循环法

Methods The intestine in rats was cannulated for in situ recirculation. UV and HPLC were used to determine the concentrations of phenol red and ferulic acid, respectively.

采用大鼠在体肠回流实验装置，采用UV法和HPLC法分别测定肠循环液中酚红和阿魏酸的量。

The effects of phthalocyanine cobalt with different substituted groups on electrocatalytic property were compared.

利用循环伏安法和线性扫描伏安法研究了修饰电极在酸性介质中对分子氧的电催化还原，比较了不同取代基的酞菁钴对电催化性质的影响。

Based on prestressed steel beams, considering effect of the method of construction to slip and stress increment, accoding to conception that procedure of calculation reflects the procedure of construction and change of structural internal force, making good use of the method of section conversion and making iteration reflect the coupling of slip and stress increment, bringing forth a method of iteration and modified stiffness to calculate the deflection of prestressed composite steel-concrete beams in normal servicing prase.

以预应力钢梁为基础，充分考虑施工方法对结构滑移和应力增量的影响，依据设计计算中反映施工过程和结构受力变化过程，通过截面换算，以循环迭代法来考虑滑移和预应力钢束的耦合作用，提出了计算预应力钢—混凝土组合梁正常使用阶段挠度变形的迭代—修正刚度法。

To detect effects on apoptosis of cortex neuron in DHCA rats, the rat model of occluding bilateral common carotid artery in the deep hypothermic (21C) rats had been established, and flow cytometry, TUNEL, electron microscope, immunohistochemistry and RT-PCR had been studied.: part I: To establish a new rat model of cerebral ischemia/protect during DHCA: 20 SD rats were used in the experiment, little animal respirator was to assist anesthetized rat's respiration after tracheal cannula, artery press through artery spile in femoral artery, electrocardiograph, temperature, blood saturation of O2 (SaO2) and arterial blood gases were monitored during the whole experiment, blood flow of bilateral common carotid artery of rat were occluded about 60 minute when its temperature was reduced to 21 C by ice, then normal temperature was resumed.

本研究采用大鼠深低温颈总动脉阻断模型，应用流式细胞仪、电镜、原位缺口末端标记法、免疫组化法和RT-PCR技术分别检测深低温脑缺血对皮层神经细胞调亡的影响方法：第一部分深低温停循环脑保护大鼠模型的建立：SD大鼠20只，麻醉后气管插管辅助呼吸，用冰块将大鼠的体温降至(21±1)℃，阻断双侧颈总动脉，记录体温、心率、血压、血氧饱和度和血气分析，60分钟后恢复颈总动脉血流，用Longa等的5级评分标准评定4小时和24小时后大鼠神经系统损伤情况。

The results show that the determination of theophylline in green tea is possible and the DPV is more sensitive than CV.

结果表明用聚苯胺膜修饰电极测定绿茶饮料中的茶碱，微分脉冲伏安法的灵敏度高于循环伏安法。

The electrochemical behavior of (4,6-dimethyl-2-pyrimidinyl thio) acetic acid on glassy carbon electrode was studied by cyclic voltammetry and differential pulse voltammetry.

用循环伏安法和差示脉冲伏安法研究了4，6-二甲基－2-嘧啶硫乙酸的电化学行为。

Their micrographs, structure, properties and applications have been investigated by Fourier transform infrared spectroscopy, scanning electron microscopy, transmission electron microscopy, energy dispersive X-ray spectroscopy, cyclic voltammetry, chronoamperometry and polarization method, etc. The main points of this dissertation are summarized as follows:(1) Nafion - thionine ion-pair as dispersant and second catalyst was introduced into the preparation of Pt catalyst for methanol electrooxidation and the resulted catalyst supported on carbon was investigated by electrochemical methods.

本论文主要研究有机化合物(染料、Nafion、脂肪胺、芳胺等)对DAFC电催化剂或载体的改性，通过傅立叶变换红外光谱、扫描电子显微镜、透射电子显微镜、X射线能量散射谱、循环伏安法、电化学阻抗、计时-电流法、Tafel极化曲线等分析测试技术，对电催化剂、电极的形貌、结构、物理化学性质等进行了详细研究。

In an ammoniacal buffer medium of pH 9.8, the electro-chemical behavior of 2,3-isatin was studied by linear sweeping voltammetry and cyclic voltammetry.

应用单扫描极谱法及循环伏安法，在pH9.8的氨性缓冲液中，对2，3-吲哚醌的电化学行为进行了研究。

The caustic was regenerated from the spent caustic in an ethylene plant which adopted precipitation with a oxide of transition metal and causticization.

采用过渡金属氧化物沉淀法和苛化法处理乙烯裂解废碱液得到再生碱液，考察了再生碱液循环使用的可行性。

Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时，再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节；实验中选用CaCl2作为电解熔盐，并对其进行预处理(100℃，保温1小时； 300℃，保温2小时)；经热力学计算，还原钛氧化物的氧分压至少要低于5.11×10-7Pa，结合电解过程中所用熔盐CaCl2有极强的吸水性的特点，电解装置应有较高的密封性，自行设计了一套密封性可靠的电解装置，便于实验过程中熔盐预处理和氧分压的控制；通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时，电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃，实验结果表明电解时间与TiO2质量密切相关，质量越大需要电解的时间越长；通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤，可减少熔盐及其它杂质对电解产物检测结果的影响；最后，通过循环伏安法、计时电流法对电解机理的研究，确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失