异色的

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

Calcium carbonate and soluble glass and so on were confected as alkaline antifouling agent. The Infrared Spectrometry results showed that 2275-2250 cm~(-1) diagnostic absorb wave crest in part A and 3390-3200 cm~(-1) in part B and 1730 cm~(-1) in coating film strongly proved polymers reacted just as the reacting mechanism, that means polysiloxane which offer low-surface-energy property linked Polyurethane system by —OH groups reacting with —NCO groups. Relative molar mass of part A and part B was determined by Gel Permeation Chromatography and the results were appropriate. Surface-energy was determined and results were between 33.6-47.17 mN/m and it increased when alkaline antifouling agent was put into the coating. Alkaline antifouling agent was releasing steadily when the coating film was dipped in seawater. As time gone, the pH value of seawater was increasing. Solubility parameter and results showed that there was no corrasive phenomenon between the polyethylene strand and the coating.

红外光谱分析结果表明，出现在A组分中的2275～2250cm~(-1)处的异氰酸酯特征吸收峰、B组分中的3390～3200cm~(-1)处硅羟基的特征吸收峰及出现在固化后涂膜中的1730cm~(-1)处氨基甲酸酯基团的特征吸收峰证明了涂料成膜物质交联固化符合本文的设计要求，即赋予涂膜低表面能特性的有机硅组分通过—OH基团与—NCO基团的反应已经链接到聚氨酯体系中；凝胶渗透色谱结果表明，成膜物质的A、B组分均为低分子量，符合预聚物的要求；涂膜表面能的测算结果表明，涂膜的表面能在33.6～47.17mN／m之间；加入碱式防污剂后涂膜的表面能略有升高；碱式防污剂的释放平稳，随着涂膜在海水中浸泡时间的增长，pH值有增加的趋势；用溶解度参数原则来评价涂料与网绳的涂装，结果表明，本试验研制的防污涂料对聚乙烯网绳无溶蚀作用。

Include: Of history of civilization of baleful and misinterpret China, China and historical historical fact; Baleful and misinterpret his country the history, do not respect what civilization and custom are used to human civilization, his country; Derogate in cold blood, evil of figure of the anybody in doing famous book of character of revolutionary cacique, hero, important history character, China and foreign countries and famous work; Ill will derogates people army, armed police, public security and judicatory figure; Have mistreat captive, inquisition by torture to extort a confession of the clue such as convict or guilty suspect; Expression violates guilty aggressive arrogance, specific reveal criminality detail, reveal special investigation shift, expose what ought to be protected to inform against the figure such as person, witness, audio; Advertise religious ultraism, instigate between each religion, denomination, the contradiction between be religious and masses of lack of faith and conflict, harm masses emotive; Advocate sees photograph, fortune-telling, see ghost of geomantic, augur, drive treat a disease those who wait for feudal superstition activity; With evil do means to depict heavy nature calamity, contingency, horrible incident, war to wait for catastrophic occasion; Specific show licentious, rape, incestuous, love cadaver, walk the street, go whoring, of the clue such as sexual allergy, masturbation; Of the detail such as means of process of expression or obscure performance sexual behavior, sex, sex and as associated as this overmuch body contact; Show intentionally, be masked with limbs only or cover position of human body privacy with very small pall; Contain sexual suggestion, sex to tease those who wait to make the person produces a gender to associate easily; Advocate extramarital love, much horn is loved, one-night standing, sex is mistreated and change wife wait for insalubrious content; In order to grow up the film, affection lubricious film, 3 class piece, pat secretly, expose one's body, dew point reachs all sorts of flirtation to sexual written language or picture regard video program as caption or be classified; Have intense of the clue such as excitant homicide, bloody, violent, suicide, kidnap, drug taking, gamble, clever different; Have picture of excessive fright bloodcurdling, caption, background music and sound effect; Specific show animal of cause sb's death by maltreating him, catch kill, edible country protects kind of animal; Contain those who encroach individual privacy content; With affirmative, favorable fundamental key or fetching me-too means expression fights other people of affray, shame, corrupt of character bawdry; The philosophy with inactive, decadent advocate, world outlook and viewpoint of value, unwisdom of sedulous apply colours to a drawing, exaggerated nation lags behind or of social the seamy side; The cutout of the program of movie and TV that total bureau of TV of national broadcast film prohibits travelling and film, teleplay reduces part; Violate relevant law, statute of spirit.

包括：恶意曲解中华文明、中国历史和历史史实的；恶意曲解他国历史，不尊重人类文明、他国文明和风俗习惯的；蓄意贬损、恶搞革命领袖、英雄人物、重要历史人物、中外名著及名著中重要人物形象的；恶意贬损人民军队、武装警察、公安和司法形象的；有虐待俘虏、刑讯逼供罪犯或犯罪嫌疑人等情节的；表现违法犯罪嚣张气焰，具体展示犯罪行为细节，暴露特殊侦查手段，暴露应当受到保护的举报人、证人等形象、声音的；鼓吹宗教极端主义，挑起各宗教、教派之间，信教与不信教群众之间的矛盾和冲突，伤害群众感情的；宣扬看相、算命、看风水、占卜、驱鬼治病等封建迷信活动的；以恶搞方式描绘重大自然灾害、意外事故、恐怖事件、战争等灾难场面的；具体展现淫乱、强奸、乱伦、恋尸、卖淫、嫖娼、性变态、自慰等情节的；表现或隐晦表现性行为、性过程、性方式及与此关联的过多肉体接触等细节的；故意展现、仅用肢体掩盖或用很小的遮盖物掩盖人体隐私部位的；带有性暗示、性挑逗等易使人产生性联想的；宣扬婚外恋、多角恋、一夜情、性虐待和换妻等不健康内容的；以成人电影、情色电影、三级片、偷拍、走光、露点及各种挑逗性文字或图片作为视频节目标题或分类的；有强烈刺激性的凶杀、血腥、暴力、自杀、绑架、吸毒、赌博、灵异等情节的；有过度惊吓恐怖的画面、字幕、背景音乐及声音效果的；具体展示虐杀动物，捕杀、食用国家保护类动物的；带有侵犯个人隐私内容的；以肯定、赞许的基调或引人模仿的方式表现打架斗殴、羞辱他人、污言秽语的；宣扬消极、颓废的人生观、世界观和价值观，刻意渲染、夸大民族愚昧落后或社会阴暗面的；国家广播电影电视总局禁止传播的影视节目以及电影、电视剧的删减片段；违反相关法律、法规精神的。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。