戊醛

Briefly, coronal brain sections (100 mm)were cut with a vibratome, postfixed with 4% glutaraldehydein 0.1 mmol/L cacodylate buffer (pH 7.4) for 1 h, andthen with 1% osmium tetroxide in 0.1 mmol/L cacodylatebuffer for 2 h. After rinsing with distilled water, the brainsections were treated with 1% aqueous uranyl acetateovernight, dehydrated in an ascending series of ethanolsto 100%, followed by dry acetone, and then embedded inDurcupan ACM. Ultrathin sections (0.1 mm) were cut andstained with 3% lead citrate and subsequently examinedwith a Zeiss transmission electron microscope (Zeiss Inc.,Thornwood, NY, USA).

简单的说，先用切刀制成100um的冠状脑切片，然后用含有4%戊二醛在0.1 mmol/L的二甲砷酸缓冲液(PH7.4)中固定1小时后，放在含有1%四氧化锇的0.1 mmol/L的二甲砷酸缓冲液中2小时，接着用蒸馏水冲洗后，放在1%的aqueous uranyl acetate中过夜，接下来用梯度酒精(至100%)脱水，然后用丙酮干燥，再用Durcupan ACM包埋，切成0.1um的超薄切片后用3%的lead citrate染色，随后用透射电子显微镜观察。

This experiment with dilute alkali swelling on collagen extraction and separation, then purified by gel from collagen, and then glutaraldehyde, carbodiimide, has three types of di-isocyanate cross-linking agent on the plastic recombinant protein molecules cross-linked, the final test of infrared spectroscopy analysis of the results of their cross-linking to determine the extent of the effectiveness of cross-linking cross-linking agent to have an initial understanding.

本实验用稀碱溶胀法对胶原蛋白进行提取与分离，接下来用凝胶层析纯化所得胶原蛋白，然后用戊二醛、碳化二亚胺、己二异氰酸酯三种交联剂对胶原蛋白分子进行重组交联，最后通过对红外光谱测试结果的分析，对其交联程度进行判断，对交联剂的交联功效有一个初步的了解。，谢谢。

Methods:GroupⅠ:fresh bovine pericardium was acellularized with Courtman's method and fixed with glutaraldehyde;GroupⅡ:first treated as GroupⅠ,then was modified with2,3-butanediol.

方法Ⅰ组新鲜牛心包片经Courtuman法脱细胞后用戊二醛(GA固定；Ⅱ组脱细胞及固定方法同Ⅰ组，随后用2，3丁二醇改性。

A useful and efficient glutaraldehyde method for covalent binding of antibodies to lipo-somes was discussed.

本文报道了一种实用、高效的脂质体与抗体共价偶联的方法—戊二醛法。

The main compositions of LPs include shorter chain carboxylic acid derivatives, furan derivatives, cyclopentanone, phenol derivatives, benzene derivatives, cinnamic acid derivatives, longer chain carboxylic esters and sterides.

秸秆在亚/超临界醇中液化产生的LPs的主要组成成分包括短链脂肪酸衍生物、呋喃衍生物、环戊酮衍生物、含有取代基的肉桂酸衍生物、芳醛或酮衍生物、苯酚衍生物、苯衍生物，长链脂肪酸衍生物和甾族化合物。

Using glutaraldehyde as a cross-linker, cystamine is coupled onto the modified electrode. Subsequently, gold nanoparticle monolayer is assembled onto the resulting surface.

使用戊二醛作交联剂将胱胺连接到经修饰的电极上，继而可组装纳米金单分子。

Methods Glutaric dialdehyde was prepared from benzimidazolium salt and saturated dihalide by the addition-hydrolysis reaction of benzimidazolium salt with Di-Grignard reagent.

方法以苯并咪唑盐和二卤代烷为原料，利用苯并咪唑盐与双Grignard试剂的加成水解反应合成戊二醛。

The chapter two was focused on the samarium diiodide promoted organic reactions and their applications in organic synthesis, firstly, a new synthesis of highly substituted cyclopentadienes from a,β-alkynone promoted by samarium diiodide was investigated and the highly substituted cyclopentadienes were prepared in moderate to good yields under mild conditions. Secondly, the Michael addition and Michael-aldol tandem reaction of diorganyl diselenides or diorganyl disulfides with α,β-alkynones mediated by samarium diiodide were studied and a series of alkenylsulfides and alkenylselenides were prepared in good yields. Then the highly regioselecfive nucleophilic addition of the allylsamarium bromide to α,β-alkynones were explored. We found that the allylsamarium bromide reacts with α,β-alkynones to afford regiospecificly 1. 2-nucleophilic addition products in good yields under mild condition. At last we studied the coupling reaction of aryl halides promoted by NiCl〓/PPh〓/Sm〓.

第二章 研究了二碘化钐、金属钐促进的有机反应：1、二碘化钐促进下α，β-炔基酮的偶联环化反应，提供了一种制备多取代环戊二烯的新方法；2、二碘化钐促进下的二硫醚、二硒醚与α，β-炔基酮的Michael加成反应，为高产率地制备多取代的烯基硫或烯基硒化合物提供了方便可靠的新方法；3、二碘化钐促进下的二硫醚、二硒醚与α，β-炔基酮和醛、酮的Michael—aldol串联反应，提供了一种一锅法高产率地制备多取代的含硫的烯丙基醇或含硒的烯丙基醇类化合物的方便可靠的原子经济性的新方法；4、烯丙基溴化钐与α，β-炔基酮的高度区域选择性的1，2-亲核加成反应；5、NiCl〓/PPh〓/Sm〓促进的卤代芳烃的偶联反应-一种从各种卤代芳烃制备联苯类化合物的有效方法。

In order to study the pyrethroids pesticides stress on the physiological and biochemical process of vegetables, effects of different concentrions of fenvalerate stress (20% emulsifiable concentrate, recommended dose: 1500 times dilution; double dose: 750 times dilution) on the activities of antioxidant enzymes, and contents of malondiadehyde in pakchoi were investigated under the open-field condition.

为探讨菊酯类农药胁迫对蔬菜生理生化过程的影响，以小白菜为研究对象，采用大田试验研究了不同浓度氰戊菊酯（20%乳油，推荐用量：稀释1500倍；加倍用量：稀释750倍）对小白菜抗氧化酶活性及丙二醛含量的影响。

OBJECTIVE To know the disinfection efficacy of electrolyzed oxidizing water and glutaraldehyde on clinical used gastroscope and enteroscope in our hospital and to analyze their stability and probable harm.

目的了解酸性氧化电位水和戊二醛用于临床无痛胃镜和肠镜消毒的效果、对人体危害及稳定性。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。