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Methods by using a broad pH range column(Gemini NX C18,4.6mm×150mm,5μm),basic mobile phase which was[H_2O-ammonia-glacial acetic acid] (96:3.6:0.4)-methanol,the related substances in etimicinsulfate were separated and detected by electrospray ionization and positive ion monitoring,the ESI ion source condition was following: temperature is 350℃,nebulizing pressure is 50 psi,dry gas flow is 10 L /min.some related substances in etimicinsulfate were identified by comparing the retention time in chromatography,~+ spectrum and MS~2 spectrum with reference substances\',the others which haven\'t reference substances were identified or speculated by analyzing their MS~2 fragmentation with the help of a rule summarized from the MS~2 fragmentation of gentamicin C1a,micronomicin and etimicin.Results nineteen related substances in etimicinsulfate were separated and detected.

方法利用宽pH范围的Gemini NX C18(4.6mm×150mm,5μm)色谱柱,在碱性条件下,以[水-氨水-冰醋酸(96:3.6:0.4)]-甲醇(70:30)为流动相,直接分离各组分;并用HPLC-ESI-MS~2检测样品中各组分,质谱条件:ESI离子源,离子源温度350□,雾化室压力50 psi,干燥气流速10 L/min,正离子检测方式;对有对照品的有关物质采用比对有关物质与对照品的色谱保留时间、准分子离子的质荷比及二级质谱方法进行鉴定,无对照品的有关物质,则是先通过解析庆大霉素Cla、小诺霉素、依替米星的二级质谱,对该类化合物的二级质谱裂解规律进行归纳,并以此推测未知新化合物进行结构,再用推测的结构对二级质谱进行解析,如所有的碎片离子均合理解释,表明推测合理。

Chapter six is a conclusion focusing on inducing the conclusions from previous chapters, positing the conclusions and suggestions.

第六章为结论,本章将针对前面各章所得之结论,进行归纳与处理,总结本文所述,提出结论与建议。

China's supply Centrum has not only upgraded its requirement of core-competitiveness, but also successfully established a big and integrated supply-chain system which is composed of three types supplier. Along with Ericsson's pullulating and development is its consummating

同时,本文试从分析爱立信中国在不断完善供应链的过程中对于企业核心竞争力的提升和优化,进一步归纳和总结其供应链管理方面的特征和优势,希望能够为我国企业在供应链管理的实际操作提供良好的借鉴。

Take the Taitung city as example; distance between any two positions in downtown area would not be far from five kilometers. Bike is definitely a good replacement for motor vehicle in daily, routine transportation. In this research, we proposed a method for popularizing of bike by reinvestigating the conditions of bike riding today, and reconcerning requirements of bike users.

以台东市为例,其市区中心内各点最远距离多不超过五公里,适合以自行车替代其他机动车辆作为日常生活旅次所使用的运具,如能针对我国目前自行车使用环境的相关课题加以检讨,并通盘考量使用者的需求,应能归纳出推动自行车使用的可行方案。

We take this as the foundations, carries on the classification to the serial products, the induction, reorganizes.

我们以此为基础,对系列产品进行分类,归纳,整理。

Mainly according to cooperation principle and relevance theory, the judgment and recognition of the rhetoric of double meanings, the regularity taking on when its deep meaning is revivified and cognized are induced; and at the same exhibiting specifically the meaning reasoning process of the acceptor of the rhetoric of double meanings of polysemy, synonymy, and antonym.

以&合作原则&和关联理论为主要依据,对双重意义修辞的判断和认定,对其语内意义的还原和认知等呈现的规律性进行了归纳,并具体地展现了接受者对于多义类、同义类和反义类双重意义修辞的意义推理过程。

But UCP was not fully applicable nor appropriate for standbys,even the least complexstandbys(those calling for presentation of a draft only)pose problems not addressed by theUCP more complex standbys(those involving longer terms or automatic extensions,transferon demand,requests that the beneficiary issue its own undertaking to another,and the like)require more specialized rules of practice.

本文采用历史的方法、比较分析的方法、归纳的方法、理论联系实际的方法,以对备用信用证制度的研究为核心,通过对备用信用证制度与其它相关制度、各国国内相关实践与国际范围内的相关实践的比较分析,试图从时间和空间两个角度来揭示备用信用证制度发展和运作的内在规律,并探讨与之其关的法律问题。

According to the comparison analysis for the force-displacement relationship obtained from stets of earthquake simulation tests for 3 RC single story structures and the quasi-static test for one RC single story structure (identical with the former 3 models), as well as the analyses for the natural frequency change of the 3 RC single story structures with the increase of the excitation levels, it is found that the accumulated hysteretic energy-dissipation capacity is critical for the structural safety even after serious damage.

本文首先通过对近场破坏性地震动的特性分析,给出了脉冲型地震动的量化定义,并通过研究归一化反应谱变化规律的方法,分析了两类脉冲组合即:波前脉冲组合以及波后脉冲组合对于主脉冲作用效应的影响,总结归纳出波前脉冲与波后脉冲对主脉冲作用效应的不同贡献规律,并通过单层钢结构模型的地震模拟振动台试验验证了理论分析结果,为进一步研究揭示脉冲型地震动中主脉冲的破坏能力奠定了基础。

The reason why this book is suffixed as "summary", it is because: First, no self-conjecture and even more no self-fantasy, and it is the summarization on the basis of analyzing massive physics experiments and human project practice.

本书出于对牛顿巨著的崇拜,起名为&自然科学原理&,之所以后缀&总结&,是因为:第一,没有自己的猜想,更没有自己的狂想,而是在分析众多物理实验和人类工程实践的基础上进行的归纳总结。

Since SVMR based on the quadratic programming unfits for the online training of control, the current research includes the online training of SV...

分析了国内外这些研究内容的最新研究进展,旨在探讨归纳支持向量机在控制领域研究的主要成果和存在的问题,以便为进一步的研究提供一定的支持与帮助。

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This paper discusses design and realizable methods of remote test output interface from logical design angle.

本文从逻辑设计的角度讨论遥测输出接口的设计及实现方法。

This also 星体投射plies to buildings, structures and geological features.

这也适用于建筑物和地质特征。

We all hope for a better life.

我们都希望好的生活。