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A series of pyridazino[3,2-c]1,2,4-triazoles were synthesized from hydrazides and 3-aryl-6- chloro pyridazine s (3a~3d), which were obtained from substituted benzene and succinic anhydride by Friedel-Crafts reaction, cyclization with hydrazine hydrate, dehydrogenation and chloro-substitution.

以取代苯和丁二酸酐为起始原料,经Friedel-Crafts反应,肼合环,Br2/HOAc氧化脱氢后得到一系列1,6-二氢-3-芳基-6-哒嗪酮(2a~2d)。然后将2a~2d与PCl5在POCl3中回流,得到相应的氯代产物3a~3d,将其与酰肼作用,合环后得到一系列未见报道的哒嗪并[3,2-c]1,2,4-三唑类化合物。所有化合物结构均经元素分析,IR,1HNMR和MS谱得以证实,并对其波谱性质进行了讨论

The reader might well interpret this card as telling the querent that they will be given a vision, an idea, a magical, mental image of whatever it is they most want: the solution to a problem, an ambitious career, a love life, a job.

读牌人看到这张牌以后,一般会给求问者这样的解释:他们将会看到或是得到任何他们最想要的东西,可是在这是虚幻不真实的,只是一个想法,魔幻,精神上的想象,还未得到行动的真实,这些最想要的东西可能是一个难题得到了解决,或是对事业雄心勃勃,或是一段深刻的恋情,又或是一份工作。

I'm still in love i'm telling you straight up still in love i can't believe we could break up i'm still in love can we get, can we get back to it, can we get, can we get back cause i'm still in love, still in love girl you got me going crazy, thinking bout you everyday the feelings that i have for you, baby they will never go away girl i'm still in love, no matter what dem wan sey you got me so caught up, so baby just come my way i'm trying, i'm trying, but i'm lying, i'm lying cause i'm crying, i'm crying, i'm dying without you there's nobody, nobody, nobody that moves me like you do i'm still in love i'm telling you straight up still in love i can't believe we could break up i'm still in love can we get, can we get back to it, can we get, can we get back cause i'm still in love, still in love i'm still in love i'm telling you straight up still in love i can't believe we could break up i'm still in love can we get, can we get back to it, can we get, can we get back cause i'm still in love, still in love

我是仍然在朝派爱注意不加冰块的仍然在朝派爱i不能相信我们是罐破碎向上的移动我是仍然在朝派爱罐我们到达罐我们回来向它罐我们到达罐我们回来原因我是仍然在朝派爱仍然在朝派爱女孩你得到自我发疯思考较量你每天每天感情那个i富人为你当作婴儿般对待他们意愿从不去在客方场地的比赛去在客方场地的比赛女孩我是仍然在朝派爱不管什么dem变苍白sey dem 变苍白sey你得到自我如此抓住向上的移动如此当作婴儿般对待仅仅来我的方式来我的方式我是请尝试我是请尝试但是我是撒谎我是撒谎原因我是高喊我是高喊我是死去外面你那里's没有人没有人没有人那个移动自我爱好你社交聚会我是仍然在朝派爱注意不加冰块的仍然在朝派爱i不能相信我们是罐破碎向上的移动我是仍然在朝派爱罐我们到达我们能重新回到它,我们能得到,我们能把原因送回去我仍然是 in love, still in love i'm still in love i'm telling you straight up still in love i can't believe we could break up i'm still in love can we get, can we get back to it, can we get, can we get back cause i'm still in love, still in love

Through a series of quenching, tempering, tensile testing, low-temperature impact test and metallographic analysis, we ultimately came to the following conclusions:(1) low-carbon alloyed steel 20CrMn2NiMoV quenching at 870℃ and tempering at 200℃, whose structure contains tempered dislocation lath martensite and few small bainite under mixed, has the best obdurability;(2) Carbon Steel 45CrMn2NiMoV quenching at 850℃ and tempering at 620℃, whose structure is sorbitic, has a performance less than that of low-carbon Alloyed steel, but it can also meet the basic design requirements.(3) Mn can substitute for the role of Ni within limited extent.

通过一系列淬火、回火、拉伸试验、低温冲击试验以及金相分析,最终得出以下主要结论:(1)低碳合金钢20CrMn2NiMoV经870℃淬火+200℃回火,得到回火位错型板条马氏体+少量细小下贝氏体的混合组织,具有最佳的强韧性配合;(2)中碳合金钢45CrMn2NiMoV经850℃淬火+620℃回火,得到回火索氏体组织,综合性能虽然不及低碳合金钢,但也能基本满足设计要求;(3)Mn在一定程度上能够替代Ni的作用,适量的Mn和Ni相互配合可以得到最佳的低温韧性,因此&以Mn代Ni&是低温钢材料研究开发中一条可行的适合我国资源状况的合金化思路。

Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.

采用&一勺烩&方法,以4-羟基苯甲腈为起始原料,首先与硫氢化钠和无水氯化镁在N,N-二甲基甲酰胺中反应,所得中间体不经分离,直接加入2-氯乙酰乙酸乙酯进行环合反应,得到2-(4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯(2);然后通过六亚甲基四胺/三氟乙酸进行Duff反应,得到2-(3-甲酰基-4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯(3);再经盐酸羟胺/甲酸/甲酸钠体系脱水得到目标化合物。

Hazard of dust and toxicoid were controlled effectively and personal protect facilities were improved. Bad habits have been changed. Smoking rate deceased from 32% to 21% while exercising rate increased from 23% to 58%, hypertension controlled rate reached 92%. All of the staff made physical examination.

粉尘、有毒化学物的危害得到有效的控制,个人防护得到加强,不良生活习惯得到一定程度的改善,吸烟率由原来的32%降低至21%,参加运动人数由23%上升到58%,高血压控制率达92%,职工体检率达100%。

No sleep no time no mercy i gotta hit em low low ground i'm low key when i spit it less carb more protein my body fitted one step to two step the routine no sign of morphine my body need iy take a trip to oc to cop live it just sip the caffeine i gotta get it one step to step the routine got it now it's going down now no time dont mess boy let's show you how just to move it let me show you just to groone now come inside let me show you how no time dont mess around boy let show you how just to move it work it out lets do girl so flwxible, accessible so hot like the sunshine mexico just feel the beat mr.bexter flow so hot so hot hot check the routine work it out just work it out mr.bexter jc turm it out sing it so fly show you what i'm about so hot so hot hot check the routine got it now it's going down now no time dont mess boy no time baby dont mess around check the routine now lets get down come inside let me show you how no time dont mess around boy no time baby dont mess around check the routine now lets get down

没有睡的时间没有怜悯我得打时间低低地,我低调,当我吐出来减少碳水化合物的蛋白质我的身体装一步一步的两个常规没有迹象吗啡需要我的身体是Iy 采取以法团,前往现场有警察刚喝咖啡因我得得到它一步步走向常规现在得到它现在下降没有时间请勿乱男孩让我们告诉您如何只将它让我告诉你现在只是groone 里面让我来告诉你如何周围没有男孩的时间请勿乱让我们告诉您如何只将它的工作中可以做女孩如此flwxible,访问这么热的阳光一样墨西哥只是觉得节拍mr.bexter流这么热这么热热例行检查工作,这只是工作中出 mr.bexter Jc的页转到出来这样唱飞告诉你什么,我对这么热这么热热例行检查现在得到它现在下降没有时间请勿乱男孩没有时间大约婴儿请勿乱现在的例行检查可以坐下里面让我来告诉你如何周围没有男孩的时间请勿乱没有时间大约婴儿请勿乱现在的例行检查可以坐下

Features of AAD and inflammation were compared between uninfected or unsensitized controls.

结果显示,在感染后的10~15天,我们观察到,衣原体诱导的中等程度的肺部病变,通过增加细菌的数量、肺的组织病理学改变和体重的降低等而得到证实。6周后,感染情况和组织病理的改变得到缓解,体重增加的比率得到恢复。

Yes you can I got, you got, we got eve rybody I got the gift, gonna stick it in the go al It's time to move your body Babylon back in business Can I get a witness, every girl, every m an Houston can you hear me, Ground control can you feel me Need permission to land I don't wanna rock DJ But you're making me feel so nice When's it gonna stop DJ, Cos you're keep me up all night Singing in the classes, music for your m asses Give no head, no backstage passes Have a proper giggle, I'll be quite poli te And when I rock the mike, I rock the mik e You got no love then you're with the wro ng man It's time to move your body If you can't get a girl, but your best f riend can It's time to move your body I don't wanna be sleazy, baby just tease me Got no family plans Houston can you hear me, Ground control can you feel me Need permission to land I don't wanna rock DJ But you're making me feel so nice When's it gonna stop DJ Cos you're keep me up all night I don't wanna rock DJ But you're making me feel so nice When's it gonna stop DJ Cos you're keep me up all night Pimpin' ain't easy Most of them fleece me, every night Pimpin' ain't easy but if you're selling, it's alright COME ON I don't wanna rock DJ But you're making me feel so nice When's it gonna stop DJ Cos you're keep me up all night I don't wanna rock DJ But you're making me feel so nice When's it gonna stop DJ Cos you're keep me up all night I don't wanna rock DJ But you're making me feel so nice When's it gonna stop DJ Cos you're keep me up all night I don't wanna rock DJ But you're making me feel so nice When's it gonna stop DJ Cos you're keep me up all night

我 ,你,我们得到前夕 rybody 我得到了礼物,要去坚持在去阿拉巴马州现在是时候将你的身体巴比伦回到业务我能得到证人,每一个女孩,每米 1 休斯顿你能听到我的话,地面控制你能感觉到我需要许可的土地我不想岩石的DJ 但是你让我觉得非常好当的是要去阻止的DJ ,余弦你把我所有的夜晚歌唱班,音乐为您的米评估也没有头,没有后台通行证有适当的笑声,我会很加里波里碲当我的摇滚麦克,我摇滚的mik é你有没有爱,那么你正在与wro 吴文现在是时候将你的身体如果你不能让一个女孩,但你最好f 友可以现在是时候将你的身体我不想被低俗,婴儿只是戏弄缅因州他没有家庭计划休斯顿你能听到我的话,地面控制你能感觉到我需要许可的土地我不想岩石的DJ 但是你让我觉得非常好当的是要去阻止的DJ 余弦你把我所有的夜晚我不想岩石的DJ 但是你让我觉得非常好当的是要去阻止的DJ 余弦你把我所有的夜晚 Pimpin '是不容易他们大多数摇粒绒箱,每天晚上 Pimpin '是不容易但如果你是销售,这是正常的来吧我不想岩石的DJ 但是你让我觉得非常好当的是要去阻止的DJ 余弦你把我所有的夜晚我不想岩石的DJ 但是你让我觉得非常好当的是要去阻止的DJ 余弦你把我所有的夜晚我不想岩石的DJ 但是你让我觉得非常好当的是要去阻止的DJ 余弦你把我所有的夜晚我不想岩石的DJ 但是你让我觉得非常好当的是要去阻止的DJ 余弦你把我所有的夜晚

In this paper we study the biodegradation of petroleum wastewater by microorganisms with a new way.For the chain alkyl hydrocarbon in crude oil, strains were isolated by screening and acclimatizing at the existence of diesel oil and kerosene. For the aroma hydrocarbon in crude oil, strains were isolated by screening and acclimatizing at the existence of phenol.

本试验我们针对石油中的链烷烃,分别以柴油和煤油为代表物进行筛选得到以降解链烷烃为主的菌种:针对石油中的芳香烃,以苯酚为代表物进行筛选得到以降解芳香烃为主的菌种:针对石油中的环烷烃,以环己烷为代表物进行筛选得到以降解环己烷为主的菌种。

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推荐网络例句

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面,更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值,分为几个相等的区间作为横轴,并将各区间内所测定值依所出现的次数累积而成的面积,用柱子排起来的图形,也叫做柱状图。

You rap, you know we are not so good at rapping, huh?

你唱吧,你也知道我们并不那么擅长说唱,对吧?