报道的

The key step involves reduction-amination of benzamine and -acetonide glycealdehyde 20 synthesized from cheap and available ascorbic acid . The hydrolysis product of 21 condensed with triphosgene to get 6, key intermediates of Linezolid and Eperizolid. After a series of reactions, we got Linezolid and Eperizolid in reasonable yields and purity. The spectrum and 〓 values of compounds 6 and other intermediates were identical with literature reported.

我们以国内非常便宜易得的维生素C为原料合成得到-丙酮保护的甘油醛20，20和取代苯胺经还原胺化反应制备得到二噁烷21，21水解后与三光气缩合成环得到利奈唑酮和埃皮唑酮的关键中间体6.6经一系列的反应合成得到了利奈唑酮和埃皮唑酮。6及一些中间体的〓D值与文献报道的数据相吻合。

In order to direct the construction of plant germplasms by elucidating the relatives among plants at the level of gene, CYP86MF gene analogues from 11 species of 6 genera in Cuciferae were respectively obtained by PCR strategy using gene specific primers designed from conserved regions of CYP86MF gene reported. Sequence comparisonindicated that the similarities among the genes at nucleotide level were over 80%, and the similarities at amino acid level remained above 70%. The differences between the genes at nucleotide and amino acid level between species were 1.0%~ 5.7% and 2.6%~ 7.3% respectively, while those between genera 5.6%~ 22.5% and 7.3%~ 31.2%, respectively. Phylogenetic analysis showed that Brassica was closely related to Raphanus, followed by Rorippa Scop, Arabidopsis Heynh, Capsella Medic orderly, most distantly related to Orychophrogmus.

为了从分子水平阐明十字花科植物间的亲缘进化关系，给植物种质资源的创建提供理论依据，试验根据课题组已报道的CYP86MF基因编码的氨基酸保守区域设计特异引物，运用PCR技术分别从十字花科6个属11个物种中分离克隆到了CYP86MF基因的同源序列，经比较分析，结果表明：这些同源序列的相似性达80%以上，所推导的氨基酸序列相似性达70%以上，且两者种间差异分别为1.0%~ 5.7%和2.6%~ 7.3%，属间差异分别是5.6%~ 22.5%和7.3%~ 31.2%；由氨基酸序列构建的分子系统树可知，在亲缘进化关系上芸薹属与萝卜属较近，其他依次为蔊菜属、拟南芥属、荠菜属，而与诸葛菜属最远。

The dressing percentage, the chet and leg muscle percentage, the weiht of chest muscle the percentage of leg muscle, the net meat per- centage contrasted no significance with the same age and the same sex of these two chick...

各品种内500日龄的净肉率极显著高于90日龄；肌肉中蛋白质，脂肪含量也是500日龄母鸡高于90日龄同品种的公母鸡，而含水量则下降。谷氨酸的含量，武定鸡的公母分别是18.23％，17.23％；茶花鸡的公母是17.43％，19.07％；已报道的太和鸡是18.31％，17.65％，三者极为近似。赖氨酸武定鸡胸、腿肌分别为9.33％，9.45％；茶花鸡为8.94％，9.41％；太和鸡为8.84％，9.08％；武定高于太和鸡和茶花鸡。

The phylogenetic analysis indicated that within the subspecies data of Canis lupus, Canis lupus laniger polarized first, then did Canis lupus arabs. Canis lupus chanco and Canis lupus lupus were sister species, which had similar phylogenetic positions.

基于12S rRNA+16S rRNA+ H链上的12个蛋白质编码基因的联合数据的系统发育分析发现，在已报道的狼亚种数据中，西藏狼的分化时间最早，其次为阿拉伯狼，蒙古狼与欧亚狼的系统发育地位最为接近。

The third part of this thesis is reactive simulating calculation In this section, some well-known auxiliaries are selected to compute in density functional theory B3LYP on Gaussian 03, from which the relationship between reaction active energies of transition states and enantiomeric excess of chiral products homoallylic alcohols isobtained based on relative reactive ratio theory. Using this relationship, calculations on the reaction of more than eight auxiliaries with four other aldehydes are carried out in AMI and MNDO, proving that N,N\'-dibenzyl tartamide has higher enantioselectivity than others in this reaction.

第三部分为计算化学部分，运用密度泛函理论B3LYP方法在Gaussian03软件上对已经报道的几种手性配体参与的醛不对称烯丙基化反应过程进行模拟计算，基于相对反应速率理论找出两种构型过渡态间活化能的差异与产物光学收率之间的关系；并以此为基础，用AM1和MNDO方法对上述合成的几种配体控制的反应过程进行量化计算，从而在理论上证实了N-苄基酒石酸二酰胺配体在醛的不对称烯丙基化反应中具有较高的立体选择性。

Strains beneficial to transform isoeugenol to vanillin were isolatied from soil based on the screening model using high concentration of isoeugenol.

在含有高浓度异丁香酚的筛选平板上获得的14支菌株均有转化异丁香酚生成香草醛的能力，其中SW-B9的转化能力最好，能从2%异丁香酚生成1.10 g/L香草醛，高于文献报道的菌种转化水平，并且其进一步降解产物香草醛的能力较为微弱。

Methods: According to the mechanism of cough reflex, the c-fibres's role in the respiratory system, and the principle of isosterism. Here, a peripheral antitussive LD was regarded as a lead compound. Amino functional groups, as substituents at the 1-hydroxy group of the racemate of LD, were introduced into the structure of the molecule. These novel compounds were confirmed by 1H-NMR, MS spectrum. Their antitussive activities were studied on mice in sequential method. The EDT50, the stimulating time that caused cough by NH3 on half of mice, were measured. Then could caculated the ratio R between the EDT50 of the treated groups and control group.

根据咳嗽反射的机制及C-纤维在呼吸系统的作用，以外周镇咳药左羟丙哌嗪为先导化合物，依据电子等排原理，在其结构中引入氨基以取代羟丙哌嗪分子中1位的羟基，设计一系列未见报道的化合物（01-15）；并采用了一条适宜的路线进行合成，通过1H-NMR、MS确证结构；采用&序贯法&实验进行新化合物的镇咳活性研究，动物模型采用氨水引咳小鼠，获得引致半数小鼠咳嗽的氨水刺激时间（EDT50）及给药组EDT50与对照组的比值R。

The initial three chapters of this dissertation aim to improve the regularity of ladderlike polysiloxane through strong H-bonding template and slowly dropping half water for hydrolysis and condensation.

本论文前三章旨在利用强氢键模板作用和半水量水解同步缩合脱氯化氢的改进方法首次合成了(1)高规整性、可溶的反应性含对苯二胺有机桥基的聚氢基硅氧烷高分子，29Si-NMR 图中显示梯形主链上硅原子-Si(HO2/2峰的基线宽度△1.0 ppm，这是至今文献报道的所有梯形聚硅氧烷规整性最好的数据；采用分段去撑法成功的合成了纯无机梯形聚氢基硅氧(来源：1bABC论文网www.abclunwen.com)烷。

The direct synthesis of dimethyl carbonate from methanol and carbon dioxide using another basic catalyst, potassium methoxide in the presence of CH〓I as a promoter was investigated.

除了用甲醇于二氧化碳合成DMC以外，我们又对以甲醇与尿素为原料合成DMC的路线进行了尝试，筛选出了两个离子液体Et〓NHCl-FeCl〓和emimBr-ZnCl〓作为用甲醇与尿素为原料合成DMC的高效催化剂，研究了各种反应条件如原料的比例、催化剂的添加量、反应的温度等对反应的影响，得到了所报道的在间歇釜中经一步反应合成DMC的最高产率（27％和26％左右）。

To discover new strobilurin analogues with high pesticidal activity, a series of new strobilurin derivatives containing substituted pyrazole and pyrimide ring, which included 124 novel compounds (73 compounds containing substituted pyrazole ring and 51 compounds containing substituted pyrimide ring) were designed and synthesized. In addition, 36 new intermediates were synthesized. Their structures were characterized by ~1H NMR and elemental analysis, partial compounds were characterized by MS and IR once again.

为了发现具有更好生物活性的新型Strobilurin类化合物，本论文在详尽总结文献的基础上，设计并合成了含吡唑和嘧啶环的新型Strobilurin类化合物124个，其中含吡唑环的新型Strobilurin类化合物73个，含嘧啶环的新型Strobilurin类化合物51个；未见文献报道的中间体36个，所合成的化合物经过~1H NMR、IR、LC-MS或元素分析等确定了结构。

They weren't aggressive, but I yelled and threw a rock in their direction to get them off the trail and away from me, just in case.

他们没有侵略性，但我大喊，并在他们的方向扔石头让他们过的线索，远离我，以防万一。

In slot 2 in your bag put wrapping paper, quantity does not matter in this case.

在你的书包里槽2把包装纸、数量无关紧要。