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Bisphenol-A polysulfone was used to modify the processability of PPESK and the blends with different compositions were prepared by meltingly extruding on a twin-screw extruder.

采用溶解度参数、差示扫描量热法、界面张力、傅立叶红外、扫描电镜等方法和手段对该共混体系的相行为进行了研究。

The methods of metallograph, SEM, EDS, dynamic potential scanning were applied to test the properties, and the coating conditions were optimized.

本工作以硫酸镍为主盐对镁合金进行了纳米TiO2/Ni-P复合镀,并用金相法、扫描电镜、X射线能谱、动电位扫描等手段研究了其性能,并优化了施镀条件。

No entire nitrendipine crystals were observed visually in SEM photos. The results of X-ray diffraction and differential scanning calorimetry analysis indicated that the crystalline form of nitrendipine was highly dispersed in microspheres, so as amorphous state. The drug release rate of microspheres could be controlled with adjusting the ratio of solid dispersion carriers and retarding agents formulated. The agitation speed and temperature of the preparation process have distinct effect on micromeritic properties of microspheres. The release profiles of the microspheres were mainly affected by the stirring rate of paddle, the concentration of SDS and pH of dissolution medium. Cooling speed and time, however, have no evident influence on the drug release rate of the microspheres. The dissolution data showed that the mechanism of drug release from microsphers was mainly diffusion-controlled. The incorporation efficiencies of 3 batches sample were exceed 96. 8%, which implied that the current method was suitable for design sustained-release dosage form for poorly water-soluble drug.

扫描电子显微镜下观察,在微球内外未发现尼群地平的完整结晶,X-射线粉末衍射和差示扫描量热试验结果也显示,尼群地平已经被高度分散在微球中;微球的释药速度可通过调整处方中固体分散体载体和阻滞剂的比例控制;制备温度和搅拌速度对微球的质量影响较大;溶出仪的搅拌速度,释放介质的浓度和pH对微球的释放有较大的影响;制备过程中的冷却速度和冷却时间对微球的释放行为影响不很明显;方程拟合的结果表明缓释微球的释药行为符合扩散机制;测定三批微球样品的包封率均在96.8%以上,表明该法适合于制备难溶性药物的缓释微球。

Results:The experimental results showed that the ultraspatial resolved imagings of plant tissues by FT-IR microspectroscopy with imaging, mapping, ChemiMap, and line scanning techniques were obtained.

结果:实验结果显示藉由傅立叶转换红外线显微光谱仪,运用光学影像、面扫描、化学官能基面像化及线扫描技术,可以获得植物组织立体空间再现性影像。

The cross-sections of plant tissues were rapidly transferred to aluminum foil-coated microscopic sides for reflectance mode analysis in FT-IR microspectroscopy with imaging, mapping, ChemiMap, and line scanning techniques.

接著植物组织之横切面薄片被迅速转移至铝箔包覆显微载玻片上,作为傅立叶转换红外线显微光谱仪在全反射模式下,运用光学影像、面扫描、化学官能基面像化及线扫描等技术分析使用。

Methods Twenty four patients with chronic renal diseases and 48 healthy volunteers were examined with SS-EPI DWI at 3.0T MR. In chronic renal disease group, RIF of 14 patients who received renal biopsy was determined as grade Ⅰ and Ⅱ based on the tubule- interstitial damage degree, while RIF of 10 patients with uremia, who did not receive biopsy but had nephrogenic renal atrophy, was categorized as grade Ⅲ.

对照组(48例正常志愿者)和慢性肾病组(24例慢性肾脏疾病患者)在肾脏常规MR扫描后行DWI扫描,慢性肾病组14例行穿刺活检,根据病理结果将肾小管间质损害程度分为Ⅰ、Ⅱ级;另10例肾脏体积缩小的慢性肾功能衰竭尿毒症期患者定为Ⅲ级。

The diameter of primary sarcomatoid hepatic carcinoma ranged 5 -10 cm. Huge cystic-solid lesions with irregular septa were found in 2 patients, multiple nodulated soft tissue shadows in 4 patients, and inhomogeneous low-density lesion with unconspicuous enhancement in the other 2 patients.

6例CT平扫表现为囊实性低密度影,其内见条状分隔影(2例)及散在分布的条状、结节状软组织密度影(4例),增强扫描呈不均匀强化,余2例CT平扫表现为不规则低密度影,增强扫描未见明显强化。

The film was scanned on a northlight scanner and was recorded on the arrilaser.

电影是一扫描就northlight扫描,并记录在仪。

The serial examinations showed possible hypertrophic pulmonary osteoarthropathy throughout the bilateral pelvic bones and the long bones of both lower limbs, with a lobulated nodule in the right middle lung and multiple small nodules in both lung fields. The CT-guided biopsy pathologic study of this pulmonary nodule was adenocarcinoma.

经详细检查,发现骨骼扫描呈现两边骨盆以及下肢长骨骨增生性病变,並且在胸部X光以及断层扫描发现右上胸肺叶有一小叶状肿瘤与数个小结节遍布两边肺叶。

METHODS 52 cases (56 ears) with different degrees of injuries of temporal bone were involved in the study. The chief complaints included otorrhagia, facial paralysis, hearing loss and vertigo. All patients were examined by HRCT with 1, 1.5 or 2.0 mm thick slices. Axial scans were overlapped when ossicular chain disruption was suspected.

收集颞骨骨折52(男45,女7)例56耳,主要临床症状有耳道流血、面瘫、听力障碍、旋晕,所有患者行1.0,1.5或2.0 mm层厚HRCT扫描,对疑有听骨链损伤者在听小骨区行重叠扫描

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