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Chitosan had been modified by polyacrylate sodium, glularaldehyde, and NaBH4, respectively, which afforded three kinds modified chitosan: polyacrylate sodium modified chitosan (CIS- PA4) chitosan bead and pentamethylene diamido crosslinked chitosan bead (CTSB- G- Hy). The adsorption properties of CTS-CTSB and CTSB-G-Hy were studied by L25(56) orthogonal experimental design. They show high adsorption activities for Pb2+ in solution. The highest removal efficiency of Pb2+ for CTS-PA4, CTSB and CTSB-G-Hy is 94%, 96% and 93%, respectively. The results showed the adsorption property of CTSB is the highest. The CTSB- G- Hy has good mechanical property, acid-resistance and alkali-resistance.

第二部分壳聚糖的改性及其对水溶液中铅离子的吸附性能研究以壳聚糖为原料制备了三种改性吸附剂——聚丙烯酸钠改性壳聚糖(CTS——PA_4)、珠状壳聚糖凝胶树脂和戊二氨交联珠状壳聚糖凝胶树脂,着重考察了CTSB—G—Hy的制备条件,并考察了三种吸附剂吸附6.3mg/L铅离子水溶液中铅的最佳使用条件,结果表明对CTS—PA_4而言当pb~(2+)溶液的pH在4~6.5之间,吸附剂用量为5g/L,吸附时间为1h时pb~(2+)去除率高于94%,CTS—PA_4可在酸性条件下使用,在碱性条件下依然有效但处理效果较差;CTSB对pb~(2+)具有很好的吸附能力吸附剂用量为5g/L,吸附时间为1h时处理效果极佳,pb~(2+)去除率高于96%;CTSB—G—Hy对pb~(2+)具有一定的吸附能力,吸附剂用量为3g/L,吸附时间为1.5h时处理效果最佳,Pb~(2+)去除率高于93%,而且CTSB—G—Hy的机械强度高,耐酸碱性强,可在较宽的pH范围内使用。

And the ability of antioxidant of polyhydroxy benzamides don't have too many differences with Trolox (IC50 =13.90 μg/ml), the substition of hydroxy group at amino benzene ring doesn't affect the whole ability of antioxidant apparently, but while the single hydroxy group at carboxylic acid benzene ring, they are apparently decrease to scavenge the ability of free radical, as a result, the hydroxy at amino benzene ring substitutes its function, without the hydroxy group, the ability of antioxidant is worst, but it upgrades its function while the hydroxy and amino are in the ortho-position or para-position.

而当多酚醯胺化合物其抗氧化能力与Trolox差不多时(IC50 =13.90 μg/ml),胺基苯环上之羟基取代对整体抗氧化能力影响不明显,但在羧酸苯环上具单羟基时,其清除自由基能力明显下降,使得胺基苯环上羟基取代发挥了影响力,无羟基取代时,抗氧化能力最差,而羟基与胺基互为邻位或是对位时较间位有提升效果。

The normally brominated Baylis-Hillman adducts were formed as the major product at low temperature. While at room temperature or heating, the α,γand β,β-dibrominated compounds were formed as the major products using 3-butyn-2-one and methyl propiolate or propynenitrile as substrate, respectively.

贫电子炔类化合物的Baylis-Hillman反应的研究在这部分工作中我们发现在用TiBr〓或BBr〓为Lewis酸催化贫电子炔类化合物和芳香醛的Baylis-Hillman反应时,温度对反应的影响很大:当反应在低温下进行时,通常生成的是正常的β-溴代的Baylis-Hillman反应产物;而在室温或加热条件下反应,以丁炔酮为底物时,主要生成的是α,γ-二溴化合物,而以丙炔酸甲酯及丙炔腈为底物时,主要生成的是β,β-二溴化合物。

Deduced by the proportion of typical sterile plants and normal fertile plants in segregative generations derived from WA zhenqiuA/6078 that:I gene could inhibit the expression of Rf gene completely by the heterozygosity of 1 pair of Rf in genotype;and only reduce the expression of Rf genes with two heterozygous Rf genes in genotype ;but it would never inhibit the expression of Rf genes if the genotype included 3 pairs of heterozygous Rf genes. When Rf gene was homozygous,the / gene could not inhibit the expression of it.

根据认叭真秋刀6078各衍生分离世代中典型不育株和正常可育株所占比例推断:基因型中仅包含1对杂合的Rf基因时,I对Rf的表达起完全抑制作用;基因型中包含2对杂合的Rf基因时,I仅对Rf的表达起削弱作用;当基因型中包含3对杂合的对基因时,I对Rf的表达不起抑制作用;I对纯合位点的Rf的表达不起抑制作用。

The experimental results shows, if the ratio between MS-1 and OP-10 rangs from 1:1 to 3:l,and the total dosage of them is about 20% of Octamethylcyclotetrasiloxane (D4 ) in quality, we can obtain a kind of stable seeded emulsion of organic silicone modified acrylic ester emulsion. At the same time, if the ratio between MS-1 and Tetramethylammonium Chlorideis l:1.7,the total dosage is about 50% of D4 in quality; the ratio between MS-1 and Cetyltrimethylammonium Chlorineis 7:1, the total dosage is about 25% of D4 in quality,we can also obtain stable seeded emulsions. But if the complex emulsifier system is made of TMAC and OP-10, MS-1 and Peregal O or CTAC and Span-80, we can not synthesize any kind of satisfactory seeded emulsions.

实验结果表明:当MS-1与OP-10的质量比为1:1~3:1,总用量为八甲基环四硅氧烷(D_4)的20%左右时,可合成稳定性良好的硅丙种子乳液;MS-1与四甲基氯化铵的质量比为1:1.7,总用量为D_4的50%左右,MS-1与十六烷基三甲基氯化铵的质量比为7:1,总用量为D_4的25%左右时,亦能得到稳定的硅丙种子乳液;而TMAC与OP-10、MS-1与Peregal O以及CTAC与Span-80的复合体系作为乳化剂时均不能得到满意的硅丙种子乳液。

The thermal property studies indicate that the mass loss of compound B was 54.39% at 242.2~750℃, and when the temperature was 1000℃, there was 25.11% char residue left, which showed that the title compound has a good thermal stability and char forming capability. Using acetonitrile as the solvent instead of trichloromethane or 1, 2-dichloethane gave higher yield. During the synthesis, the yield was very low when triethylamine was used as acid acceptor alone, and when a little amount of 4-dimethylaminopyridine was added at the same time, the yield could be 81%.

结果表明,所合成的化合物B的结构与预期的结构一致;热性能研究表明,化合物B在242.2~750℃质量损失为54.39%,1000℃时仍有25.11%的炭残渣,显示出优异的热稳定性和成炭性;在相同反应条件下,用乙腈作为溶剂的反应产率比使用氯仿和二氯乙烷为溶剂的高,并且在合成过程中,单独使用三乙胺作为缚酸剂时产率很低,而当同时加入少量4-二甲氨基吡啶时,产率可达81%。

Interest state must be kept up to date at all times - whenever a downloader doesn't have something they currently would ask a peer for in unchoked, they must express lack of interest, despite being choked.

当某个peer需要下载某个文件块时,它应该向状态时unchoked的peer明确表示它需要的文件块,同时忽视那些状态时choked的peer。

"In fact, one way to think about that when we're on the International Space Station and all the lights are on when we look outside, it's very much like trying to look at the stars when you're in Boise. You can see some, but then if you go up high in the mountains, up to McCall, and you have all the lights out, that's what it will be like once we undock from station and we can turn all our shuttle lights out, and also for the station folks they can turn all their lights out."

事实上,有一种情况是我们可以想到的:在灯火辉煌的国际空间站向外看时可看到一些星星,这与你在博伊西费劲看到的是相类似的,,但是当你在山上一直往上爬,爬至与McCall一样高时,你就会忽略所有的灯光,这与我们一旦驶离空间站时所有梭子灯灭掉的情况是一样的,并且对于空间站的人来说,他们也可以把他们的灯都熄灭。

Bruno answered the sentence of death by fire with the threatening:"Perhaps you, my judges, pronounce this sentence against me with greater fear than I receive it."

布鲁诺在回答这个判决时说:&我的裁判官,当你在宣判我的死刑时,也许你比我接受它时更为恐惧。&

The results indicate that the formation of loess vertical joints can be divided into two phases:① the formation of inner fissure, i.e. in the beginning of deposition, the undulation of terrain leads to uneven distribution of loess, then when it rains uneven collapsibility generates, which leads to generate inner fissures ;② the stage of fissure extension, namely loess continues deposition after the inner fissures have been formed, the increasing of the top pressure makes the top of inner fissure lie in the state of tensile stress, so, when the stress reaches its tensile strength, the inner fissure extends along the vertical direction and then becomes a vertical joint.

结果表明黄土垂直节理的形成可分为 2 个阶段:①内裂隙形成阶段,开始沉积时,由于地形的起伏导致黄土厚度上的分布不均匀,在降雨时产生不均匀湿陷,从而导致产生内裂隙;②裂隙扩展阶段,内裂隙形成后黄土继续堆积,顶部压力的增长致使裂隙顶部土体受到拉应力作用,当达到其抗拉强度时裂隙就会沿竖直方向产生扩张而形成垂直节理。

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I will endeavour to find you some assistance.

我尽力帮你找人帮忙。

At first I only know bruck is the idol of American younglings, afterwards I returned back to Taiwan ,even in Beijing last year ,I saw her poster everywhere, I was so surprised at her charm.

起初我只晓得布鲁克雷德丝是美国少男少女崇拜的偶像,后来回台湾,甚至去年在北京,居然也四处看见她的海报,才惊讶她的魅力之大。

Ah may dee:You are chinese living in a democratic country.

你是居住在民主国家的中国人吧。