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The results show that the SAPO–5 has a pillar-like morphology with the size of about 20 μm×5 μm×5 μm.The ratio of P:Al:Si is 1:1.19:0.67 in its crystal structure, the content of Si is high. The total acidimety fo the SAPO–5 is 578.0 μmol/g , hihger than that of prepared by one step crystalline hydrothermal method.And its initial catalysis character performance on normal butane isomerization reaction reach 24.8 %, higher than that of prepared by one step crystalline hydrothermal method.

实验结果表明:产物为柱状的磷酸硅铝分子筛,其晶粒尺寸大约为20 μm×5 μm×5 μm,其晶体结构中P:Al:Si=1:1.19:0.67,硅含量较高;采用分段晶化方式制备的SAPO-5分子筛的总酸量为578.0 μmol/g高于一段晶化方式制备的SAPO-5分子筛的总酸量;采用分段晶化生成的SAPO-5分子筛的催化正丁烷异构化反应初始活性可达到24.8 %,远高于一段晶化制备的SAPO-5分子筛的初始活性14.1 %。

The earth is a complicated system, and it has been continuously moving differentiating and evolving since it had been formed. Not only has the earth layering structure, but it has vertical movement of materials. The movement is prompted by the mechanism of force and heat of the centrifugal force to be formed by the rotation and revolution of the earth, and difference of temperature, pressure, density, viscosity and velocity in the between core and mantle, and radioactive heat, et al. The expressive means of the mechanism of force and heat are the precesses of mantle plume and mantle fluid. Not only are ore-materials of core and mantle carried directly into crust, but ore-materials of crust are activated and accumulated into proper location by the mantle fluid having the supercritical nature.

地球是一个复杂的系统,自形成以来,一直处于不停地运动、分异和演化过程;它不仅存在着圈层结构,而且伴随其自转和公转的离心力,以及核幔间的温度差、压力差、密度差、粘度差、速度差和放射性蜕变热等动热机制,同时存在着以地幔柱和地幔流体作用方式的物质垂向运动;这一过程,不仅直接向地壳带入核幔成矿物质,而且通过流体自身的超临界性质,将沿途活化已有初步富集的成矿物质转移至地壳适宜部位集中成矿。

The influences of various separartion conditions including buffer concentration,pH value,voltage and detection wave-length were investigated.

建立了柱前衍生化测定低聚异麦芽糖中主要组分的毛细管电泳方法。

Configuration has underground person defence and frame - to cut , the structures such as different shape column, light steel, net frame, curtain wall, seaffold, bridge and landscape, still include the concrete structure of steel tube and steel bone reinforced concrete structural etc..

结构形式有地下人防、框-剪、异形柱、轻钢、网架、幕墙、脚手架、桥梁、景观等结构,还包括钢管混凝土结构和钢骨钢筋混凝土结构等。

The structures of the isomers were assigned by using 2D NMR techniques such as gCOSY. Comparing to the eluates from the chromatographic column, the first band contains the m2, the second band contains the ml.

利用一维及二维核磁共振(2D NMR)技术,结合三元胺中吡啶环的磁屏蔽效应,对两个异构体在溶液中的结构进行了解析,对应于Dowex 50Wx 2柱色层分离的第一包带的H离子为n2(cmen的2位胺基与Cl处于邻位):第二色带的阳离子为ml。

We selected different eluents according to different diasteroisomers and gained the singles of the diasteroisomers by the column chromatography.

经过简单易行的薄层色谱分析法选择了不同的洗脱剂,然后通过柱色谱分离,得到了多对非对映异构体的α-体和β-体。

Separation of racemic mixtures of benzyl glycidyl ether was achieved with HPLC by using Chiralcel OD as chiral stationary phase and hexane/2-propanol mixture of different ratios as eluents.

在 Chiralcel OD多糖类手性固定相上,以各种不同配比的正己烷-异丙醇为洗脱剂,对苄基缩水甘油醚的外消旋体进行对映体拆分,考察了不同洗脱剂配比、柱温和流速对分离度和出峰时间的影响。

Separation of racemic mixtures of thirty-eight secondary aromatic alcohols and arylethanediols with different substituting group was achieved with HPLC by using Chiralcel OD and Chiralcel LJ as chiral stationary phase and hexane/2-propanol mixtures of different ratios as eluents. The chromatographic parameters of these racemates on OD and OJ columns were examined.

在ChiralcelOD和ChiralcelOJ两支多糖类手性固定相上,以各种不同配比的正己烷-异丙醇为洗脱剂对38种带有不同取代基的芳香仲醇及芳香乙二醇类手性化合物的对映体进行拆分,考察了这些外消旋体在这两支手性柱上的色谱行为。

61Ppm, REE distribution patterns of apatite standarded by NASA are classified into two types: The one is concave,"hat-shaped" REE pattern which is slightly enriched in intermediate REE and has a weak or even wanting Ce anomaly. To which, the sandy phosphorite of Jile is representative; the rest REE pattern is shown by more or less complete curve, although distinct Ce negative anomaly or weak Ce positive anomaly is shown up well. The stromatolitic apatite is the representative of this type.

其稀土元素北美页岩标准化配分型式主要分为两类:一类为中稀土略显富集的帽状形态的稀土元素配分型式,微弱的铈负异常或无铈异常,以极乐矿段砂屑磷块岩样品最为典型;另一类为轻稀土、中稀土和重稀土自然分异的三段弧形折线衔接而成的稀土元素配分型式,铈负异常较明显或微弱的铈正异常,以叠层石柱体磷灰石最典型。

Extract with iso-octane and Cleaned up on a silica column.Monensin and salinomycin were separated by methanol and detected at UV 520 nm.

鸡蛋用异辛烷提取,采用硅胶柱净化分离,洗脱液浓缩后用纯甲醇溶解,反应产物在可见光520nm处检测。

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