戊酸

Phosphotungstic acids (PW12) supported on activated carbon were prepared, characterized by XRD, IR and N2 adsorption, and used as the catalyst for synthesis of n-amyl chloroacetate.

制备了活性炭为载体负载型磷钨酸催化剂，并采用XRD、IR、N2吸附等手段进行了表征。将其用作合成氯乙酸正戊酯催化剂。

The main products are formic acid, propionic acid, methyl acetate, morpholine, imidazole, methyl chloroformate, 1,2-pentanediol, nylon and engineering plastic.

代理BASF和HONEYWELL优质产品散水化工品：甲酸，丙酸，醋酸甲酯中间体：吗啉，咪唑，氯甲酸甲酯，1，2－戊二醇，尼龙和工程塑料。

The emphasis was on chemical properties,application,main production methods,market,and prospects of main deriva- tives of acetaldehyde such as ethyl acetate,pentaerythritol,glyoxal,peracetic acid, crotonaldehyde and pyridine.

介绍了国内外乙醛及其主要衍生物的生产技术发展及其市场供需状况，尤其对乙醛主要衍生物乙酸乙酯、季戊四醇、乙二醛、乙醛酸、丁烯醛、吡啶的化学性质与用途、主要生产方法、市场供需状况及开发前景作详细介绍和分析。

Synthesis of Antidote of N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane BI Hong-mei, ZHANG Jin-yan, LIANG Ying, SHEN Yong (College of Arts and Sciences Heilongjiang August First Reclamation University, Daqing 163319, Heilongjiang, China) Abstract: N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane was synthesized by one pot method with isopropanolamine, cyclopentanone and dichloroacetyl chloride. The optimum reaction conditions obtained are as follows:the proportion in moles of the above materials is 1∶1∶1.2, reaction solvent is toluene, reaction temperature is -15 to -10 ℃,reaction time is 3 h, under the optimum condition, the yield of the compound is 50.0%.

除草剂解毒剂N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷的合成毕洪梅，张金艳，梁英，沈勇(黑龙江八一农垦大学文理学院，黑龙江大庆 163319)摘要：以33%的氢氧化钠水溶液为缚酸剂，异丙醇胺、环戊酮和二氯乙酰氯为原料，采用&一锅法&合成了N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷，采用正交实验法得到最佳反应条件：反应原料摩尔比为1∶1∶1.2，苯作溶剂，反应的温度为-15 ℃~-10 ℃，搅拌时间为3 h，产率达到50.0%。

The main compositions of LP are shorter chain carboxylic acid and their ethyl esters, furan derivatives, cyclopentanone, phenol derivatives, benzene derivatives, aromatic ketone, aromatic acid derivatives, longer chain carboxylic ethyl esters and sterides. After upgrading, the main indexes reach the standard of fuel oil.

结果表明，LP的主要成分包括短链或环状脂肪酸及其酯、呋喃衍生物、环戊烯衍生物、苯酚衍生物、苯衍生物、芳酮、芳酸及其乙酯、长链脂肪酸乙酯和甾族化合物，经提质其主要指标达到了燃料油的标准。

The main compositions of LPs include shorter chain carboxylic acid derivatives, furan derivatives, cyclopentanone, phenol derivatives, benzene derivatives, cinnamic acid derivatives, longer chain carboxylic esters and sterides.

秸秆在亚/超临界醇中液化产生的LPs的主要组成成分包括短链脂肪酸衍生物、呋喃衍生物、环戊酮衍生物、含有取代基的肉桂酸衍生物、芳醛或酮衍生物、苯酚衍生物、苯衍生物，长链脂肪酸衍生物和甾族化合物。

The orthogonal experimental result showed that the optimum reaction conditions were as follows: citric acid 7.7 g, isoamyl alcohol 21.7 mL(the molar ratio of citric acid to isoamyl alcohol, 1:5); 1.0 g (4% of the total weight of raw material) NaHSO4H2O as catalyst; 25 mL dimethyl benzene as deaquation reagent; microwave irradiation time 15 mm; the yield of product was 83.2%(the rate of esterification was 95.1%).

通过正交实验，得到最佳的工艺条件如下：柠檬酸7.7g，异戊醇21.7mL（酸醇摩尔比为1：5）；一水合硫酸氢钠作催化剂，用量为1.0 g（为原料总质量的4%）；带水剂为二甲苯，用量为25mL；微波辐射时间为15min。

In this paper, the thermally reversible crosslinking reaction and the properties of synthesized TPE based on the reactions of chlorine containing polymers such as PVC , chlorined polyethylene , epichlorohydrin rubber and acrylic rubber with salts of dicyclopenladienyl dicarboxylate crosslinking agents were studied.

本研究以环戊二烯二酸盐衍生物作热可逆共价交联剂，通过与聚氯乙烯、氯化聚乙烯、氯醚橡胶和丙烯酸酯橡胶等含氯聚合物的脱MX酯化反应来实现共价关联，并制取相应的新型TPE。

Besides, HFA with dicarboxylic acid not only as the thermal cross-linking agent but also enhanced the flexibility and chemical stability.

此外，六氟戊二酸因具有双石炭酸，不但可以当作热交联剂，且可提升膜的韧性和化学稳定性。

Trifluoromethyl-3-heptadfluoroisopropyl-2-perfluoropentene-4-(N',N'-dimethylamino propyl) imino was prepared by the reaction of hexafluoropropene timer with N,N-dimethyl propanediamine in the molar ratio 1:1.0 at room temperature for 8h, and the structures of VIII were identified by IR and NMR spectra.

以六氟丙烯三聚体与N，N-二甲基丙二胺为原料合成叔胺2-三氟甲基-3-七氟异丙基-2-全氟戊烯-4-(N'，N'-二甲胺丙基)亚胺，利用红外光谱和核磁共振确定其结构，并通过对合成条件的考察得其最佳合成条件：乙醚为溶剂，碳酸钠为缚酸剂，摩尔投料比为1：1.0，在室温下反应8小时。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。