene, molten sulphur, sulphur dichloride and related services within a temperature range from -300oF to + 450oF within pressure limits of the valves.

楔塞O形密封旋塞阀具有积极的、无泄漏特性,不但是最好的通用的阀门,用于处理碳化氢,植物油,溶剂等,还特别适用于严酷的应用环境,如丁烷,丙烷,丁二烯,丙酮,乙醇,氨,无水氨,苯,氯乙烯,干氯,道氏热载体,乙烷,乙烯,氯化氢,萘,氧,氢,邻苯二甲酸酐,干碳酰氯,磷酸,碳酸钾,苯乙烯,融化硫,二氯化硫,以及温度在-184oC至232oC之间,压力在阀门额定压力等级范围内的有关应用。

In the present invention, platinum-carbon catalyst, perfluoro sulfonic acid resin solution and absolute ethyl alcohol are uniformly mixed under ultrasonic conditions; mixture is uniformly smeared on a micro-porous layer of carbon cloth or carbon paper in a brushing or printing method, and a traditional Pt/C gas porous electrode is obtained after drying; silicon oil is adopted to infiltrate into pores of a catalyst layer and a diffusion layer of the traditional Pt/C gas porous electrode, and then the ordering anti-drowning gas porous electrode is obtained after drying.

本发明是将铂碳催化剂、全氟磺酸树脂溶液和无水乙醇在超声波条件下混合均匀,采用涂刷或印制的方法将混合物均匀涂布到碳布或碳纸的微孔层上,干燥后制得传统Pt/C气体多孔电极;然后将硅油渗入到传统Pt/C气体多孔电极的催化层和扩散层孔隙中,干燥后制得有序化抗溺水气体多孔电极。

The results show that with the increase of deformation strains and thinning of Fe-Cr fibers, the saturation magnetization are about 140 A·m2/kg constantly, and the remanent magnetism and coercivity increase gradually.The magnetic properties of Fe-Cr fibers are invariant when the Fe-Cr fibers were preserved in absolute alcohol or air for more than 1 a. After Fe-Cr fibers heated in air at temperature higher than 300 ℃ for 1 h, the Fe-Cr fibers transform from ferromagnetic α-solution to paramagnetic2O3, and the saturation magnetization of samples decreases remarkably. With the increase of deformation strains, the thermal stability of thinner Fe-Cr fibers decreases.

结果表明:随着变形量的增大和Fe-Cr纤维的细化,纤维的饱和磁矩基本恒定(约140 A·m2/kg),而剩磁和矫顽力则逐渐增加; Fe-Cr纤维在无水乙醇和空气中储存一年以上,磁性基本保持不变; Fe-Cr纤维在空气中经300 ℃以上加热1 h后,逐渐由铁磁性的α-固溶体转变为顺磁性的2O3,饱和磁化强度显著下降;且随着变形量的增大,较细Fe-Cr纤维的热稳定性较差。

2 BJP direct toxicity on TEC NRK52E cell were subcultured on a 24-well plate (3×10〓/ml/well) and exposed to BJP κ or BJP λ in concentration 1, 5, 10, 20mg/ml for up to 24h, then the media was changed, and 〓H-thymidine was added for incubation for 18h at 37℃, the corporation was terminated, Acid-insoluble DNA was precipitated by adding 5% trichloroacetic acid radioactivity in the extracts was determined in scintillation counter.

细胞增殖的影响:将TEC株NRK52E以3×10〓/ml/孔分别加入24孔培养板,分别加入BJPκ与BJPλ(浓度1、5、10、20mg/ml)共同培养,均设3个复孔,24小时后加入〓H-TdR(1μCi/孔)在5%CO〓37℃孵育18小时,终止反应,加胰酶脱壁半小时后移到普通干燥试管,多头细胞收集器抽滤,用5%三氯醋酸,无水乙醇分别冲洗,烤干,冷却后加入闪烁液,放入液体闪烁计数仪测定放射性。

The line of isothermal adsorption with polysacharidcs adsorbent at 70℃, 80℃ and 90℃ respectively is determined by the method of frontal chromatography in this paper.

本文是在研究以多醣类物质作吸附剂制取无水乙醇的新工艺基础上,采用迎头色谱法测定了吸咐等温线,突验数据通过回归分析,获得符合Freundlich型的吸咐等温方程,计算值与实验结果吻合较好。

Results Except the normal control group, absolute alcohol lead to multiple gastric ulcerations in all animals. However, the frequency, number, and size of gastric ulcers were significantly reduced both in GWYQT group and western medicine group rats, especially in the GWYQT group animals.

结果 除正常对照组外,无水乙醇使各组大鼠均有糜烂或出血点形成,而中药组的糜烂、出血明显减少,较试验对照组为轻。

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