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The method comprises:(1) weighing lead acetate hexahydrate and thioacetamide, and preparing aqueous solutions respectively, so that the concentration ratio of Pd2+ to S is 1:(1-4);(2) adding acetic acid into thioacetamide solution to adjust the pH value to 2-4;(3) adding poly surfactant into lead acetate solution, ultrasonicating to mix uniformly and obtain a colorless and transparent sol;(4) mixing the sol and thioacetamide solution;(5) placing the mixed solution in a sealed container, irradiating by 2.5 MeV and 40 mA electron accelerator with irradiation dose of 25-40 Mrad;(6) washing the product, centrifuging for separation, and drying to obtain black PdS nanoparticles.

本发明方法的工艺过程如下:首先称取一定量的六水合醋酸铅和硫代乙酰胺,各自配制成水溶液,其浓度比为使其中的铅离子浓度与硫原子浓度的比例为1∶1~1∶4;在硫代乙酰胺溶液中加入适量醋酸调节其pH值至2~4;醋酸铅溶液中加入少量表面活性剂聚乙烯醇,然后超声振荡,混合均匀,制成无色透明溶胶;随后将溶胶与上述的硫代乙酰胺溶液混合;将该混合液置于密闭容器中,并将其放置于2.5MeV、40mA的电子加速器产生的电子束辐照下进行辐照处理,其辐照剂量为25~40Mrad;然后将反应生成物清洗,并用高速离心机离心分离,然后干燥,最终得到黑色纳米硫化铅颗粒。

METHODS: According to adherent + Thy1.1 antibody and complement-purification method, cranium was opened to expose olfactory bulb. Thereafter, two olfactory bulbs were obtained to remove cerebral pia mater, blood capillary, and peripheral tissues; additionally, olfactory nerve layer and olfactory bulb granular layer were sheared into 1-mm3 pieces for extract single-cell suspension. The cells were adjusted at the density of 1×107 /L and incubated with poly-l-lysine-coated culture bottle or culture plate in 5% CO2 incubator at 37 ℃. On the third day, cells were cultured with serum-free DMEM/F12 culture media.

在差速贴壁+Thy1.1抗体及补体纯化法的基础上,剪开大鼠颅骨,显露位于颅腔前方的嗅球,取出2只嗅球,在显微镜下去除嗅球表面的软脑膜和毛细血管及外周组织,保留富含嗅鞘细胞的嗅神经层和嗅球颗粒层,剪成1 mm3小块分离获取单细胞悬浮液,调整细胞密度至1×107 L-1,接种在用poly-l-lysine包被的培养瓶或培养板中,于37 ℃、体积分数为5%的CO2培养箱中培养,第3天用无血清DMEM/F12培养基换液培养。

The sludge in SBMBR1 presented granular characteristics and settled very well. The sludge in SBMBR1was brown and the sludge flocs was smashed by the shear force due to high intensity of aeration. The sludge size decreased and the sludge flocs blended with water forming ropy solutions, and there was no distinguish interface between water and sludge. Low sludge age and high loading operation enabled the sludge in SBMBR1 keeping higher sludge activity and the MLVSS/MLSS ratio and SOUR values of SBMBR1 were higher than SBMBR2. Both in SBMBR1 and SBMBR2, there were large amount of zoogloea, bacillus, coryneform of bacteria, and pediococcus. However, in SBMBR1 there were also a lot of Protozoa like epistylis and etc. A certain amount of filamentous bacteria can also be found in SBMBR1. The biological species in SBMBR1 were much more abundant than that in SBMBR2.3. Membrane fouling on flat-sheets membrane was observed and analyzed with AFM, SEM and TEM. After the measurement of membrane surface EPS and membrane surface ETX analysis, the pollutants composition on the surface of flat-sheets membrane was calculated.

从外观观察SBMBR1反应器中的活性污泥呈浅黄色,随着运行时间的增加,污泥粒径逐步增加,SV、SVI值逐步下降,呈现出较强的颗粒特征,沉降性能良好;SBMBR2污泥呈土黄色,污泥絮体被高强度的曝气所产生的切应力所打碎,污泥粒径迅速降低,絮体较为细碎,和水相混合成均一粘稠的溶液,看不到泥水分界面;低泥龄、高负荷运行,使得SBMBR1可以保持较高的微生物活性,MLVSS/MLSS值、SOUR值均高于SBMBR2;两级反应器活性污泥中均有大量的菌胶团,长杆菌、短杆菌和球菌是构成主体,但SBMBR1活性污泥中含有大量固着型原生动物如累枝虫等,还存在着一定数量的丝状菌,生物相要比SBMBR2丰富。3、借助原子力显微镜、扫描电镜、透射电镜等手段对平板膜污染现象进行观测和分析,并通过膜表面污染物EPS测定、污染膜表面能谱分析,得出平板膜表面污染物的组成。

Pollution discharge pump, adopting special big channel impeller structure, greatly increases feculency discharging ability, and effectively make solid particle with diameter being 50% of pump outlet diameter; the type 4 can be fitted with various protective devices according to customer's requests, including stator winding temperature-rise protection, bearing temperature rise protection, oil container leakage protection, etc to enhance the exploitation reliability; adopting inner flowing recycling system to use medium cooling electric machine section to make usage more safe.

排污泵采用了独特的大通道叶轮结构,大大提高了污物通过能力,能有效的通过直径为泵口径约50%的固体颗粒;本泵型4可根据用户的要求安装各种保护装置,包括:定子绕组温升保护、轴承温升保护、油室漏油保护等以提高电泵的使用安全性;可采用内自流循环系统,利用介质冷却电机部分,使用更加安全,同时,还可以利用此结构将电泵以干式固定形式安装;采用最新材料精制而成的机械密封,其使用寿命可达8000小时以上;可采用双导轨自动耦合安装装置,使机组的安装、维修方便、快捷;可根据用户的需要配备各种形式的排污泵专用控制柜以实现自动化管理。

The addition of phosphorus has a negative effect on the tensile properties on account of its solubility in CuAl 2 , and the formation ofO 2 oxide particles, where the latter act as nucleation sites for the formation of the CuAl 2 phase.

磷的增加有O 2的氧化物颗粒,就考虑其在CuAl 2溶解度,及在的形成拉伸性能的负面影响下,作为后者的成核行为的网站编队CuAl 2相。

The experimental evidence has shown that the polygonal Co particles are the final form. We found that Co formed nanocrystallites of 2-5 nm in diameter in the surface coating layer of the Mg_2SiO_4 crystalline stems and then aggregate into large clusters. These clusters further grow and recrystallize into polygonal single crystals. Instead of the single crystals, it is the polycrystalline clusters that played the most important role in Mg_2SiO_4 growth.c.

b。实验中观察到的现象表明多面体的Co颗粒并不是一开始就形成的,而是首先在Mg_2SiO_4的枝干表面以2-5nm的纳米晶体聚集成较大的团簇,这些团簇再继续生长并在最后重结晶为多面体的形状。

It is well known that the large lattice mismatch (16%) and thermal expansion coefficient mismatch between GaN and sapphire substrate are the main origins of TDs. By new growing technique of LEO, we acquired high quality GaN films almost free of TDs. The stress characteristics in GaN films with MLTB growing technique is dependent on growing systems and conditions, and the changes of stress and dislocation density are rightabout; Combining buffer layers of high temperature and low temperature is first developed to growing GaN films with low dislocation density, and the mechanism of lowering TDs density is that the first buffer layer of high temperature can make nuclear in second buffer layer of low temperature bigger. This technique also can restrain yellow luminescence effectively.

众所周知,晶格失配和热应力失配是GaN异质外延中位错产生的主要原因;为此,我们对几种降低缺陷的MOCVD外延生长方法进行了新的尝试,其中尝试了侧向外延生长技术,得到了低位错密度(小于10〓/cm〓)、高质量的GaN外延层;尝试多低温缓冲层法,发现材料中的应力特性与生长系统和生长条件有关,材料中的应力与位错密度按相反方向变化;首次尝试高低温联合缓冲层法,材料中高温缓冲层可以使随后的低温缓冲层中成核颗粒增大,从而导致随后高温GaN外延膜中位错密度降低,并且能够有效地抑制黄光峰。

The agitation power consumptions in boiling systems decrease uniformly with the increase of agitation speed, whereas the relative power demand (RPD-the ratio of agitation power input of HEDT for gassed system to that for ungassed system and under the same agitation speed) can maintain at a high level for high gas loadings even when the impeller is operating with a high impeller tip speed. The gas hold-up in the boiling system is much lower than that in the cold gassed system, and the gas hold-up in boiling system increases at first and then decreases with the increase of the agitation power consumption per liquid mass P(subscript m. It implies that the boiling three-phase system has a maximum gas hold-up point. The changes of nucleation site of vapour bubble and the character of suspension of the solid particles with the rotational speed of the impeller are responsible for those behaviors mentioned.

在沸腾条件下,搅拌功率消耗随着搅拌转速的增加有所下降,但HEDT桨具有较高的载气能力,即使在高叶端线速度下,相对功率消耗仍能保持在较高的水平;沸腾体系的气含率随单位质量流体输入功率的增加表现出先增后减的规律,即存在气含率的极大值,蒸汽成核位置和固体颗粒悬浮特性随搅拌功率增加而改变是造成上述行为的主要原因;沸腾体系中的气含率远远低于常温通空气体系。

The content and size of the plastic grains in the reservoir clasts are important factors controlling the reservoir property. Diageneses are a crucial factor of reservoir property, in which consolidation heavily affected reservoir property, cementation was only an important controlling factor influencing reservoir property in the partial area and the influence of dissolution was weak.

储层碎屑组分中的塑性颗粒含量和粒径是储层性质的重要控制因素;成岩作用是储层性质的决定性因素,其中压实作用对储层性质的影响最大,胶结作用仅在局部地区成为重要的控制因素,溶蚀作用的影响是比较有限的。

P species, main as Ca-P and organic P forms, showing rego〓 pollution and karst area of lake watershed, inorganic P〓 related to Ca〓, Al〓, Fe〓 content in the overlying water, sediments is not a simple reservoir of dissolved phosphate and particle phosphate, near the interface, near 98% of total P existed as active forms, they may release to overlying water through reduction dissolution, deadsorption in the period of early diagenesis, only 2% of P as fixed forms, which mainly remained in the sediments, sediment was an important resource of nutrients of ovrelying water.

高原湖泊沉积物中的磷以有机磷和Ca-P形式存在为主,反映了高原湖泊流域污染和碳酸盐地区的整体背景,无机磷形式与水体吸附体Ca〓,Al〓和Fe〓的含量有关。底部沉积物不是溶解性磷酸盐和颗粒磷酸盐的长期储存场所,几乎有98%的磷是活性的形态存在,它们通过早期成岩作用在还原条件下还原,溶解和释放又重新回到上覆水体,只有2%的磷以固〓态的形式稳定保存于沉积物中,因此,沉积物为水体营养程度的重要来源。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。