得到

The first synthetic route uses 1,2,4-trimethoxybenzene and chloroacetonitrile in forming 2,4,5-trimethoxy-a-chlor-acetophenone under the anhydrous condition, then the intermediate condensates with papaverine forming the core pyrro[2,l-a]isoquinoline, followed by formation and lactonization to form the lactone ring. The second synthetic route uses prepared aldehyde with prepared ethyl nitroacetate by Knoevenagel condensation to obtain 2-Nitro-3-(2,4,5-tris-methoxy-phenyl)-acrylic acid ethyl ester and 2-Nitro-3-(2,4,5-tris-benzyloxy -phenyl)-acrylic acid ethyl ester etal intermediates. The lamellarin skeleton could arise from condensation of the papaverine and these intermediates by Michael reaction, the ester group is provided for subsequent lactonization. The third synthetic route uses coumarin or indan-l,3-dione derivatives and papaverine to form lamellarin under basic conditions.

第一条路线首先从1，2，4-三甲氧基苯出发与卤乙腈作用合成卤代芳酮中间体，然后与罂粟碱反应合成开链片螺素，最后经乙酰化、去保护、成内酯环得到片螺素；第二条路线由制备的芳醛和制备的硝基乙酸乙酯经缩合得到2-硝基-3-芳基丙烯酸乙酯，然后由该中间体与罂粟碱反应，在完成关环的同时也引入酯基，最后去保护、成内酯环得到片螺素；第三条路线是由香豆素或茚二酮出发，经溴代后的中间体与罂粟碱反应，得到片螺素的基本框架。

It was a thirty eight, the poor mans machete Held it in my hand, thinking damn man it's heavier then expected, Wedged it behind my belt buckle Knowin that its evil, even thought that I could smell trouble The extra strength felt weak, But over there on the corner saw what I needed and proceeded to cross the Street Put the heat in the mail box to loose it Figured that the post office knows whats best to do with it Mosey down the road thinkin' bout the old I use to roam this zone with two feet of snow Right here, this use to be a record shop I've gotten love, I've gotten drunk, I've gotten beat up in that parking lot I've had my lake street pride for three decades These alleyways, and these streetlights have seen my best days Before I was a germ learnin how to misbehave, All the way to the grave, south side is my resting place Took a right on Lindale I'm getting near But then the road became empty and the people disappear'd The clowds ran away, opened up the sky And one by one I watched every constellation die And there I was frozen, standin in my backyard Face to face, eye to eye, starin at the last star I should've known, walked all the way home To find that she wasn't here, I'm still all alone

It是三十八，贫困者大砍刀 Held它在我的手，想法的人它是更重然后期望， Wedged它在我的皮带扣之后它邪恶，甚而认为的Knowin我可能嗅到麻烦感到的The额外力量微弱， But在角落在那看了什么我需要并且继续横渡 Street Put在疏松它的邮箱的热邮局知道的Figured什么是最佳做与它 Mosey击倒路thinkin回合老 I用途漫游有雪的二英尺的这个区域 Right这里，这个用途是记录商店 I在那停车场得到爱，我得到了喝，我得到了打了 I有我的湖街道自豪感三十年 These巷道和这些街灯看了我的最佳的几天 Before我是毒菌learnin如何行为不端，一直对严重，南侧是我的休息处 Took在我得到近的Lindale的权利另一方面But路成为了空和人disappear'd The clowds跑掉了，开放天空 And我逐个观看每个星座死那里And我在我的后院结冰了，替换者面对面，眼睛注视的，在最后星的starin I应该知道，一直走在家 To发现她没有在这里，我仍然是所有单独的

Reaction of 9-bromofluorenewith diethyl malonate and sodium carbonate gives diethyl 2-(9-Fluorenyl)malonate.Aminolysis of diethyl 2-(9-Fluorenyl)malonate in ethylenediamine and propylene diamine give〓 and 〓, respectively.〓 and 〓 were synthesized by the reaction of 9-bromofluorene with oxalyl bisethylenediamine. Copper and nickel complexes of 〓 and 〓 were obtained by the reaction of 〓 and 〓 with copper and nickel salt, respectively, in aqueoussolution and extrusion of two hydrogen ions from the amide groups.

使9-溴芴与丙二酸二乙酯在无水碳酸钠存在下反应合成出2-(9-芴基)丙二酸二乙酯。2-(9-芴基)丙二酸二乙酯在乙二胺中胺解得到配体〓，2-(9-芴基)丙二酸二乙酯在1，2-丙二胺中胺解得到配体〓，使9-溴芴与草酰二乙二胺作用得到配体〓和〓与相应的金属盐作用分别得到它们的铜、镍配合物。

Tyson Chandler added 18 points and eight rebounds, Jannero Pargo scored 17 points and Chris Paul had 15 points and 17 assists.

佩甲得到24分，泰森钱德勒得到18分和8个篮板，帕戈得到17分，保罗得到15分17次助攻。

The basic data obtained from the experimental research were calculated and disposed with computer and concluded an important principle of Li〓O by silicon thermoreduction. The factors affected the reduction such as temperature, pressure and time were dicribed by methematical equations. The relation ships of reduction rate with temperature, pressure and time were directly expressed by three-dimension figures. The relating mathematical equations described the process derived from research were proved to be coincided with the practice. Therefore, the obtained results were accurate and reliable and of important value.

运用计算机对试验研究得到的基本数据进行计算和处理，得到了氧化锂硅热还原的重要规律；用数学方程描述了温度、压力和时间还原的影响；用三维立体图直观地表现了温度、压力和时间〓与还原率的关系；研究得到的描述过程的有关数学方程，经验证与实际相符，因此得到的结果准确可靠。

When stratified by type of leukoplakia , the response was more pronounced in homogeneous lesions: complete regression was seen in 16 of 28 (57%) subjects with homogeneous leukoplakia , 2 of 8 with erythroplakia , 2 of 4 with verrucous leukoplakia , and 0 of 4 with ulcerated and nodular lesions.

以口腔黏膜白斑病的种类分层时，同类口腔黏膜白斑病的反应更加显著：28位同类口腔黏膜白斑病患者中，有16位(57%)得到完全的逆转；8位口腔黏膜红斑病患者中，有2位得到完全的逆转；4位口腔疣性黏膜白斑病患者中，有2位得到完全的逆转；8位溃疡性和结状损害患者中，没有任何人得到完全的逆转。

The latter is chlorinated in the side chains under free-radical conditions to give 2,4-dichloro-5-fluoro-3-dichloromethyl-1-trichloromethylbenzene. The latter is hydrolysed via 2,4-dichloro-5-fluoro-3-dichloromethylbenzoic acid, which can be isolated if necessary, to give 2,4-dichloro-5-fluoro-3-formyl-benzoic acid, the aldehyde group of which is reacted to give 2,4-dichloro-5-fluoro-3-N-hydroxyiminomethyl-benzoic acid, from which, with simultaneous conversion of the carboxyl group into the chlorocarbonyl group, water is eliminated using an acid chloride to give the nitrile 2,4-dichloro-3-cyano-5-fluoro-benzoyl chloride.

随后，在游离基条件下进行侧链的氯化，得到2，4-二氯-5-氟-3-二氯甲基-1-三氯甲基苯、后者被水解，经过2，4-二氯-5-氟-3-二氯甲基苯甲酸(如果需要此化合物可以分离)，得到2，4-二氯-5-氟-3-甲酰苯甲酸，将其醛基反应，得到2，4-二氯-5-氟-3-N-羟基亚氨基甲基苯甲酸，用酰氯从其中除去水，同时将羧基转化为碳酰氯，得到一种腈，即2，4-二氯-3-氰基-5-氯-苯甲酰氯。

And a relative preparation is characterized in that according to mol ratio (0.8-0.975):(1.8-1.95):(0.010-0.15):(0.010-0.15) to prepare and mix Mg powder, B powder, C nanometer powder, and SiC nanometer powder uniformly to be filled into an iron tube or iron-copper composite tube to be sealed, rotationally forges, draws and rolls to obtain MgB2 superconductive material containing C and SiC nanometer powder, or tablets the raw powder mixed uniformly via a tablet press, to obtain MgB2 superconductive block containing C and SiC nanometer powder, arranges obtained band or block in a vacuum furnace, vacuums and fills argon gas, keeps temperature for 0.2-3h at 600-1200DEG C, and obtains MgB2 superconductive material containing C nanometer powder and SiC nanometer powder.

制备这种MgB 2 超导材料的方法，其特征在于，将Mg粉，B粉，C纳米粉，SiC纳米粉按照摩尔比(0.8-0.975)∶(1.8-1.95)∶(0.010-0.15)∶(0.010-0.15)配制并混合均匀，装入铁管或铁铜复合管中密封后，按顺序先后进行旋锻、拉拔、轧制，得到含C和SiC纳米粉的MgB 2 超导线材；或者将混合均匀的原料粉用压片机进行压片，得到含C和SiC纳米粉的MgB 2 超导块材；将得到的线带材或块材放置真空炉中，抽真空后充入氩气，在600℃-1200℃保温0.2-3小时，最终得到含有C纳米粉和SiC纳米粉的MgB 2 超导材料。

Further isomerization and substitution of this central intermediate leads to the synthesis of other flavonoids. CHSs has been isolated from different plant species, including both monocots and dicots, some of their genomic DNAs and/or cDNAs have also been isolated.

目前，包括单子叶和双子叶植物的很多物种中，有的物种查尔酮合成酶已经得到纯化且基因组、cDNA克隆得到分离，有的或者得到了纯化酶，或者分离得到了基因组、cDNA克隆。

The simulation results of the cylinder-block model were given in the article, consistent with that of Middlemen"s. It was shown that the block part could improve the uniformity of the flow distribution. The analysis of the flow field of some materials with different power-law factor in the die designed by Mckelvey was close to that of Mckelvey"s. It was shown that the flow distribution was uniform in the die that can producesheets with 1200mm in width. During the analysis the flow channel was divided into several parts to get the details about the fluid flow in each area. A conclusion was drawn after analyzing the influence of the die pressure on the flow distribution, that the higher pressure is good for the output and bad for the uniformity of the distribution. Simulation of the die applying the cylindrical main runner showed the fact that when the cylinder replaced the cone the change of uniformity was trivial. The uniformity of the non-block flow channel was so poor that the block in the proper position of the die channel was necessary. The project of the die for the wider sheet was put forth, and the analysis of the fluid flow in the die was shown.

本文模拟了圆柱管缝隙流模型的三维流动场，得到了与Middlemen结论一致的流动均匀性，并通过模拟直观地展示了采用阻尼块可以改善挤出均匀性的现象；分析了多种幂率指数的流体在Mckelvey等人设计的流道模型中的流动分布，得到了与Mckelvey的分析结果接近的压力降和流量偏差；本文建立了1200mm幅宽机头流道的三维有限元模型，并逐个分析各个区域和多个截面的流动分布状况，由此揭示了1200mm幅宽L-型机头流道内的流北京化工大学硕士学位论文动分布基本均匀，并在分析了机头压力对于挤出流动分布的影响后得出结论：较高的机头压力可以获得较大的产量，但是不利于物料均匀分布；模拟了采用圆柱管主流道时机头流道内的流动分布，得出结论：主流道由圆锥管改为圆柱管时对流动均匀性影响不大，通过设置适当的阻尼仍然可以达到挤出平衡；模拟了两端进料式圆柱管无阻尼流道的流动均匀性后得到结论：两端进料式无阻尼结构的流动均匀性较差，宽机头中仍然有必要设置阻尼块；确定宽幅机头流道的基本方案，并设计了一种宽幅防水卷材挤出机头流道的结构，通过流动模拟表明该种结构的流动均匀性较好；考察了宽幅机头对于不同厚度片材的挤出适应性，得到结论：当生产不同厚度的片材时，阻尼块高度需要调整。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。