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In this dissertation, we choosed anisole as starting material, via chloromethyla tion, cyanogenation, to prepare methoxybenzeneacetonitrile, then fractionated in a fractionating tower, and finally...

本论文也对两步的反应条件进行了探索，获得了比较理想的反应条件。文中还对对甲氧基苄氯自聚的原因与机理进行了探讨，并找到了比较理想的阻聚剂，使得粗品收率提高了10％。

Analyzed errors of auto-reclosing synchronization and offered the countermeasure for the errors; analyzed the misoperation reason of the high-voltage line microcomputer reclosing device and discovered the root of errors and put forward three solutions; compared the three methods and selected the best one to run in practice.

论文对自动重合闸检同期所存在的误区进行了分析与研究，为走出误区提供了对策；对高压输电线路微机重合闸装置所出现的误动作原因进行了分析研究，找到了问题的根源，提出了三种解决问题的方法，并对每种方法的利弊进行了比较，选取最优方案投入现场运行。

These compounds are of substantial interest both inviewpoints of theory and practical applications, mainlyunder the stimulus to achieve synthetic models either foractive sites of iron-sulfur proteins or for transitionmetal catalysts. This thesis describes the synthesis, structures andconformations of 51 new iron-sulfur cluster complexes,which have been characterized by elemental analysis andstandard spectroscopic methods. In addition, single-crystalX-ray diffraction analyses were performed for 4 representa-tive new compounds. Reactivities of μ-〓 with mono- and di- Grig-nard reagents derived intermediates toward various organicelectrophilic substrates were studied, along with complexa-tion of arynyl-containing iron-sulfur clusters by 〓Thus, several bridged, non-bridged, monomeric, dimeric,homonuclear, heteronuclear iron-sullfur and iron-sulfur co-balt-carbon cluster complexes were synthesized. A novelreaction and convenient route for the synthesis in highyield of tetranuclear iron complexes 〓 containing atetracoordinated sulfur atom was discovered, whereas aplausible mechanism based on experimental results was propo-sed for the formation of the new cluster type.

鉴于有机铁硫原子簇化学在基础理论发展和应用方面的重要意义，因此我们开展了这一课题的研究，并取得以下主要成果： 1、本文共合成了51个新有机铁硫及含钴碳簇基的有机铁硫原子簇配合物，除用元素分析，NMR，IR，MS法表征其结构和构象外，还用X-光衍射技术测得四个代表性配合物的单晶结构和构象； 2、我们业已发现炔基Grignard试剂同〓可形成一种&开环&与&闭环&中间物的平衡混合物，研究该平衡混合物同各种亲电试剂的反应； 3、研究发现了一种可高产率地形成〓含〓四配位硫挛合簇的新化学反应并对此反应提出了—种有趣的反应机理； 4、首次由1，4-二溴丁烷双Grignard试剂与〓制得一种新型铁硫簇双硫阴离子活性中间体，并进而研究了它的亲核反应性能； 5、找到了通过〓的光化学反应来合成簇合物〓-〓的一条有实用价值的新路线。

Research result indicated that the cooperative effect between swell and precursor is main factor for the nanoparticle loaded in Nafion, and moreover, polarity of solvent and water content in Nafion also affects the load largely. To improve away the surface concentration of CdS nanocrystal on two side of membrane for general preparation, thioacetamide was first used as a precursor instead of inorganic sulfur source(H2S and Na2S) in synthesis of CdS nanocrystal. The assembly mechanism for several sulfur source had been studied, and CdS/Nafion with the character of homogeneous disperse had been prepared, which is fit for mass transmission in photocatalitic reaction. Following the investigation of several crystallizing way, simple and reliable hydrothermal-crystallizing was found. According to this way, maximal TiO2 load in Nafion achieved 43%. Activity of TiO2/Nafion or CdS/Nafion as a photocatalyst was explored initially for disintegrating liquid contamination. Maximal decompose rate achieved 86% under condition of this research.

研究结果表明：Nafion膜对纳米粒子负载量的主要影响因素是溶胀作用与前驱体协同效应，同时溶剂极性和薄膜含水量对负载量也影响相当大；本课题首次使用硫代乙酰胺代替传统无机硫源（H2S、Na2S）合成CdS纳晶，研究了各种硫源的组装机理，克服了常规技术存在的CdS纳晶趋于膜表面富集的缺点，得到了有利于光催化传质需要的体相均匀分布CdS/Nafion；研究了多种Nafion膜内纳米粒子晶化途径，找到了简单可靠的水热晶化法，TiO2纳晶最高负载量达43％；初步探索了TiO2/Nafion、CdS/Nafion作为光催化剂降解水中模拟污染物的活性，在本实验条件下最高降解率达86％。

This was a fair proposal, it must be confessed, had it been made toany one that had not had a settlement and a plantation of his ownto look after, which was in a fair way of coming to be veryconsiderable, and with a good stock upon it; but for me, that wasthus entered and established, and had nothing to do but to go on asI had begun, for three or four years more, and to have sent for theother hundred pounds from England; and who in that time, and withthat little addition, could scarce have failed of being worth threeor four thousand pounds sterling, and that increasing too - for meto think of such a voyage was the most preposterous thing that everman in such circumstances could be guilty of.

其次，我必须搞到枪枝和弹药。大舱里原来存放着两支很好的鸟枪和两支手枪，我都拿了来，又拿了几只装火药的角筒，一小包子弹和两把生锈的旧刀。我知道船上还有三桶火药，只是不知道炮手们把它们放在什么地方了。我找了半天，终于找到了。有两桶仍干燥可用，另一桶已浸水了。我就把两桶干燥的火药连同枪支一起放到木排上。这时我发现木排上装的东西已不少了，就开始动脑筋如何运上岸，因为一没帆、二没桨、三没舵，只要有点风，就会把木排打翻在海里。

Say 「good bye」差点不加思索的脱口而出如果你没有溜走我并不想失去你 my on mind 我是如此的爱著你呀所有的一切皆是liaison在心底深处 I need you baby 嘶吼著 every night 虽然疑问折磨著我还是能听见 Love forever and only one 你的声音说著 just next stage resume and "Revive"曾混乱不堪的思考回路慢慢的将它解开你的声音说著 Don't stop 明明泪水以热泪盈眶 Say 「good bye」竟不加思索的脱口而出如果你没有溜走我并不想失去你 my on mind 我是如此的爱著你呀某处faraway Do you mind if I open the door 嘶吼著 every night 以及挑战不安的心我还是能听见Love forever and only one 你的声音说著 just next stage resume and "Revive"所有的一切皆是liaison在心底深处 I need you baby 嘶吼著 every night 虽然疑问折磨著我还是能听见 Love forever and only one 你的声音说著 just next stage resume and "Revive" Tonight I Feel Close To You Close my eyes and feel your mind Time has passed I walked like a shadow Never knew What I am going through You touch my heart and take my breath away Wispier on the wind so softly Let the bright stars fill out dreams with love Reach for your hand and you show me the way Tonight, I feel close to you You open my door and light the sky above When I need a friend, you are there right by my side I wish we could stay as one (I wish we could stay forever as one) All the tears that haunt my past You promised It'll be better tomorrow play that song You and I listened to And let it gently ease our pain Tender rain drops from the blue sky Flowers blooming, life is so divine like sunlight on a stream (you're holding my key) You show the world to me Tonight, I feel close to you You open my door and light the sky above When I need a freand, you are there right by my side I wish we could stay as one So much love in this beautiful world Search for the brightest star in the sky You will find the meaning of love Don't be afraid (Don't be afraid) Just be yourself We need this love...

Time after time 如果上天让我们再次相见我决不会再松开你的手在这个宣告春去的佛之花殿朦胧的花朵一瓣飘零记忆中的歌缓缓苏醒至今在胸中温柔回荡 time after time 和你的相遇是奇迹在那微风扑面的城市轻轻的牵起手走过长长的坡道至今无法忘记的约定在风中传来你的声音遥远的记忆冰般澄澈许下了誓言无惧伤害总会有一天我们在此笑颜重逢在这粉红的季节 time after time 独自在飞花烂漫的城市就算落花凋零无法挽回也在这不变的景色中如同昔日我在泪光中守侯着你轻舞飞扬的花瓣安抚着水面愈想珍惜就愈想你人们都说自己是孤独的却都不能停止寻找依托结果只找到了脆弱的虚幻 time after time 若能在初红的街上与你重逢就不再需要承诺比任何人都容易受伤的你这次我一定永远陪伴你身边 Puzzle 今晚果然也还是一个人走出房间一个人看电视没有值得自己笑的地方不是谁的错已经没有什么了，以无所谓的面容转移对你的视线了分手了潜入谷底，还是等待对方的电话相互把名字写到信箱里心系在一起无论如何也消失不掉曾经我们总是肩并肩坚强的活着即使心走不到一起成了没有结束的谜团理所当然总是在我身边但是就到此为止就好对于我不足的地方，你再想寻找一个伴侣这样的谜团今夜果然还是一个人走出房门半夜2点多收到你的的电话信号只是留言的嘟嘟声言叶选ぶ马上切断给你留言虽然想一个人继续下去，但是一个人的日子已经厌倦已经习惯了2人的生活为什么无话可说，自己为了什么而活着？

Can modify whole station program namely at most, 2007, I did my individual website, content of it doesn't matter, the page is simple, do not have discharge at all, because do not have time, also not was in charge of a website all the time, 08 year arrived, I have enough time bubble to be on the net, begin to care the station that has me to come, made the best of time to arrange the website one time, made some of self-help chain, sent dot rubbish to stick promotion to other forum, ah, do not see effect, wander in a few Ip everyday, really pained, the night of Yuanxiao, a person is dull, net of all night on preparation, admire to comparative on the net according to the door in the discovery on the net innocently fire, I had not heard of this thing before, do not follow to go up tide, do not have method ~~, one is searched on the net, stick in Baidu good found a few pieces of relevant pictures not easily, ah, stick to my forum immediately.

顶多就是能修改一下整站程序，2007年，我做了我的个人网站，没什么内容，页面简单，根本没流量，由于没时间，也就一直没管网站，08 年到了，我有充足的时间泡在网上，开始关心起我的站来，抓紧时间把网站整理了一番，做了些自助链，到其他论坛发了点垃圾贴推广，呵呵，不见成效，天天徘徊在几十个ip，真是苦恼，元宵之夜，一个人无聊，预备上通宵网，无意在网上发现&艳照门&在网上相当火，之前我还没听说这事，跟不上潮流，没办法~~，在网上搜索了一把，在百度贴吧好不轻易找到了几张相关图片，呵呵，马上贴到我的论坛上。

This "importation" of the individual consciousness of the creator must however remain controlled. This is of the utmost importance, without constraints or measures we would fall either into the aesthetics of popular taste or into an escalation of elitist vocabulary that would weaken the language. If I myself no longer dare to use oil paints, to revisit or augment, it is due to its intrinsic overabundance of culture; having barely touched the palate, there is an immediate return to the domain of noble art. I would be too scared of creating some useless work while loosing the intensity afforded to a more direct language. Fluctuations in our cultural structure have resulted in vernacular embodying the new norm while I, in the domain of artistic language, have opted for the mode and techniques of traditional embroidery. A long while ago, during the time of the Yuan Ming Yuan artist village, I was convinced that I would run into problems if I applied myself to oil paint. I had produced next to nothing up until the day when, by coincidence, I noticed the many works of embroidery being sold at the entrance to the Summer Palace. I felt like I had finally found my mode of expression, my own personal artistic language. Due to the fact that embroidery belongs to the pre-industrial age, there is a "folkie" quality to it, rural and natural. This ill-defined modern world in which we live must also respond to the demands of "common people", the "lowly" and the "nouveau riche". In some sense, the re-appropriation of this folkloric technique was a necessity, much as it was during the time of the shift from "prose to spoken language" [1], an unavoidable consequence of social upheaval. It was not limited to a mere question of the stylistic signification of the semantic form. What embroidery embodies is a structural modification of society at its most basic level.

虽然它注入了艺术家的个人意识，但关键就是分寸感的把握，不然，或者伦为真的大众趣味，或者切入过多的经英语词汇，而使语言虚弱，就我而言，我不敢重操油画，或是改造扩充，就是由于它本身太文化了，一出手就高雅了，怕弄个不伦不类而失掉语言直接性的强度，文化结构的改变，艺术的俗语是一种趋势，从艺术语言上，我是用传统刺绣方式和手法的，早在圆明园画家村时，我几乎没有画出什么东西，油画肯定觉得使用起来有问题，在当时偶然在颐和园门前，看到很多刺绣的艺术品，一下子感到找到了方法，因为刺绣这种手段属于工业文明之前的东西，它有种土色和平民的感觉，这种也对应了时下的&平常人&、&小人物&、&暴发户&对现代化的消费趣味的追求，那种不伦不类的现代性，正好我的家乡唐山有一个很有名的刺绣厂，找师傅做作品可能更方便，有了这个想法之后，也得到朋友的鼓励，刺绣这一传统民间资源的再利用，在某种意义上说就像&白话文&始于当时社会巨大的转型出现的必然，它不单单是语言风格样式上的意义，它体现的是深层的社会文化结构改变的宣示。

While I was doing this, I found the Tyde began to flow, tho' very calm, and I had the Mortification to see my Coat, Shirt and Wast-coat which I had left on Shore upon the Sand, swim away; as for my Breeches which were only Linnen and open knee'd, I swam on board in them and my Stockings: However this put me upon rummaging for Clothes, of which I found enough, but took no more than I wanted for present use, for I had other things which my Eye was more upon, as first Tools to work with on Shore, and it was after long searching that I found out the Carpenter's Chest, which was indeed a very useful Prize to me, and much more valuable than a Ship Loading of Gold would have been at that time; I got it down to my Raft, even whole as it was, without losing time to look into it, for I knew in general what it contain'd.

在我这般忙碌的时候，只见潮水开始上涨，虽然风平浪静，但还是把我留在岸边的上衣、衬衫和背心全部冲走了。这使我非常懊丧，因为我游泳上船时，只穿了一条长短及膝的麻纱短裤和一双袜子。这倒使我不得不找些衣服穿了。船里衣服很多，但我只挑了几件目前要穿的，因为我认为有些东西更重要，尤其是木工工具。我找了半天，总算找到了那只木匠箱子。此时工具对我来说是最重要的，即使是整船的金子也没有这箱木匠工具值钱。我把箱子放到木排上，不想花时间去打开看一下，因为里面装些什么工具我心里大致有数。

My next Care was for some Ammunition and Arms; there were two very good Fowling-pieces in the great Cabbin, and two Pistols, these I secur'd first, with some Powder-horns, and a small Bag of Shot, and two old rusty Swords; I knew there were three Barrels of Powder in the Ship, but knew not where our Gunner had stow'd them, but with much search I found them, two of them dry and good, the third had taken Water, those two I got to my Raft, with the Arms, and now I thought my self pretty well freighted, and began to think how I should get to Shore with them, having neither Sail, Oar, or Rudder, and the least Cap full of Wind would have overset all my Navigation.

其次，我必须搞到枪枝和弹药。大舱里原来存放着两支很好的鸟枪和两支手枪，我都拿了来，又拿了几只装火药的角筒，一小包子弹和两把生锈的旧刀。我知道船上还有三桶火药，只是不知道炮手们把它们放在什么地方了。我找了半天，终于找到了。有两桶仍干燥可用，另一桶已浸水了。我就把两桶干燥的火药连同枪支一起放到木排上。这时我发现木排上装的东西已不少了，就开始动脑筋如何运上岸，因为一没帆、二没桨、三没舵，只要有点风，就会把木排打翻在海里。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了