散射

Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.

该论文在综述前人工作的基础上，开展了如下未见文献报道的创新性的研究工作：(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究，建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法，与以前的报道相比，灵敏度和分析时间均有很大改善；(2)使用荧光素钠作为背景荧光试剂，建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法，扩大了激光诱导荧光检测的应用范围，对难衍生化合物的分离分析提供了一种新思路和新途径；(3)以荧光素钠作为背景荧光试剂，建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法；(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物，为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。

Chapter 4:The interactions between bergenin,esculin,gallic acid and caffeic acidwith HSA in AOT/isooctane/water microemulsions were characterized for the firsttime using fluorescence spectroscopy in combination with UV absorptionspectroscopy,FT-IR spectroscopy,CD spectroscopy and dynamic light scattering technique.

第四章：利用荧光光谱法、紫外-可见吸收光谱法、圆二色性光谱法、傅里叶变换红外光谱法和动态激光散射技术首次系统研究了在AOT/异辛烷/水构成的反相微乳介质中岩白菜素、秦皮甲素、没食子酸和咖啡酸与HSA之间的相互作用。

A backscatter fiber is used to expand the width of laser pulse. A locking filter is added to dual F-P etalon. Photo Multiplier Tube is used to detect the intensity of light and a frequency tracking circuitry is designed.

使用散射光纤对激光脉宽进行扩展，在双通道标准具的基础上增加专用于频率跟踪的通道，使用光电倍增管检测光强，设计制作了基于采样的频率跟踪电路。

As the result of using Euclidean norm metric, the performance of traditional FCM clustering algorithm is subject to the structure of sample patterns in feature space.

一是针对SAR图象，提出了基于混合偏移Rayleigh分布假设的最小误差算法；二是针对低质量图象，提出了基于散射图SEM估计的MAP聚类算法。

Moreover, the intensity corresponding to surface excitation in effective energy loss functions decreases with the increase of primary electron energy.

在用Monte Carlo方法模拟电子与物质相互作用过程时，常用Mott截面描述电子与原子的弹性碰撞，而用介电函数理论描述电子的非弹性散射。

The numerical results show that this method is effective for solving 2D acoustical radiation and scattering problems in exterior domain.

给出的数值算例结果表明：该方法对于求解二维外域声辐射和散射问题十分有效。

The problems of acoustic radiation and scattering in infinite exterior domain are studied by employing fractal two-level finite element method.

应用二级分形有限元方法研究了无限大外域声辐射和散射问题。

Multiple'.'' reflections at front and back surfaces of the glass faceplate.

散射'。''或荧光在玻璃片前后面上多次反射引起的。

The vibration spectrum of CaWO 4 crystal was analyzed theoretically by means of factor group method in this paper.

本文借助商群方法对CaWO4 晶体的振动谱进行了理论分析，明确地指出了红外吸收光谱和喇曼散射光谱的激活结果。

First, based on the factorization theorem for lepton-induced hard diffractive scat-tering and the factorization framework of the nonrelativistic Quantum Chromodynamics for quarkonia production, We present a study of J/〓+jet diffractive productionin the direct photon processes at DESY HERA.

首先，基于轻子引起的inclusive硬衍射散射的因子化定理和重夸克偶素产生的非相对论QCD因子化框架，我们研究了DESY HERA对撞机上J／〓+jet的衍射直接光产生。

Recall that, in the Kolmogorov axiomatization, measurable sets are the sets which have a probability or, in other words, the sets corresponding to yes/no questions that have a probabilistic answer.

延期开工的Kolmogorov宣布要衡量所有套职能有限许多坐标限制在于衡量子寅。换句话说，如果是/否的问题回答f可看的价值观念在许多最有限坐标，然后它有一个概率的答案。

The experimental results showed that the algorithm can filter singular points and remain fixity of the target edge.

实验表明：基于模糊理论的图像智能滤波方法比常规图像滤波方法运算量小，它既能去除奇异点，又能保持图像中目标的边缘不变性，具有很好的滤波效果。