微量分析

A flow injection spectrophotometry is proposed for simultaneous determination of iron ion andiron ion(Ⅲ based on o-phenanthroline spectrophotometry,using double zone injection and a reduction column packed with cadmium plated zinc power.

将流动注射技术引入邻菲罗啉分光光度法测定Fe2+分析体系，采用单阀双带镀镉锌片还原柱带隔离的阀体流路，建立了同时测定微量Fe2+和Fe3+的分析方法。

It is very difficult to eliminate these influence factors completely by conventional treatment. Surface properties and surface treatment of ultrafine red phosphorus and MMT and their interface properties with polymer matrices were studied in this thesis. The results were characterized by GC, FTIR, XRD, DTA, TG, XPS, UV, SEM, TEM and other physical and chemical methods. The main contents are as following: 1. The study of factors influencing ultrafine red phosphorus's invariability and phosphine liberation indicated red phosphorus undergone oxidation and dismutation reaction in air, and trace ion of iron, copper and nickel fastened water absorption and oxidation, in which the effect of copper ion was the most, while aluminium and zinc ion could slow down red phosphorus'oxidation, and silver ion had the best effect on red phosphorus moisture absorption. Inhibitors such as aluminium hydroxide, magnesium hydroxide, organic phenol and ferrous potassuim cyanide had a good effect on reducing red phosphorus moisture absorption and restraining phosphine liberation.

本文围绕纳微米材料的表面处理及其在高聚物基体中的应用这一主题，系统地研究了超细红磷和蒙脱土两种常见材料的表面特性、表面处理方法及其与高聚物基体的界面特性，通过气相色谱、红外光谱、X射线衍射、差热、热重、X射线光电子能谱仪、紫外光谱、扫描电镜、透射电镜等现代分析仪器以及其它物理、化学方法对实验结果进行了表征和分析，全文主要内容如下： 1、对影响超细红磷安定性的因素以及磷化氢的缓释研究表明：红磷在空气中发生缓慢氧化、歧化反应，微量的铜、铁、镍等金属离子增加了它的吸水和氧化速度，其中铜离子的作用最为明显，而铝、锌等离子减慢了红磷的氧化速度，银离子对减少红磷的吸湿性效果最好。

In order to identify the mechanism of melanic mutant of S. exigua, genetic regulation on pupae body color, puparial exuviae, phenoloxidase activity, dopamine andβ-alanine of SEW and SEM were investigated.

本文以SEW和SEM为材料，分别从蛹黑色性状的遗传规律、多酚氧化酶活力、电镜分析、高效液相分析、多巴胺和β-丙氨酸的微量注射及饲喂诱变几个方面进行了研究，以期找出甜菜夜蛾黑化的机理。

Development of high throughput microanalysis is proposed, which is a key issue in analytical chemistry and is essential to break through the bottle-neck emerged in life science since the outburst of post-genomic projects.

本文讨论了微量水平的高通量分析问题，认为这是当前生命科学向分析化学所提出的最主要的挑战，也是分析化学发展必须解决的核心问题之一。

Based on the domestic and foreign researches on information analysis of statoliths in Cephalopods during recent years, the paper summarized the current status of daily growth increment and microchemistry of statoliths in Cephalopods; and generalized its application in fishery resource and environmental science. In the meanwhile, the paper made the prospects on direction and content of the future research.

文章依据近年来国内外有关头足类耳石信息分析的研究成果，综述了头足类耳石日轮及微量化学的研究现状，概括了耳石信息分析在渔业资源及环境科学等方面的应用，并对今后的研究工作提出了方向与内容上的展望。

Of the 200 babies born, 146 were included in the analysis of birth size and 170 (88 in the micronutrient group and 82 in the placebo group) in the analysis of death or illness within seven days.

对200名婴儿出生， 146个被列入分析的出生人数和170 （ 88 ，在微量营养素组和82名在安慰剂组）在分析中的死亡或生病七天以内。

Based on the complexity of the sources for the sediments in the Okinawa Trough, the sequential extraction procedure was applied to the hydrothermal influenced sediments in the core H9 recovered from the middle Okinawa Trough. Five fractions, including exchangeable, bound to carbonates, bound to iron and manganese oxides, bound to organic matter, and residual were acquired. Based on detailed analysis for major, minor and rare earth element compositions, the distributions of the elements in various speciations of the sediments were determined and the controlling mechanism was discussed. The variations of hydrothermal signatures in the core, partitioned from the terrigenous, volcanic and biogenic materials, have been demonstrated and the accumulation rates of some elements were evaluated.

本文针对冲绳海槽多种物源沉积作用混杂的特征，采用顺序淋滤萃取方法对海槽中部受热液活动影响的H9岩芯沉积物进行了分离，将沉积物中分为可交换态、碳酸盐结合态、铁锰氧化物结合态、有机结合态和残渣态五个部分，并对各个结合态中常量、微量和稀土元素组成进行了分析，确定了不同元素在不同结合态中分配的比例，分析了控制不同元素进入沉积物的主要机制。

This paper deals with and summarizes the research and importance of ductile shear zones and presents the future direction and aim for the research of the ductile shear zones around the world. Four aspects of studies of the ductile shear zones have been proposed in this paper as follows:(1) The stress environment including the mineral assemblages, deformation, stress-shearing parameters;(2) The major element sequence and activation under condition of stress;(3) The variations of trace elements and REE, their transportation distributions under strong natural deformation as well as variations of mineral crystal parameters, which can also control the element changes during the ductile deformation;(4) The relationship between element migrations, activation and stress, which will present the new evidences for the studies of dynamic diagenesis and mineralization as well as the studies of evolution of ductile shear zones developed in middle and low levels.(5) The analysis of elements and isotopes in mylonites on the micro-scale are crucial for the understanding of component migrations during the mylonization.

对韧性剪切带及其变形岩石的研究现状和研究意义进行系统的综述，提出了未来韧性剪切带及其糜棱岩的研究方向和目标：①系统研究糜棱岩中主要造岩矿物组合及其变形特征，计算剪切变形岩石的应力－应变参数，搞清韧性剪切带所处的应力应变环境；②系统研究韧性剪切带岩石在天然分强剪切应力作用条件下常量元素迁移机制及活化转移的应力排序问题；③系统研究剪切变形作用过程中岩石化学组成的微量和稀土元素变化，讨论强变形条件下岩石中微量元素活化和迁移规律，深入探讨微量元素迁移的动力控制，包括稀土元素配分变化的应力制约以及应变矿物晶格化学变化行为及其对其寄主的变形岩石元素在应变过程中迁移变化的制约和影响；④从理论上探讨天然强剪切应变条件下岩石中组分活化、转移与应力的因果联系，为深入探讨韧性剪切带动力成岩作用提供理论的科学依据，为探讨中、下地壳中韧性剪切带的形成和演化提供科学依据，同时为韧性剪切变形作用条件下成岩、成矿地球化学作用提供理论和实验依据；⑤现代分析技术如激光同位素原位分析以及激光ICP-MASS分析技术对研究变形域内的岩石的元素和同位素的活化迁移规律，对深刻揭示糜棱岩化过程中的元素活化迁移机制提供更高质量的地球化学证据具有重要的作用。

The adding of anatase nano-crystalline TiO_2 to the deposition solution accelerates the depositing of TiO_2 articles from the deposition solution on the silica glass fiber. A well-combined and durable TiO_2 thin film on silica glass fibers surface obtained by controlling the deposition temperature, deposition time, deposition cycles, concentration of the deposition solution, relative concentration of the deposition materials, pH value of the deposition solution. The effect of the deposition conditions, the drying conditions and the annealing treatment conditions on the surface morphology, section morphology, growth patterns, thickness of the deposited TiO_2 thin films were investigated. Growth rate and particle size of the thin films were controlled by the deposition conditions.

实验结果表明加入微量的锐钛矿型纳米TiO_2诱导晶可以使沉积液中析出的TiO_2粒子更大程度的以锐钛矿型纳米TiO_2粒子的形式析出；通过对沉积温度、沉积液中组分浓度及相对浓度、沉积溶液的pH值的调节与控制，从而控制沉积溶液中化学反应平衡的移动，研究了以上条件对沉积速率、沉积溶液中[Ti6]2–与—OH、[Ti6]2–之间的脱水聚合反应速率的影响，总结出了获得均匀致密质量较好的TiO_2薄膜的一系列实验参数，并对薄膜的生长模式进行了系统的分析研究；通过对沉积时间及沉积次数的分析，可以有效的控制TiO_2薄膜的厚度及质量；通过对薄膜的干燥条件及热处理条件的控制，可以使利用液相沉积法获得的TiO_2薄膜进一步晶化；并分析了对薄膜引起缺陷的主要原因。

Firstly, micro-thermal calorimeters were used to qualitatively analyze the thermochemistry behaviour of reactants system under adiabatic mode; Subsequently a series of toluene nitration experiments were carried out in an isothermal reaction calorimeter to study the influences of different operating conditions such as stirring speed feeding rate and setting temperature and so on . The thermal hazard assessment of toluene nitration was derived from the measured calorimetric data, the rate of the reaction the adiabatic temperature increase △T_ad and maximal temperature attainable MTSR_max in a runaway situation can also been derived.

首先采用微量热分析仪对反应体系在绝热状态下的热行为进行分析；再采用等温条件下的反应量热器实验研究不同的工艺条件如搅拌速度、加料速度和设定温度等参数对反应结果的影响；结合热分析数据和RCle数据，对甲苯的一段硝化过程进行了初步的热危险分析，推导出反应速率方程、反应失控条件下的绝热温升△T_和反应所能达到的最大温度MTSR等参数。

However, as the name（read－only memory）implies, CD disks cannot be written onorchanged in any way.

然而，正如其名字所指出的那样，CD盘不能写，也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口，替代木托盘，免薰蒸，符合欧盟、北美各国对出口货物包装材料的法令要求；喷涂钢托盘适用于重载上货架之用，托盘表面根据需要制作成平板状、波纹状及间隔形式，满足不同的使用要求。