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The steam distillation. 2.Rotary evaporation distillation, 3.supercritical extraction for the extraction of volatile oil oriental arborvitae, the experiment results showed, 1.the best conditions for the extraction by rotary evaporation are NG:water:ethanol=l:4:4 sawdust under the conditions 50 ° C in temperature, atmospheric pressure 0.1 Pa, extract maximum extraction rate of 90 minutes.

对不同方法提取得到的侧柏挥发性物质的粗提物进行了的触角电位测定和行为测定,确定了利用水蒸气蒸馏、旋转蒸发蒸馏、超临界萃取三种方法进行侧柏挥发油的提取,并通过试验得到旋转蒸发仪萃取的最佳方法为:在木屑:水:乙醇=1:4:4;50℃温度;0.1个大气压的条件下,提取90min的提取率最高。

The results showed that most of the microbes could be inactivated for the ultra high pressure treatment, the accumulation of total volatile basic nitrogen was restrained, and the change of pH value was delayed. The shelf life of white shrimp was prolonged with the enhancement of high pressure. High pressure treatment could make fresh shrimp with boiled flavor in some degree. Trements of 400 Mpa and 600 MPa aggravated blackening. However, melanotic reaction was not observed during the whole storage of shrimp treated by 700 MPa. High pressure could change the metabolizing of ATP and its metabolites, but did not impact the metabolic pathway of AMP decomposition.

结果表明:超高压处理可以有效地杀灭南美白对虾中绝大多数微生物,抑制贮藏过程中挥发性盐基氮的积累,延缓pH值的变化,从而延长南美白对虾的货架期,且处理压力越高延长效果越显著;超高压处理会给鲜虾带来不同程度上的煮熟虾的风味;400 MPa和600 MPa处理使虾在冷藏过程的黑变提前,而700 MPa处理可以完全抑制南美白对虾黑变现象的发生;超高压能够改变腺苷三磷酸及其代谢产物的代谢情况,但不影响腺苷酸的代谢途径。

Of Fe , Cu in the metal phase and Mg, Si in the silicate phases to understand the processes of mixing of metal and silicate phases and further decipher the mechanism of formation of mesosiderite;(2) to study in detail the geochemical characteristics of each phase in the meteorite, to provide necessaryevidence for the model of formation of mesosiderite;(3) to study and update in detail the composition of each phase in the meteorite, and provide a new and complete set of data for understanding the mechanism of formation of mesosiderite.

Cu和硅酸盐相中的Mg, Si等中等挥发性元素的稳定同位素进行分析,判断中铁陨石的金属相和硅酸盐相混合过程的环境特征,进而阐明中铁陨石的形成机制;(2)对这块陨石的各相进行详尽的地球化学分析,通过这些相的地球化学关系判断中铁陨石的形成机制,对中铁陨石的形成模型提供必要的制约和证据;(3)全面更新对中铁陨石各矿物相化学成份的认识,为中铁陨石的成因之谜的全面揭开提供最新最完整的数据。

Flame retardants may interrupt or change the decomposition process in several ways:(1)they may melt at relatively low temperatures and resolidify in the form of a foam, which serves as a barrier to heat transfer from the flame to the substrate;(2) they may be converted upon heating into acids or bases, which catalyze the decomposition of the substrate at lower temperatures than are required for the formation of volatile combustibles;(3 ) they may decompose orsublime upon heating to release large amounts of nonflammable vapors which exclude oxygen from the flame; or (4) they may react with chemicakl species within the flame to stop the combustion reaction.

阻燃剂可以从几个方面干涉或改变织物的分解过程:(1)阻燃剂在相对较低的温度时会熔化,然后重新固化成泡沫状,这样就形成了一个屏障,阻止了从火焰向织物的热传递。(2)阻燃剂受热时会分解成酸或碱,这些酸或碱在低于可生成挥发性可燃物的温度下可以催化织物的分解。(3)阻燃剂在受热时会分解或升华,同时释放出大量不可燃气体,这就阻止了氧气对火焰的供应。(4)阻燃剂可以与火焰中的化学物质起反应,使燃烧反应终止。

The SPC-2S fraction with 30% EtOH were constituted epicatechin and epicatechin gallate ester ;The SPC-2S fraction with 50% EtOH contained epicatechin and dimeric procyanidins, another SPC-3S contained epicatechin ,dimeric procyanidins and trimeric procyanidns ;Dimeric procyanidins and trimeric procyanidns constitute SPC-5S fraction;monomer dimer trimer tetramer pentamer of procyanidins were the major fractions in 70% acetone elute solution.

1和 2.01:1,也以添加0.1%SPC酒样中两者的比例最为协调;对小曲酒中酸的影响表现为,添加SPC后有利于降低酒样中乙酸的含量,各酒样中乙酸的量随着SPC添加量高粱外种皮中原花青素及其对小曲白酒挥发性成分影响机制研究的增加而降低;对醛类的影响为,添加SPC可降低酒样中糠醛的含量,其中以添加 0.1%SPC酒样中含量最低,为对照组的39.3%,而4个酒样中乙醛含量则无明显差别;低SPC添加量有降低酒样中杂醇油含量的趋势。

The research suggested that American white oak is the best choice for the production of grape wine with strong oak aroma and European oak is the best choice for the production of grape wine with harmonious oak aroma, fruit aroma and wine aroma; air drying process of barrel plates would influence the content of total phenol, tannin and volatile substances including vanillin and MOL; and baking intensity will change original content of chemical compositions in oak and make oak barrel possess different aroma characteristics and phenol substance content.

研究表明,酿制橡木香较浓郁的葡萄酒选用美国白栎较好,酿造像木香、果香、酒香协调的葡萄酒则选择欧洲橡木较适宜;板材风干过程对橡木板材中的总酚、单宁含量及挥发性香气物质香兰素和橡木内酯的含量均有影响;烘烤强度可改变橡木木材原有的化学组分含量,使橡木桶具有不同的呈香特性和酚类物质含量。

The research suggested that American white oak is the best choice for the production of grape wine with strong oak aroma and European oak is the best choice for the production of grape wine with harmonious oak aroma, fruit aroma and wine aroma; air drying process of barrel plates would influence the content of total phenol, tannin and volatile substances including vanillin and MOL; and baking intensity will change original content of chemical compositions in oak and make oak barrel possess different aroma characteristics and phenol substance content.

研究表明,酿制橡木香较浓郁的葡萄酒选用美国白栎较好,酿造橡木香、果香、酒香协调的葡萄酒则选择欧洲橡木较适宜;板材风干过程对橡木板材中的总酚、单宁含量及挥发性香气物质香兰素和橡木内酯的含量均有影响;烘烤强度可改变橡木木材原有的化学组分含量,使橡木桶具有不同的呈香特性和酚类物质含量。

In the contaminated lard sample, 6 organic compounds have been thus identified to be the raw materials or byproducts in the production of organic tin compounds. Based on the identified contaminants, it can be postulated that the chemical structure of the organic tin compound is dibutyltin-bis-(2-isooctyl thioacetate). The method is simple and precise, and has not been reported in the local literature.Keywords Organic tin compound, Lard, SPME-GC-MS

经过摸索研究,采用固相微萃取方法富集挥发性杂质,直接注入色谱中,经色谱分离,质谱测定,确定了杂质的结构,由杂质成分推断生产有机锡所用的原料,然后判断合成路线,最后确定有机锡的结构,从有毒猪油中鉴定出2-巯基醋酸异辛酯、双(2-醋酸异辛酯)二硫、双醋酸异辛酯硫醚等6种与有机锡有关的杂质,并与相应的有机锡工业品对照,发现工业品中也含有这些杂质,与其合成过程的原料及副产物相符,从而确定有机锡化合物为二硫代醋酸异辛酯二丁基锡。

Second,we set the database of morphological characteristics of intercepted and captured bark beetle during quarantine,and the last,we studied the molecular identification of 15 species.The results were showed as below.1.Application of bark beetle semiochemicals in timber quarantine1.1 EAG and walking responses of bark beetle to different semiochemicalsSemiochemicals which can induce the olfactory response and aggregation behavior of bark beetle include host volatile components,pheromones secreted by bark beetles itself or synthesized with host compounds by bark beetles,and the compounds released by tissue of decaying wood under the pressure of microorganism after bark beetle colonization.

信息化合物在小蠹虫检疫中的应用1.1小蠹虫对各种信息化合物的触角电位及嗅觉反应能诱发小蠹虫产生嗅觉反应,进而使之产生聚集行为的信息化合物有很多种,主要包括:树木的挥发性组分;小蠹虫自身产生的信息素和寄生后转化寄主化学物质合成的信息素统称虫体信息素以及树木被小蠹虫寄生后,其组织在微生物作用下释放的物质。

For ozonolysis, the SOA yield has not been changed by inorganic seed aerosol, because the products are mainly carboxylic acids, which has much lower saturation vapor pressure and thus easily undergo homogeneous nucleation or gas-particle partitioning to be in the aerosol phase.

而对于α-蒎烯臭氧氧化的过程,实验结果表明,干态硫酸铵颗粒物种子的存在对SOA产率无影响,对臭氧氧化生成的SOA分子鉴别的结果表明,可鉴别组分中有很高比例的有机羧酸类物质,这一比例远高于光氧化产物,这些有机酸具有较低的挥发性而极易形成颗粒相,并且不参与异相酸催化反应。

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On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面,更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值,分为几个相等的区间作为横轴,并将各区间内所测定值依所出现的次数累积而成的面积,用柱子排起来的图形,也叫做柱状图。

You rap, you know we are not so good at rapping, huh?

你唱吧,你也知道我们并不那么擅长说唱,对吧?