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Given the current complexity of industrial recovery of 3'-methyl-2'-butenyl 3, 3-dimethyl-pentenoate and the decomposition problems with 2-methyl-1-butene, research was conducted on a process for direct recycling of MBDP involving an ester exchange reaction of MBDP with either methanol, trimethyl orthoacetate, or solutions of methanol and trimethyl orthoacetate.

针对目前工业上回收3,3-二甲基-4-戊烯酸-3'-甲基-2'-丁烯酯工艺复杂、异戊烯大量分解问题,研究了MBDP直接返回循环使用工艺,MBDP与甲醇、原乙酸三甲酯或与甲醇原乙酸三甲酯混合溶液进行酯交换反应的回收新工艺,比较了四异丙基钛酸酯、甲醇钠、氢氧化钾用作酯交换催化剂的效果,筛选出回收MBDP&一锅煮&最佳工艺:按照n:n:n:n=1.0:9.8:9.2:0.05物质的量比投料,74℃~78℃反应21h,MBDP转化为贲亭酸甲酯和异戊烯醇,单程转化率87.7%,用85%的磷酸中和甲醇钠,蒸出甲醇,直接用于合成贲亭酸甲酯。

The results show that by providing wastewaters pH of about 3 and reaction time of 2 hours, the quantity of H2O2 of 40 mL/L, the concentration of ferrous iron is 0.4 g/L, the effluent of microelectrolysis goes into Biological contact oxidation process, in which DO, HRT and volume load are 4.5 mg/L, 10 hours and 1.0 kg CODCr/(m3·d) respectively, satisfying the first grade of the national standard.

结果表明,在废水pH值为3左右、反应时间2 h的前提下,双氧水投加量40 mL/L,二价铁离子质量浓度为0.4 g/L,再经过微电解处理后的出水进入接触氧化阶段。在溶解氧为4.5 mg/L左右,水力停留时间为10 h、容积负荷1.0 kg CODCr/(m3·d)左右的条件下,出水CODCr小于100 mg/L,可达到国家对丙烯腈废水处理要求的一级标准。

In the top of the fifth, Posada helped Wang do just that. Rodriguez lined a single into the gap in left-center and reached second when Joey Gathright misplayed it. After Hideki Matsui walked, Posada - batting righthanded against lefthanded reliever John Bale - lifted a long fly to rightfield on which Teahen turned the wrong way. Possibly affected by the wind, the ball wound up hitting the base of the wall for a two-run double that gave the Yankees a 5-3 lead. www.wangfans.com; h2 E# 7 \/ f* i

而在五局上,胖波帮助小民做到这点,A-Rod打出穿越中间方向的安打并且造成Joey Gathright的失误,在松井秀喜被保送后,面对后援的左投John Bale而站在右打击区的胖波,击出右外野方向的高飞球,而Teahen接球时转向错误的方向,也许是受到风的影响,那球打在全垒打墙上形成2分打点的二垒安打让洋基取得5:3的领先。

In the top of the fifth, Posada helped Wang do just that. Rodriguez lined a single into the gap in left-center and reached second when Joey Gathright misplayed it. After Hideki Matsui walked, Posada - batting righthanded against lefthanded reliever John Bale - lifted a long fly to rightfield on which Teahen turned the wrong way. Possibly affected by the wind, the ball wound up hitting the base of the wall for a two-run double that gave the Yankees a 5-3 lead.王建民加油站2 W5 l! N8 X- u

而在五局上,胖波帮助小民做到这点,A-Rod打出穿越中间方向的安打并且造成Joey Gathright的失误,在松井秀喜被保送后,面对后援的左投John Bale而站在右打击区的胖波,击出右外野方向的高飞球,而Teahen接球时转向错误的方向,也许是受到风的影响,那球打在全垒打墙上形成2分打点的二垒安打让洋基取得5:3的领先。

On a recent evening a single round from a Soviet-era anti-aircraft gun, fired from six kilometres away, provoked a full pyrotechnic response: dozens of mortar rounds, bursts of red tracers from a 50-calibre machinegun, illumination flares, the flaming rush of a Javelin missile and the juddering explosion of a 1,000kg guided bomb dropped from a Harrier jet.

在最近的一个晚上,苏联时代的高射炮自6公里(近4英里)开外对北约阵地仅发射了一发炮弹,却引发了一轮全面反应,北约还击的火力如焰火一般:迫击炮发射了数十轮,50口径(0.5英寸)机枪中喷涌出红色曳光弹,照明弹闪耀,&投枪&导弹自&鹞&式战斗机引火射出,还投下了1000吨制导炸弹,爆炸效果震颤。

"The Warriors outworked us, they outhustled us, they got all the loose balls, all the rebounds," said Jason Terry, averaging 25.0 points against the Lakers this season."When you are scrapping for your playoff lives, you cannot come out and put up a performance like that. We are disappointed, but we have one more game on this trip, and we need to find a way to get a win."

&勇士完胜了我们,他们几乎抢下了所有投失的球,所有的篮板,&杰森-特里说道,特里本赛季对湖人的两场比赛中场均拿下25分,&当你正在为季后赛拼搏的时候,你不能拿出这样的表现,我们很失望,但是我们还有很多比赛,我们必须要找出赢球的方法。&

Nevertheless, by revealing the enslavement that women have suffered, Emecheta reminds later readers to pursue self, freedom and independence by unfettering the yokes of any traditions or chains of any outside forces.

此小说的意义也就在于,通过揭示出当时女性所遭受的隐形奴投,埃梅切塔向后来的读者传达出挣脱传统糟粕及外势力量,并追求自我、追求自由和独立的深刻寓意。

Truly, can give elegant look, can let a person feel kind of thick one conversation elegant flavor is the people, only can lift the foot shots in the first between the two word flashed out of cultivation.

真正能透出书香,能够让人一眼,一交谈就感受到那种浓浓的书香气息的是人,只有人才能在那种举首投足之间就闪现出修养这两个字。

Five of the next six hitters singled and the Yankees found themselves down 3-0 with the bases loaded and only one out.

他今天所投的第二球就被Chone Figgins打出全垒打,而接下来六名打者中的五位都击出一垒安打,很快的洋基发现他们已经落后三分却仅只抓到一名出局者。

G9 p( _ S The Yankees had 17 hits and drew five walks but left 16 runners on base and were 4-for-18 with runners in scoring position. They loaded the bases with one out in the 11th but Hideki Matsui struck out on three pitches and Robinson Cano grounded out against lefthander Steve Kline. In the fifth, Cano grounded into a double play with runners on first and third and one out.

R( X3 M, h; H2 x5 vwww.wangfans.com 洋基打了17支安打,获得5次保送,却留下16个残垒,当跑者站上得分位置时18个打数只有4支安打,第11局在1出局时他们攻占满垒,但大松井3球就领到一张老K,坎诺对左投克莱Steve Kline的球打出滚地球,结果出局,第9局在1出局1、3垒有人时,坎诺击出滚地双杀打。

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