戊醛

The condensation reaction,in which the yield of intermediate product after refining process was more than 90%,used iso-butylaldehyde and formaldehyde as materials,Et 3N as catalyst.The hydrogenation,in which the conversion of hydroxypivaldehyde and selectivity of NPG were respectively 99% and 95%,used Cu-ZnO as catalyst,and ethanol as solute,meanwhile in the hydrogenation,the impurity in material could also ...

缩合反应采用异丁醛和甲醛为原料，三乙胺为催化剂，在 60℃左右反应，缩合产物经减压蒸馏和结晶、干燥，得到收率为 90 %以上的中间体羟基戊醛；加氢反应采用自制的Cu -ZnO催化剂，乙醇为溶剂，在 15 0℃将HPA加氢生成新戊二醇，HPA转化率为 99%，新戊二醇收率在 95 %以上，而且HPA缩合反应的副产物在加氢反应中也转化为新戊二醇。

It was preliminarily determined that the polysaccharide in flower contains glucose, pentose; and the polysaccharide in stem contains glucose, rhamnose and pentose.

初步判断珍珠梅花中多糖含葡萄糖和戊醛糖；茎中多糖合葡萄糖、鼠李糖、戊醛糖。

The acetalization and ketalization of various aldehydes and ketones with catechol by using HY zeolite as catalyst were studied.

研究了 HY分子筛催化邻苯二酚与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正己醛、正辛醛、苯甲醛、二苯甲酮等十余种醛的缩合反应。

The acetalization and ketalization of various aldehydes and ketones with glycerol by using KHSO4 as catalyst were studied. Effect of reaction time, mole ratio of reactants and amount of catalyst on yield of acetals were investigated.

研究了在KHSO4催化下，丙三醇与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正辛醛、二苯甲酮、苯甲醛等十余种醛的缩合反应。

The acetalization and ketalization of various aldehydes and ketones with glycols using FeCl3 as catalyst were studied. The effects of reaction time, mole ratio of reactants and amount of catalyst on the yield of acetals were investigated.

研究了在FeCl3催化下，乙二醇与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正辛醛、二苯甲酮、苯甲醛等十余种醛的缩合反应。

The related reaction conditions and factors such as catalysis of some catalysts etc were discussed. In the procedures, 2-pentylidene cyclopentanone intermediate, which could be isomerizated into a 2-pentyl cyclopentenone under acidic conditions, was effectively prepared in the presence of a phase transfer promotor.

讨论了正戊醛和环戊酮在碱性条件下缩合生成2-亚戊基环戊酮的反应温度、碱浓度、相转移催化剂等因素对反应的影响。2-亚戊基环戊酮中间体化合物能在酸催化剂作用下，异构成2-戊基环戊烯酮，其中酸浓度和溶剂等参数对反应影响明显。

A synthesis of 2-pentylidene cyclopentanone starting from cyclopentanone and n-valeraldehyde through aldol condensation, followed by dehydration, was studied, and the yield reached 85.6%. 2-Pentenyl cyclopentanone was prepared in a yield of 95.0% from 2-pentylidene cyclopentanone with a hydrogenation methodology. Through Baeyer-villiger oxidation,δ-decalactone was synthesized in a yield of 63.9% from 2-pentenyl cyclopentanone with hydrogen peroxide.

研究了以正戊醛和环戊酮为起始原料，经羟醛缩合、脱水反应合成2-戊叉环戊酮，产率达到85.6%，2-戊叉环戊酮加氢制备2-戊基环戊酮，产率为95.0%，2-戊基环戊酮在双氧水作用下经Baeyer-villiger氧化重排反应合成δ-癸内酯，反应产率为63.9%，合成δ-癸内酯的总产率为52.0%，气相色谱分析纯度为98.7%。

This paper mainly studies the synthesis of 2-Isopropyl-5-Methyl-2-Hexenal from the optimum reaction conditions of from self aldol condensation of Isovaleraldehy,with NaOH solution as the catalyst of the condensation.

本文以NaOH水溶液为催化剂，探讨了异戊醛Aldol缩合制备可可醛(2异丙基5甲基2己烯醛)的最佳反应条件：反应温度50℃、反应时间9h、催化剂NaOH水溶液的浓度2mol.L1、OH-/异戊醛为1/1，主产物可可醛的产率为92.2%。

The research results demonstrated that it was a good method that hydrxoypivalic acid was prepared from hydroxypivalaldhyde by the direct electrooxidation method at the lead dioxide and tin dioxide electrodes.

以羟基新戊醛为原料，PbO2电极对羟基新戊醛的电催化活性最高，以硫酸为支持电解质，有隔膜电解槽内，生成羟基新戊酸的选择性和电流效率最高。

The electrooxidative activity of hydroxypivalaldehyde was studied at a tin dioxide electrode by voltammetry, polarization curve and Potentiostatic electrolysis.

考察了温度、羟基新戊醛浓度、硫酸浓度和阳极电位等因素对羟基新戊醛电氧化的影响。

Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

I am coming just now,' and went on perfuming himself with Hunut, then he came and sat.

我来只是现在，'歼灭战perfuming自己与胡努特，那麼，他来到和SAT 。