无反应的

The influence of synthesis parameters on the purity of sodium cyanate was investigated,such as the mole ratio of urea to anhydrous sodium carbonate,reaction time and reaction temperature.

研究了尿素/无水碳酸钠物质的量比、反应时间和反应温度等反应条件对氰酸钠产品纯度的影响。

After 14 weeks of operation, the structure of epineurium was in integrity and there was no obvious difference in perineurium and endonurium between two groups.

结果 术后 2周，A组炎性反应稍重于 B组；至 4周时两组的炎性反应程度相似，近端少许胶原纤维增生；8周时两组的炎性反应基本停止，胶原纤维增生稍明显；14周时两组神经外膜构成完整，束膜、内膜结构无明显差异。

Results: No severe side-effects were observed after taking the FS oral bivalent live vaccine capsule of dysentery. Milk side-effects such as bellyache diarrhea-s sick up and hypersusceptibility were observed in a few people. The total rate of side-effect was 3.94%.

结果：无严重副反应发生，服药后的副反应均为一过性的腹痛、腹泻、呕吐或过敏，总副反应发生率3.94%，主要以腹痛、腹泻为主。

Methane, oxygen and H_2O molecules are activated, ionized and dissociated into active particles such as CH_3~+, O~-, H_2O~+, CH_3, CH_2, CH, H,OH and O, by nonelastic collision with high energy electrons. The particles react with each other in the reactor to synthesize chemically products including gaseous oxy-hydrocarbons.We study the rule of reaction by changing electrical parameter, gas flow etc. Study the conversion of methane, selectivity of gaseous hydrocarbons and yield of methanol under different reaction condition.

针对常规甲烷催化转化和氧化偶联制备含氧化合物的问题，遵循国际化学科学研究前沿"绿色化学"原则，采用自然界存在丰富的CH_4、H_2O和O_2为原料，在绿色友好的常温大气压无任何催化剂的条件下，采用强电场电离放电加速电子及其激励气体分子的极端物理手段，在反应腔体内进行无任何环境污染的非平衡等离子体化学反应，将气体分子激发、电离、离解成CH_4~+、CH_3~+、CH_4~·、H_2O~+、H_2O~·、O_2~+、O(~1D)等活性粒子，生成气态烃及含氧碳氢化合物，整个反应过程实现零污染、零副产品。

Anhydrous alcohol and glacial acetic acid were used as component solvent, which the volume ratio was 2:1, zinc dust as reductant, reaction temperature was 25~35℃, reaction time was 2 h, the yield was 81%.

在还原反应中采用无水乙醇和冰醋酸的混和溶剂，两种溶剂的体积比为2：1，以锌粉为还原剂，反应温度为25~35℃，反应时间为2h，产率为81%。

The test results showed that under low ambient temperature and aphotic storage conditions jet fuel exhibited good color stability.Oxidation reactions,such as photo-catalyzed oxidation and radical oxidation,were the main reaction mechanism of color degradation,and copper played an important role in catalyzing the oxidation reactions.Under static thermal stability testing condi...

试验结果表明，喷气燃料在较低温度、无光储存条件下具有很好的颜色安定性；氧化反应是导致喷气燃料颜色变深的主要反应机理；静态热安定性试验条件下，喷气燃料的颜色随氧化时间呈相对稳定的加深趋势；氧化铝吸附脱除了喷气燃料中的一些原有氧化抑制剂，使喷气燃料在较高温度、有氧条件下易于发生氧化反应；铜在喷气燃料氧化变色反应过程中具有明显的催化作用。

The biomechanical tests showed that two kinds of artificial bones had not significant difference on compressive strength and Young\'s modulus(P＞0.05),while the flexural strength of nano-nacre artificial bone was less than the control group(P＜0.05).3.The results of CCK-8 showed that the difference were not significant in each group,the proliferation of osteoblast reached the peak at the 5th day;7 days after being co-cultured,the total protein content of study group was higher than control group and blank group(P＜0.05),while the difference between control group and blank group was not significantP＞0.05The difference of alkaline phosphatase activities among three groups was not significant(P＞0.05The SEM view showed that osteoblast attached and grew well in two kinds of artificial bone.4.X-ray photography showed that two kinds of powder started to degrade in 2 weeks;this phenomenon became more appear in 4 weeks,nano-nacre powder degraded faster than micron-nacre powder,while the hole shadow was easy to be found;in 8 weeks,all the femoral holes recovered and returned to normal bone mineral density in all groups.Analysis of tetracycline fluorescent double marks in the hard tissue grinding slices indicated that new bone grew fastest around the bone defect area in study group,while most slowly in blank groupP＜0.05 SEM(scanning electron microscope observation showed that nano-nacre powder degraded more quickly.The same result can be found through the demineralized sections morphometric analysis,and both of the composite artificial bones made from those two kinds of nacre powder had the good connection with the adjacent tissue in rats body without apparent inflammatory response.5.X-ray photography showed that rabbit\'s bone defects healed faster in study group since NNAB implanted than in control group since MNAB implanted.At 24 weeks after operation,bone density in radial defects had nearly accessed to the normal area,while lower in control group,and turned up nonunion in blank group;The checking of BMD showed that results in study group were higher than those in control group at 8,16 and 24 week(P＜0.05), and the difference between the BMD values in study group at 24 week and those in blank group was not significant(P＞0.05).The gross specimens showed satisfactory histocompatibility both in study group and in control group,with bone tissue growing from two sides into the center of implanted materials; Normal slices in HE stain and hard tissue grinding slices in Stevenel\'s blue/Van Geison\'s picro-fuchsin stain showed that the bone growth tendency was better in study group than that in control group,and the medullary cavity had been penetrated to the implanted materials in study group at 24 week;Analysis of tetracycline fluorescent double marks in the hard tissue grinding slices indicated that new bone in both groups grew fastest 8 weeks after surgery,while slow down at 16 week.

纳米珍珠层/消旋聚乳酸复合人工骨与微米珍珠层/消旋聚乳酸复合人工骨分别与成骨细胞共培养后，其各时间点CCK-8法检测值与空白对照无显著差异(P＞0.05)，成骨细胞均在第5天达到增殖高峰期；培养7天后，实验组细胞蛋白含量高于对照组及空白组(P＜0.05)，后两者之间则无显著差异P＞0.05碱性磷酸酶活性在三组间均无显著差异(P＞0.05电镜下可见成骨细胞在两种人工骨上都有良好生长贴附能力。4.X-ray显示两种粉体在大鼠股骨骨洞植入第2周时都开始出现了降解，第4周时更为明显，纳米珍珠层粉较之微米珍珠层粉降解更快，而空白对照组骨洞阴影仍可见，至8周时，则所有组骨洞均己闭合修复，X-ray下已不可见原钻孔痕迹，恢复正常骨质密度；硬组织磨片四环素荧光双标记结果显示纳米珍珠层粉植入组较其余两组在骨缺损区周围新骨生长速度更快，空白组速度最慢P＜0.05电镜观察及常规脱钙切片亦可见到纳米粉体降解较快；由以上两种原材料制得的纳米珍珠层/消旋聚乳酸复合人工骨与微米珍珠层/消旋聚乳酸复合人工骨在大鼠体内均与周围组织结合良好，无明显炎症反应。5.X-ray显示纳米珍珠层/消旋聚乳酸复合人工骨植入兔桡骨缺损区后其骨愈合速度较对照组微米珍珠层/消旋聚乳酸复合人工骨植入的快，至植入术后24周，实验组骨缺损区接近正常骨密度，对照组骨缺损区密度较低，空白组则呈现骨不连状态；骨密度测量结果显示术后8周、16周、24周实验组的骨密度值高于对照组(P＜0.05，24周实验组的骨密度值与术前所测得的正常值无显著性差异P＞0.05动物取材大体所见均显示组织相容性良好，骨组织逐渐由植入材料两端向中央生长；常规切片HE染色及硬组织磨片Stevenel\'s blue/Van Geison\'s picro-fuchsin联合染色均可见实验组骨缺损区长势优于对照组，至术后24周，实验组骨髓腔与材料已呈相交通状；硬组织磨片荧光显微镜下观察，两组材料在术后8周处于骨生长最快速时期，16周时速度开始减慢，术后4、8、16周时实验组的新骨生长速度均较对照组的快

Meantime, we further studied this reaction under microwave irradiation conditions and first introduced the concept of the solvent-free and no-catalyst in this reaction, expanded the olefination of organozinc halides reagents with aldehydes, enlarged the application scopes of this reaction.

同时在微波辐射条件下进一步研究了该类反应，并在该类反应中初步引进无溶剂、非催化的概念，扩展和完善了有机卤化锌试剂与醛的烯基化反应，扩大了其应用范围。

Latest researches in the catalysts for synthesis of carbamate by ammonolysis of dimethyl carbonate;2. Progress in the catalysts for synthesis of carbamates by ammonolysis of dimethyl carbonate;3.4,4′-Methylene diphenyl carbamatewas synthesized by ammonolysis of dimethyl carbonate, a substitute of phosgene, and 4,4′-diaminodiphenyl methane with anhydrous zinc acetate as catalyst.

用碳酸二甲酯代替光气，以4，4′-二氨基二苯基甲烷为原料，在无水醋酸锌催化剂的作用下，经胺解反应合成了4，4′-二苯甲烷二氨基甲酸甲酯；测定了MDC的熔点；采用傅里叶变换红外光谱和氢核磁共振对产品结构进行了表征；考察了反应温度、DMC用量、反应压力、反应时间、催化剂用量对MDC收率的影响。

The progress levels of symptoms after pathogen infection showed that interaction of gray leaf spot pathogen and host has differentiation or polymorphism. The progress levels of symptoms is different.The aggressively has polymorphism. The pathogenicity of different isolates in same cultivar has polymorphism, or the host reaction type of same isolate in different cultivars has polymorphism.The host reaction type has differentiation. There are seven types of host reaction in cultivar and inbred after infected by GLS pathogen:Rectangular lesion without chlorotic halo, Rectangular lesion with chlorotic halo,Irregular lesion without chlorotic halo,Irregular lesion with chlorotic halo, Spot lesion with chlorotic halo,Rectangular and irregular lesionand Rectangular and spot lesion. The host reaction type is coalesced lesion when disease severely. Frequency of each reaction types is different.

通过对玉米灰斑病菌侵染后的显症过程的系统观察，可在组织水平上说明该病菌与寄主互作反应存在分化或多样性：玉米灰斑病菌不同菌株侵染后显症过程表现出明显的差异；玉米灰斑病菌在侵袭力上存在多样性，菌株间对同一种品种的致病性表现多样化，或者同一菌株对不同品种侵染引起的寄主反应表现为多样性；病斑反应型的分化，玉米灰斑病菌侵染玉米品种或自交系后，主要有7种病斑反应类型，即RH型、RN型、IRH型(不规则形具褪绿晕圈病斑)、IRN型(不规则形无褪绿晕圈病斑)、SH型、RI型(长矩形与不规则形混合病斑)和RS型(长矩形与斑点形混合病斑)，若发病严重，病斑连成片，而且这些反应类型出现的频率也不同。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。