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Secondly this paper design acentric objective for the pin's imaging. And lastly this paper chooses the suitable CCD sensor and video card for the detection request.

然后针对钻针针面的倾斜性,设计了采用远心光路进行光学成像的成像方案,最后针对钻针检测的需求,对CCD传感器、图像采集卡进行了选型。

Vanillin 58 was used as starting material, which underwent methylation, bromination, acetalization, lithiation followed by nucleophlic addition to aldehyde, Diels-Alder reaction, selective reduction and lactonization to produce diphyllin in an overall yield of 38%(7 steps).

这个方法从香兰素58开始,经过甲基化、溴化、成乙二醇缩醛反应、锂化而后对醛亲核加成、Diels-Alder反应、选择性还原反应和内酯化反应共7步,最后得到diphyllin,总产率38%。

A series of p-toluene sulfonylamido acetacylhydrazone derivatives were synthesized from p-toluenesulfonyl chloride which reacted with glycine to get the intermediate p-toluene sulfonylamido glycine, then through the esterification, hydrazinolysis to afford another intermediate p-toluene sulfonylamido acethydrazide, which condensed with different aldehydes to obtain the target compounds that were characterized by IR, 1H NMR, 13C NMR spectra and elemental analysis.

魏太保 ;冷艳丽;王永成;张建辉;张有明*摘要:以对甲苯磺酰氯为原料,通过与氨基乙酸反应得到中间体对甲苯磺酰氨基乙酸,再经酯化、肼解得到对甲苯磺酰氨基乙酰肼,然后与相应的醛缩合得一系列对甲苯磺酰胺基乙酰腙类化合物。其结构经元素分析, IR, 1H NMR和13C NMR确证。

We review the effect of rare earth ions on bone metabolism as the following three aspects:(1) effect of rare earth ions on differentiation and function expression of osteoblasts and osteoclasts;(2) effect of rare earth ions on the osteogenic and adipogenic differentiation of bone marrow stromal cells;(3) effect of rare earth ions on bone mineral phase of animals.

本文回顾了稀土离子对骨代谢影响的研究进展,探讨了其药用和安全性问题,主要从以下三个方面进行综述:(1)稀土离子对成骨细胞和破骨细胞的分化和功能表达的影响;(2)稀土离子对骨髓基质细胞成骨分化和成脂分化的影响;(3)稀土离子对动物骨矿物相的影响。

We review the effect of rare earth ions on bone metabolism as the following three aspects:(1)effect of rare earth ions on differentiation and function expression of osteoblasts and osteoclasts;(2)effect of rare earth ions on the osteogenic and adipogenic differentiation of bone marrow stromal cells;(3)effect of rare earth ions on bone mineral phase of animals.

本文回顾了稀土离子对骨代谢影响的研究进展,探讨了其药用和安全性问题,主要从以下三个方面进行综述:(1)稀土离子对成骨细胞细胞和破骨细胞的分化和功能表达的影响;(2)稀土离子对骨髓基质细胞成骨分化和成脂分化的影响;(3)稀土离子对动物骨矿物相的影响。

E. value of productions were detected by high performance liquid chromatography. Results The chiral aminoalcohol ligand compound Ⅰ can promote the asymmetric allylation of acylhydrazones and the yield was 57%; The highest values of e. e. obtained for this reaction was 22%.

结果 手性氨基醇配体化合物Ⅰ能够促进烯丙基三氯硅烷和酰腙的烯丙基化加成反应,在它的辅助作用下,烯丙基化加成产物的产率可达到57%,对映体过量值最高达到22%。

Similarly, in Afghanistan (along with other non-Turkic Muslim countries) he is generally viewed unfavorably though some groups display ambivalency as it is believed that the Hazara of Afghanistan are descendants of a large Mongol garrison stationed therein.

类似的,在阿富汗(同样在非土耳其的穆斯林国家),尽管一些群体因为相信阿富汗的哈扎拉人是以前驻扎在哪里的蒙古守卫军的后代,因此而对成吉思汗的态度犹豫不绝,但是成吉思汗通常被认为是不让人喜爱的 [5],[6]。

Young Ampullaria gigas maturates after developing for 38 days under water temperature 20-30°C with sufficient food.

成螺密度、性比及水草覆盖率对雌螺的产卵频数、产卵量及成螺生长速度均无显著影响。

In this research, the spider silk from the major ampullate gland of native Nephila pilipes was collected via the forced-silking apparatus at the reeling speed of 3 m/min. The obtained silk was dissolved in hexafluoro-isopropanol. The influence of pH and temperature over the secondary structure of the silk protein in solution state was examined via Circular Dichroism. The effect of silk concentration and electrical field strength on the structure conformation of silk protein during film casting process was investigated via FT-IR. During the drying process, the increase of silk concentration and the presence of electric field tend to form β-sheet and β-turn. Finally, the dried film of silk protein was treated with different temperatures and cation solutions to study the post-treatment effects.

本研究所采用之蜘蛛丝蛋白质系取自本土品种人面蜘蛛之大囊壶腺体,以3 m/min之卷丝速度强迫取丝(forced-silking)收集蜘蛛丝,再将纤维溶於六氟异丙醇溶剂中配制成溶液,以圆二色光谱仪分析在不同 pH 值与温度条件下丝蛋白质在溶液中之二级结构变化,再将蜘蛛丝溶液以不同浓度及电场强度下乾燥成薄膜后,以傅立叶红外线光谱仪检测分析丝蛋白质在固体状态下之二级结构,最后以不同温度加温、离子溶液浸泡等条件对乾燥所得之薄膜进行后处理,并分析其二级结构之变化。

Synthesis and liquid crystalline behavior of three recently reported mesogenic block-molecules,namely polyhydroxy 1-benzoylaminopropane-2,3-diols Ⅰ,star-shaped pentaerythritol tetrabenzoates Ⅱ and calamitic bolaamphiphiles with lateral chains Ⅲ which are constituted of anisometric block,amphiphilic block and alkyl or perfluorinated chains with different topologies are reviewed in this article.

这些分子由各向异性嵌段、两亲性嵌段和烷基链以不同的拓扑形式组合而成,其合成的关键步骤是Pd(0)催化下碘代全氟烷烃对双键的自由基加成反应以及Pd(0)催化的偶合反应。

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