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A novel synthetic approach of 3,3'-azobis(6-amino-1,2,4,5-tetrazine) was firstly devised. Taking 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine as a primary material, DAAT was synthesized by high pressure ammonolysis and potassium permanganate oxidation. Compared with the four-step reaction in the literature, this new approach was reduced to two steps with a yield of 58.1%. The intermediate and DAAT were characterized by elemental analysis, IR and NMR spectra.

自行设计了3,3'-偶氮双(6-氨基-1,2,4,5-四嗪)新合成路线、采用3,5-双(3,5-二甲基吡唑-1-基)-1,2,4,5-四嗪为原料,由文献报道的4步反应缩减为2步,经高压氨解、高锰酸钾氧化合成了DAAT,总收率大幅提高,达到58.1%,并采用元素分析、红外光谱、核磁共振光谱等进行了结构表征。

It can be used to synthesize a variety of α-aryl malononitriles and gave the yields of 50-96%.

参考文献报道的方法并经适当改良后,共合成了12个咪唑鎓盐。

Leone then reports the arrival of Asteria and Bajazet.

塞拉利昂则报道的到来asteria和巴雅泽。

And so there is no news to report about Auschwitz.

今天,在奥斯维辛,并没有可供报道的新闻。

In the present study,using PCR amplification and automatic sequencing of EDA gene coding region,we report five mutations identified in 6 Chinese families with XLHED, including three novel ones:p.M1T,p.L62P and

其中3个点突变(p.M1T、p.L62P和p.G195E)为国际首次报道的新突变。

On the basis of synthesis of the H+/K+-ATPase inhibitor omeprazole,seven benzimidazole derivatives were synthesized for the first time,and their structures were identified by 1H-NMR、MS and elementary analysis.

设计合成了7个未见文献报道的苯并咪唑类衍生物,经质谱、核磁共振氢谱和元素分析确定了结构。

Six novel dihydrobenzofuran and benzofuran neolignans compounds(1~6) were synthesized by knoevenagel reactiton,esterfication, biomimetic oxidative coupling ,DDQ dehydrogenation,reduction and hydrolysis with 4-hydroxybenzaldehyde and malonic acid as starting material.

以对羟基苯甲醛和丙二酸为原料,经Knoevenagel缩合反应,酯化、仿生氧化偶联、DDQ脱氢、还原和水解等反应步骤,合成了6种未见文献报道的苯并二氢呋喃新木脂素和苯并呋喃新木脂素类化合物(1~6)。

Berry: Yeah, but not as difficult as it's been reported.

贝瑞:是的,但不像报道的那么困难。

For the moment, there was nothing to do but carry on and hope the story would blow over.

一时间,我们毫无对策,只能继续工作,希望这篇报道的影响尽快平息。

On November 24 six people were killed in automobile accidents, and by the end of the week the Los Angeles Times was keeping a box score of traffic deaths.

二十四日有六人在车祸中丧生。到了那个周末,洛杉矶时报报道的车祸死亡人数达到了二十人。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。