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First, from room temperature to 500oC, the shell structure is amorphous with crinkly and airtight character. The shell structure begins to change into γ-Al2O3 and α-Al2O3 at 900oC. The surface of shells shows nano-sized pores at 900oC from SEM and BET analyses. When heated to 1000oC and 1100oC, the shell forms stable α-Al2O3 structure with smooth surface. Cracks often occur at the triple grain junctions. The specific surface area and the total pore volume of the hollow spheres increase with the calcination temperature.

首先,将锻烧温度由室温提升至500℃时,球壳属非晶相皱褶状致密结构;在900℃时开始有γ-Al2O3相及些许的α-Al2O3相出现,由SEM及BET结果得知,900℃之球壳表面有许多奈米级孔洞出现;当加热至1000℃和1100℃时,球壳形成稳定相之Al2O3结构,壳层表面趋於平滑,且球壳在晶界处有微裂缝存在;由BET 结果得知,比表面积及总孔洞体积会随锻烧温度之增加,有增加之趋势。

The value of specific capacitance was 56.4 F/g and the ESR value of the supercapacitor was 12.5 .f On the back surface of co substrate of carbon micro coils, Ni particles exhibited face centered cubic phase and hexagonal close packed phase. Only hcp Ni was found in the vicinity of the gas inlet, and Ni monolith shaped as flat hexagonal plates. Far from the gas inlet, Ni grains aggregated into flat plates without total fusion.

电容器等效串联电阻为12.5.6、碳微线圈碳基底背面有密堆六方和面心立方两种晶格结构的Ni共存;进气口附近,Ni为密堆六方晶格结构,颗粒为近似六边形的扁平晶体;离进气口较远处,催化剂小颗粒聚集成饼状的结构,相互之间没有完全熔合在一起。

It was found that because of the difference in component distribution and structure, the tendency that pores furcate and bend was smaller in amorphous precursor than in crystalline precursor, and for the amorphous precursor, the velocity of Al leaching-out and the expanding of specific surface area of catalyst were more sensitive to activation process parameters.

结果发现,由于两者在组元的分布及结构上的差异,非晶态前置体合金在活化过程中形成的微孔发生弯折、分叉的倾向要小于晶态前置体合金,同时前者在活化过程中的抽Al速率、以及所得到的催化剂的比表面积等对活化工艺更为敏感。

On one hand, the grain boundaries are the sites of microcrack nucleation, microcracks first occur at grain boundary zone, whose propagation type depends on lamellar orientation of both side of grain boundary.

一方面,微裂纹首先萌发于晶界区,其扩展方式取决于晶界两侧片层的取向。

When increasing PEO content or molecular weight, although the confined environment is extended and PEO can crystallize, the crystallization of PEO is still retrained and crystallization temperature decreases to 5℃, 35℃lower than the crystallization temperature of neat PEO, forming POM/PEO interfibrillar segregation.

随PEO含量或分子量提高,POM微纤晶间距增大,球晶尺寸增大;继续增大PEO的含量和分子量,PEO形成独立的球晶结构。3。

In addition to the black-white double-lobe caused by the displacement field around pores, we demonstrate that LSC should correspond to a novel, peculiar class of anti-phase domain, of which the interior is a local isomorphism with a non-zero phason-type displacement ε〓w〓 i.e.

利用这个结果,我们发现黑白双瓣衬度是二十面体准晶中的多面体微孔引起,而环形衬度则对应于一种二十面体准晶中新奇的反相畴界,其两侧是由相位子型位移ε〓w〓=B〓联系着的局域同晶类。

An EPMA was performed quantitatively on the influence of Ce upon the Mn segregation in cellcrystals, columnar and Equiaxial dendrites of high-Mn steel.

与此同时,用电子探针微区分析考察了Ce对高锰钢中Mn在胞晶、柱状树枝晶及等轴晶内偏析的定量影响。

It has been found that the mat-like crystal is made of zigzag fibrillar structure oriented along the shear direction in the film. The periodical length of the zigzag fibrils is about one micron, corresponding to the width of a band in mat-like crystal.

其锯齿周期的大小平均约为1微米左右,正好与在偏光显微镜正交偏振片下所观察到的草席晶形态中一条晶带宽度的尺寸相当,因此可以认为在偏光显微镜下所看到的草席晶图像只不过是这种锯齿状微纤规则弯曲所形成周期性结构的一种光学效应而已。

The results indicate that only tungsten oxide grains are formed without sodium sulfate additions, while tungsten oxide whiskers with 0.20.3 μm in diameter and aspect ratio of 5-50 or tungsten oxide nanowires with 1030 nm in diameter and aspect ratio of 50200 are synthesized by some sodium sulfate additions on conditions at 180 ℃ for 1236 h. The phase composition of tungsten oxide whiskers is hexagonal tungsten trioxide. The whiskers/nanowires grow oriently through 〈200〉,〈002〉,〈202〉and〈100〉.

结果表明:未添加硫酸钠时,在180 ℃水热反应12~36 h只能得到氧化钨颗粒粉末,而添加适量硫化钠后,可制备出直径为0.2~0.3 μm、长径比为5~50的氧化钨晶须和直径为10~30 nm、长径比为50~200的氧化钨纳米线;氧化钨纳米线晶体结构良好,物相为六方晶系WO3;微/纳米氧化钨晶须/线主要沿〈200〉,〈002〉,〈202〉和〈100〉方向定向生长。

Microsilica silica fume and micro-production processes is the difference from natural quartz silica (SiO2) or fused silica (natural quartz at high temperature melting, after cooling the amorphous SiO2) by crushing, ball milling , flotation, acid purification, high purity water treatment by multi-channel processing of the powder.

硅微粉与微硅粉的生产流程上的差异硅微粉是由天然石英(SiO2)或熔融石英(天然石英经高温熔融、冷却后的非晶态SiO2)经破碎、球磨、浮选、酸洗提纯、高纯水处理等多道工艺加工而成的微粉。

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呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

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However, to get a true quote, you will need to provide detailed personal and financial information.

然而,要让一个真正的引用,你需要提供详细的个人和财务信息。