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戊醚

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Under high dilution,the cross-coupling reactions of 4,5-dicyano-1,3-dithiol-2-one(6) and dithia crown-ether annulated tetrathiafulvalenes(3a~3c) in toluene gave asymmetrical dicyano tetrathiafulvalene derivatives(7a~7c) in the presence of triethyl phosphite.The compounds 7a~7c were characterized by(~1HNMR,EA,MS and IR.

在甲苯溶液中,在亚磷酸三乙酯存在下,采取高度稀释的方法,使4,5-二氰基-1,3-二硫杂环戊二烯-2-酮分别和多缩硫杂冠醚进行交叉偶联反应,成功地得到了不对称的2,3-二氰基四硫富瓦烯衍生物。

Both acrous gramineus and α-asarone can suppress seizure and abnormal discharge of frontal cortex induced by pentylenetetrazol in young rats availably.

石菖蒲及α-细辛醚均能有效抑制戊四氮诱发的幼鼠癫痫发作和额叶皮层的异常放电。

Objective To observe the effect of acrous gramineus and its main component α-asarone on eclamptic behaviors and frontal lobe discharge in the young rats with experimental epilepsy induced by pentylenetetrazol.

目的:观察中药石菖蒲及其主要成分α-细辛醚对戊四氮诱发的实验性癫痫幼鼠惊厥行为和额叶皮层放电的影响。

Objective To observe the effect of acrous g ramineus and its main component α-asarone on eclamptic behaviors and frontal lobe discharge in the young rats with experimental epilepsy induced by pentylenetetrazol.

目的:观察中药石菖蒲及其主要成分α-细辛醚对戊四氮诱发的实验性癫痫幼鼠惊厥行为和额叶皮层放电的影响。

Quinone methides, generated in situ from the reaction of 4-hydroxycoumarin with benzaldehyde, formaldehyde and pentanal, underwent the Diels-Alder reaction with silyl enol ethers to give a series of 3,4-dihydro-2H,5H-pyrano[3,2-c][1]benzopyran derivatives in high yields.

通过4-羟基香豆素与苯甲醛、甲醛和戊醛缩合产生的quinone methide与烯醇硅醚的Diels-Alder反应,以较高产率合成了一系列含有硅氧基的3,4-二氢-2H,5H-吡喃并[3,2-c][1]苯并吡喃-5-酮衍生物。

The poisoning effects of alkyl sulfur compounds on the reactivity of isoprene hydrogenation over supported Pd catalyst are more and more serious with the decrease of the molecular mass of alkyl thiols and dialkyl disulfides.

乙硫醇和二甲基二硫醚使Pd/树脂催化剂中毒的机理是,它们分别在催化剂上发生SH和S-S键断裂,并与Pd形成带烷基基团的S-Pd吸附络合物,致使催化剂上异戊二烯选择加氢活性降低。

In this paper, the thermally reversible crosslinking reaction and the properties of synthesized TPE based on the reactions of chlorine containing polymers such as PVC , chlorined polyethylene , epichlorohydrin rubber and acrylic rubber with salts of dicyclopenladienyl dicarboxylate crosslinking agents were studied.

本研究以环戊二烯二酸盐衍生物作热可逆共价交联剂,通过与聚氯乙烯、氯化聚乙烯、氯醚橡胶和丙烯酸酯橡胶等含氯聚合物的脱MX酯化反应来实现共价关联,并制取相应的新型TPE。

In order to carry out the separation of the azeotropic mixture dipropyl ether + 1-propyl alcohol by extractive distillation, we are studied the influence on the phase equilibria behavior four different solvent: 1-pentanol [2], butyl propionate [3], N,Ndimethylformamide [4] and 2-ethoxyethanol.

为了用萃取性蒸馏法分离二丙醚和1-丙醇组成的共沸混合物,我们正在研究4种不同溶剂对相平衡行为的影响:1-戊醇[2]、丙酸丁酯[3]、N,N-二甲基甲酰胺[4]和2-乙氧基乙醇。

As can be seen in Fig. 5, dipropyl ether will be recovered in the distillate using 1-pentanol, N,N-dimethylformamide and 2-ethoxyethanol as entrainers and butyl propionate is the only entrainer studied that inverts the volatility of the azeotropic mixture.

从图 5可以看出,使用1-戊醇、N,N-二甲基甲酰胺和2-乙氧基乙醇作为共溶剂时二丙醚将在馏分中回收,丙酸丁酯是唯一与共沸混合物挥发性相反的共溶剂。

Dipropyl ether will be recovered in the distillate using 1-pentanol.

使用1-戊醇。N.N-二甲基甲酰胺和2-乙氧基乙醇作为共溶剂时二丙醚将在馏分中回收。

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