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1 At a reaction temperature of 100 ℃ and a reaction time of 30 min to give 2,which was then subjected to condensation reaction with p-propoxy mandelic acid in the presence of phosphoric acid at a molar ratio of m(2)∶m( p-propoxy mandelic acid )∶m=1∶1∶1 at a reaction temperature of 60 ℃ for 3 h to yield 3,which was further oxidized by chloranil to give t.

对现有分散红356合成工艺进行了优化,以n∶n=1.2∶1投料,100℃反应30 min得缩合物2,再在等质量磷酸催化下与分批加入的等质量对丙氧基扁桃酸60℃缩合3 h得缩合物3,经温和氧化剂四氯苯醌氧化得标题化合物,总收率55%。

It is demonstrated that the chiral quaternary ammonium salts catalysts exhibit promising catalytic properties for the substrate. Part III: The synthesis and the characterizing of the macroporous aminomethyl resin-supported cinchona alkaloid complexes and the study on its catalytic properties The part consists of two subsections. the macroporous aminomethyl resin -supported cinchona alkaloid complexes were synthesized by the stuff (cinchonine, quinine and macroporous aminomethyl resin). Their structures were characterized by means of elemental analysis, XPS, TG/DTA; the chiral polymer-supported complexes were first used as catalysts for the reduction of ketones. Their catalytic properties for the reduction processes were investigated. The comparison of the products e.e., the conversion of the substrate among different reduction processes was employed with determined by HPLC. The effects of the time, the temperature, the ratio of catalyst to substrate, reaction solvent as well as the recycle times were also discussed.

第三章聚-4-氨甲基苯乙烯负载金鸡纳碱金属络合物的合成与表征及其不对称催化性能研究本章分为两节,以辛可宁和奎宁及聚-4-氨甲基苯乙烯为原料,合成了4种聚-4-氨甲基苯乙烯负载金鸡纳碱络合物催化剂,并对它们的结构用元素分析、X-射线光电子能谱、TG/DTA等几种测试手段进行了表征;首次将所合成的手性高分子负载的金属络合物用于催化芳香酮不对称还原反应,详细研究了所得的手性高分子负载的金属络合物对不同底物的催化性能,用HPLC等分析手段定量检测了还原过程的底物转化率及其产物对映异构体选择性,并考察了反应时间、反应温度、催化剂和底物投料比、反应溶剂和循环次数对催化性能的影响。

The scanty, daringly short skirt, riding up at the knee to show a peep of white pantalette, is a potent weapon and transparent stockings, emeraldgartered, with the long straight seam trailing up beyond the knee, appeal to the better instincts of the blas?

窄小而毫无顾忌,只及膝盖的短裙,裙裾掀起,露出一抹白色宽松裤子,乃是强有力的武器。还有那透明的长袜,笔直的长长的棱线直伸到膝盖上端,再系上鲜绿色袜带,很投合城里玩厌了的人那种想别开生面的本能。

In high-voltage var compensation field, when switching the capacitor banks by mechanical switch, it is easy to bound when it closes and to restrike when it opens, and the mechanical switch can not be switched frequently. When switching the capacitor banks by electronic switch in series, it needs dynamic and static voltage sharing circuit and synchronous triggering circuit. It leads to complex structure and high cost.

为解决当前高压无功补偿领域采用常规机械开关投切电容器组开关合闸时触点弹跳产生过电压,分闸时易重燃及不可频繁操作,而采用串联固态电子开关需要相应的动、静态均压及同步触发电路导致系统结构复杂且成本较高的问题,提出一种基于新型高压投切开关的高压动态无功补偿装置。

It was an occupation that appealed to his sardonic temper.

由于他惯爱嘲讽挖苦,这倒是一个投合他脾气的职业。

The upshot? Some venture capitalists are starting to resemble private equity investors , looking for fast growth from their more established portfolio companies instead of doing the spade work of assembling a management team, evangelizing a product, and building a market—tasks often associated with nurturing the fledgling companies that VCs typically target."Some funds have come out of the bubble and said,'We're going to go even bigger,'" says Bryan Roberts, a managing general partner at Venrock Associates.

结论是?某些创投家开始像是私募基金投资者,从他们许多已建好档案的公司中寻找快速成长的公司,取代组成一个管理小组,传播产品的好处,及建立市场这类型从事挖掘好公司的工作-这些工作常常时和培育刚开始营运的公司有关,这一型的公司是创投公司典型的投资目标"某些资金的梦想泡泡已成型,且说道'我们'将会变得更状大," Venrok Associates 的合夥管理人Bryan Roberts 说道。

Warnaco relies on its highly recognized brand names to appeal to a broad range of consumers.

Warnaco 仰赖它的高度地公开的商标命名投合宽广范围的消费者的心意。

After feeding of 20 d, 40 d and 60 d, the activities of nitric oxide synthase, bacteriolytic, superoxide dismutase, alkaline phosphatase and acid phosphatase in the serum were determined and the relativities between them were also analyzed.

在饲料中添加不同剂量的嗜酸小球菌投喂凡纳滨对虾,并在投喂后的20、40和60d,分别测定凡纳滨对虾血清中的一氧化氮合酶、溶菌活力、总超氧化物歧化酶、酸性磷酸酶、碱性磷酸酶,并分析了这5种酶之间的相关性。

There has never been any spiteful matter in history that culture is hoaxed and fooled like that, the present culture soil is too fit and satisfactory for the hoaxers to play their tricks.

历史上从没有过这样恶肇的拿文化来开涮的事,今天的文化土壤太投合恶搞者心意了。

When an artist deserts to the side of the angels it is the most odious of treasons.

艺术家投合传统派的观点,便是最可恶的叛逆行为。

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The absorption and distribution of chromium were studied in ryeusing nutrient culture technique and pot experiment.

采用不同浓度K2CrO4(0,0.4,0.8和1.2 mmol/L)的Hoagland营养液处理黑麦幼苗,测定铬在黑麦体内的亚细胞分布、铬化学形态及不同部位的积累。

By analyzing theory foundation of mathematical morphology in the digital image processing, researching morphology arithmetic of the binary Image, discussing two basic forms for the least structure element: dilation and erosion.

通过分析数学形态学在图像中的理论基础,研究二值图像的形态分析算法,探讨最小结构元素的两种基本形态:膨胀和腐蚀;分析了数学形态学复杂算法的基本原理,把数学形态学的部分并行处理理念引入到家实际应用中。

Have a good policy environment, real estate, secondary and tertiary markets can develop more rapidly and improved.

有一个良好的政策环境,房地产,二级和三级市场的发展更加迅速改善。