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The result indicates that those four resuscitation-inducing aromatic herbs mainly contain volatile oil ,and all contain alicyclic compounds; the volatile oil of Borneolum Syntheticum and Styrax both contain Sesquiterpenes of caryophyllene; as resin herbs , Styrax and Benzoinum both contain vanillin, resin ester and balsamic acid .

结果表明,四味芳香开窍药主含挥发油,均含有脂环化合物,并存在一些共有成分,如龙脑冰片与苏合香挥发油中均含有倍半萜类成分石竹烯;苏合香和安息香皆为树脂类中药,两者均含有香荚兰醛成分,尚含树脂酯,香脂酸等。

by summarizing and analysing the progress on studies of pharmacodynamic material basis of resuscitation-inducing aromatic herbs such as moschus,borneolum syntheticum,styrax,benzoinum, and exploring the generality of those herbs,to provide scientific reference for further studies on the relevance of common substance ,nature and the efficiency of restoring consciousness and inducing resuscitation of those herbs.the result indicates that those four resuscitation-inducing aromatic herbs mainly contain volatile oil ,and all contain alicyclic compounds; the volatile oil of borneolum syntheticum and styrax both contain sesquiterpenes of caryophyllene; as resin herbs , styrax and benzoinum both contain vanillin, resin ester and balsamic acid .

通过对芳香开窍药麝香、冰片、苏合香、安息香的药效物质基础研究进展的整理、分析,探索其共性,拟为深入研究该类药的共性物质—药性—开窍醒神效应之间的关联性提供科学参考。结果表明,四味芳香开窍药主含挥发油,均含有脂环化合物,并存在一些共有成分,如龙脑冰片与苏合香挥发油中均含有倍半萜类成分石竹烯;苏合香和安息香皆为树脂类中药,两者均含有香荚兰醛成分,尚含树脂酯,香脂酸等。

Anethole accounted for 82.65% of the whole oil. Selective isolation of anethole form the volatile oil was carried out using an inclusion crystalline method with 1,1,6,6- tetraphenylhexa- 2,4-diyne-1,6-diol inclusion complex with anethole . The crystal structure of the inclusion complex was determined by IR, 1^H NMR and single crystal XRD techniques.

采用包结结晶方法对小茴香挥发油中的对-丙烯基茴醚进行了选择性分离,以1,1,6,6-四苯基-2,4-已二炔-1,6-二醇作为主体分子,小茴香挥发油中的对-丙烯基茴香醚作为客体分子,D.D选择性地与之形成超分子包结物晶体。

Based on the retrieval and analysis of the Bibliographer, the methods of water-disitillation extraction, sametime-disitillation extraction and supercritical CO_2 extraction for the extraction of three typical kinds of natural substances in Zhejiang Province were evaluated exp...

论文在文献阅译和工艺原理分析的基础上,以浙江比较有特色的三种天然物质为研究对象,实验评估了水蒸气蒸馏、同时蒸馏萃取和CO_2超临界萃取等方法,研究了金柑挥发油、白玉兰花挥发油和香菇精等三种天然香精的不同提取工艺,重点研究了CO_2超临界萃取工艺与成份分析方法。

Based on the retrieval and analysis of the Bibliographer, the methods of water-disitillation extraction, sametime-disitillation extraction and supercritical CO_2 extraction for the extraction of three typical kinds of natural substances in Zhejiang Province were evaluated experimentally.

论文在文献阅译和工艺原理分析的基础上,以浙江比较有特色的三种天然物质为研究对象,实验评估了水蒸气蒸馏、同时蒸馏萃取和CO_2超临界萃取等方法,研究了金柑挥发油、白玉兰花挥发油和香菇精等三种天然香精的不同提取工艺,重点研究了CO_2超临界萃取工艺与成份分析方法。

Were extracted by sterilize distillation and analyzed by GC-MS, 69 constituents were identified according to NIST MS database, the main constituents were thymol, carvacrol, p-cymene, caryophyllene, terpineol. 27 constituents from this plant were discovered for the first time. The phytochemical study of this plant was also conducted.

通过水蒸气蒸馏法提取牛至挥发油,利用GC-MS现代技术分析,通过NIST质谱库检索,鉴定了挥发油中的69种成分,其主要成分为麝香草酚、香荆芥酚、对聚伞花素、石竹烯、松油醇等;其中27种化合物为首次从该植物中鉴定。

ConclusionMicrowave extraction has the highest yield in the shortest time. But volatile oil in Heracleum hemsleyanum Diels extracted by supercritical CO2 extraction or steam distillation has better quality. Thus the supercritical CO2 extraction is the best way.

结论微波萃取挥发油得率最高,时间最短;超临界CO2和水蒸馏法萃取挥发油的质量最好,因此使用超临界CO2是萃取牛尾独活挥发油的最佳途径。

This article reviewed the research progress of anti-bacterial and anti-fungal activity of volatile oil from kinds of aromatic Chinese herbs including aromatic herbs for relieving exterior syndrome, aromatic herbs for clearing heat syndrome, aromatic herbs for resolving dampness, aromatic herbs for resuscitation and aromatic herbs for warming and dredging meridians, and also reviewed our antibacterial experimental results of aetherolea from ramulus cinnamomi, Herba Schizonepetae, Herba Moslae,et al, which may provide new ideas for the development of volatile oil preparations.

本文综述了多种来源于芳香解表类、芳香清热类、芳香化湿类、芳香开窍类和芳香温通类的挥发油在抗细菌和抗真菌作用方面的研究进展,结合笔者对桂枝、荆芥、香薷等中药挥发油抗菌实验研究结果,为挥发油抗菌制剂的开发提供新思路。

The essential oil was extracted by the water streem distillation . And the components of the essential oil from Sonchus brachyotus were identified by GC-MS. Result: 36 components were identified and represented 89.49% of the peak of the essential oil.

采用水蒸气蒸馏法提取长裂苦苣菜挥发油,然后采用气相色谱-质谱联用仪分析和保留指数分析相结合的方法鉴定其挥发油的化学成分,结果:共鉴定出36种成分,所鉴定的组分占挥发油总离子流色谱峰面积的89.49%。

The number of components in steam distillation extraction for chafu was about 13,mainly containing Thymyl methyl ether,Beta-selinene and so on,which occupied over 18% in all components.

水蒸气蒸馏法和超临界萃取测定柴胡挥发油成分比较发现,鉴别峰的数量相对较少,水蒸汽蒸馏法提取的柴胡挥发油中鉴定出13个主要成分,占挥发油组分的18%以上,主要成分为百里基甲基醚、β—蛇床烯等;超临界萃取的柴胡低极性成分中鉴定出9个主要成分,占低极性组分的20%以上。

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