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The material is titanium alligation implant and has good biocompatibility. Till the end of follow-up, blood, immune or tissue reactions were not found. No peplos or cytoplasmic change was seen. Besides, titanium alligation corrosion or abrasion did not appear.

材料与组织的生物相容性反应:术中所用材料均为铁合金体内植入物,与人体组织的生物相容性好,到随访结束时,无血液、免疫、组织等反应,无囊膜形成及细胞质的转变;亦无钛合金腐蚀、磨损等材料反应的发生。

Complete antiemetic response, defined as no vomiting/retchingor rescue medication use, was measured through 24 h and 48 hafter surgery.

完全止吐反应的定义为无呕吐/干呕或无解救药物治疗使用,在术后24小时和48小时判断完全止吐反应。

Results:Monoclonal antibodies IH3,5A12,7E5,7F9 showed specific respo nse to NIH3T3-erbB2 cell and SKBR3 cell,no response to NIH3T3 cell.1H3 also boun d specifically to the extracellular domains of P185 protein that expressed by E.

结果:单克隆抗体1H3、5A12、7E5、7F9可与NIH3T3-erbB2细胞、SKBR3细胞特异性结合,与NIH3T3细胞无反应;1H3与原核表达的c-erbB2胞外区蛋白有特异性反应,而与无关蛋白KDR无反应。

The bane argues to know data Endanger an effect healthily:NONE The environment influence:NONE The physics and chemistry bane:NONE Special bane:The AZO-FREE passes the ICP method analysis test to have no related of lead over 100 ppms, Ge over 5 ppms 9.5 a fires and the explosion danger The order:Obsolescent Combustible extreme limit(the air lie quality:Vol%):non-combustible product Apply to extinguish fire:The water,water sprays fog,carbon dioxide,the stem powder to extinguish fire a ,foam to extinguish fire The special sex protection equipments of the fire fighter:Need to go together with to take the goggle and anti-virus mask Very the rules a fire and the explosion danger:When the temperature hoick, the product meeting because of hot bulge cold but cause to open 9.6 Respond sex Stability:Under the normal regulations condition stability Environment should avert from:The water immerse,affect by damp and cold,clear fire perhaps the temperature is high in 500 ℃s Incompatibility:Have no Dangerous of decline a solution an outcome:Have no Dangerous polymer reaction:Will not take place 9.7 health dangers Dangerous way:Inhale, take, the skin and eyes get in touch with solid perhaps dust-The physics contact may result in allergic sex respond.

危害辩识资料健康危害效应:NONE 环境影响:NONE 物理性及化学性危害:NONE 特殊危害:AZO-FREE 通过ICP方法分析测试无相关之铅超过100ppm,镉超过5ppm 9.5火灾和爆炸危险闪点:不适用可燃极限:不燃物品适用灭火剂:水、水喷雾、二氧化碳、干粉灭火剂、泡沫灭火剂消防人员之特别性防护设备:需配带护目镜和防毒面具非常规火灾和爆炸危险:当温度急剧上升时,产品会由于热胀冷缩而导致开裂 9.6 反应性稳定性:在常规条件下稳定应避开的环境:水浸、受潮、明火或者温度高于500℃不相容性:无危险的降解产物:无危险的聚合物反应:不会发生 9.7健康危险危险方式:吸入,摄取,皮肤和眼睛接触固体或者灰尘----物理接触可能造成过敏性反应。

Due to the ability of the bivalent magnesium cation to form stable chelate complexes with carbonyl compounds,magnesium methylate for example is used as a selective carbonyl condensing agent. Three synthesis routes was proposed based on literatures and comprehensive comparison with other ways. First,Magnesium methylate is prepared by reacting magnesium metal with dry methanol.The magnesium salts of"higher"primary alcohols,i.e.alcohols with ≥ 2 carbon atoms,do not react directly with pure alcohols under normal conditions.In fact catalysts are required to set the reaction in motion and the preparation is performed under pressure at the higher temperatures.

一、直接合成法:本文将镁与无水甲醇直接反应制得甲醇镁;"更高级"的醇(比如C≥ 2的醇)在无催化剂的条件下无法直接和镁进行反应,本文以CCl4为催化剂将无水乙醇与镁直接反应制得乙醇镁,但是以原甲酸三乙酯为催化剂无水乙醇与镁无法反应;不论是以CCl4为催化剂还是以原甲酸三乙酯为催化剂,丙醇均无法与镁直接反应。

Due to the ability of the bivalent magnesium cation to form stable chelate complexes with carbonyl compounds,magnesium methylate for example is used as a selective carbonyl condensing agent.Three synthesis routes was proposed based on literatures and comprehensive comparison with other ways.First,Magnesium methylate is prepared by reacting magnesium metal with dry methanol.The magnesium salts of higherprimary alcohols,i.e.alcohols with ≥ 2 carbon atoms,do not react directly with pure alcohols under normal conditions.In fact catalysts are required to set the reaction in motion and the preparation is performed under pressure at the higher temperatures.

一、直接合成法:本文将镁与无水甲醇直接反应制得甲醇镁;"更高级"的醇(比如C≥2的醇)在无催化剂的条件下无法直接和镁进行反应,本文以CCl_4为催化剂将无水乙醇与镁直接反应制得乙醇镁,但是以原甲酸三乙酯为催化剂无水乙醇与镁无法反应;不论是以CCl_4为催化剂还是以原甲酸三乙酯为催化剂,丙醇均无法与镁直接反应。

Biocompatibility of tissue and material: All the materials used in operation were interstitial implant of titanium alloy. To the end of follow-up, there were no reaction of blood, immunization and tissue, no peplos formation or changes in cytoplasm, and no reaction of materials such as alloy corrosion and worn out.

材料与组织的生物相容性反应:术中所用材料均为钛合金体内植入物,与人体组织的生物相容性好,到随访结束时,无血液、免疫、组织等反应,无囊膜形成及细胞质的转变;亦无钛合金腐蚀、磨损等材料反应的发生。

The results were as follows:(1) The spectral sensitivity response at 14 monochromatic light selected through 340nm to 605nm occurred in curve with multiple peaks, the primary peak in 340nm (ultra-violet) is the highest response rate of phototaxis (21%), the secondary in 524nm, and the rest in 400-440nm and 483nm in order;(2) The response rate of phototaxis is increasing as the relative intensity of light, it is showed as curves with inverse "L" shape in white light and the monochromatic light of 483nm, as an upward ladder at 524nm and a near straight line at 340nm. However, the response rate could be detected at the lowest intensity and not arrived to the summit at the strongest yet;(3) The effect of sex to response to the spectral sensitivity and intensity is not significant;(4) There was not significant photophobism response to light for the ladybird, the behavior probably derived from phototaxis or partly due to random movements. It can be concluded that both the spectrum and intensity of light stimulus gave rise to the phototaxis of P.

结果显示:(1)在340~605nm波谱内其光谱趋光行为反应为多峰型,峰间主次不明显,紫外340nm处峰最高,趋光反应率达21%,其它各峰依大小次序分别位于绿光524nm、蓝光400~440nm和483nm处;(2)随光强增强其趋光反应率增大,白光和483nm刺激时其光强趋光行为反应呈一倒"L"型式样,524nm时呈一阶梯型,340nm时为一较平直的线型;光强最弱时仍均有一定趋光率,最强时均未出现高端平台;(3)性别对其光谱和光强度行为反应均有一定影响,但影响不大;(4)龟纹瓢虫无明显的避光反应,其避光行为可能是趋光行为衍生或其随机活动造成。

Through the thermodynamic calculation of the reaction that aluminum and magnesium reduce anhydrous scandium chloride molten salt to prepare aluminium-magnesium-scandium master alloy, we got that the standard equilibrium constant of the reaction is 1.074 ×10~(19), and the experimental equilibrium constant of it is approximately 6.874 × 10~(14)under around 1200 K and 1 standard pressure, which demonstrate that the reaction can take place and proceed thoroughly.

通过铝镁热还原无水氯化钪熔盐制备铝镁钪中间合金反应的热力学计算,得出:在1200K左右温度,1标准大气压下,该反应的标准平衡常数K为1.074×10~(19),经验平衡常数K′约为6.874×10~(14),这说明铝镁热还原无水氯化钪熔盐法制备铝镁钪中间合金的反应能够进行,而且进行的很彻底。

First, the geometry optimization for 1-phenyldibenzophosphole and triphenylphosphine were carried out using quantum chemical AM1 method.

用量子化学AM1方法优化了1-苯基二苯并膦和三苯基膦的几何构型,比较了两种化合物的电子结构和空间结构,发现PDBP作为羰基合成铑膦催化剂的配体要优于三苯基膦;系统研究了PDBP的合成方法,其最佳合成条件为:在无水无氧的条件下,采用二乙胺锂与溴化四苯基膦摩尔比为3,反应温度为22 ℃,反应5 h,反应后酸化, pH值为1~2,产物收率可达到85%~88%。

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