异柱

In order to do these, we made three cruciform steel reinforced concrete special-shaped short columns and one ordinary reinforced concrete short column, and subjected them to eccentric load.

对3根含钢率不同的十字形截面钢骨混凝土异形短柱和1根无钢骨的十字形截面普通混凝土异形柱进行单向偏压试验。

According to generating finite element model by meshing for special-shaped section columns and the conversion of coordinate,a computer program considered sliding of reinforcement anchoring using the digital iteration method for full range analysis of special-shaped columns is complied.

通过异形柱截面的有限元单元网格划分及坐标变换，在本文确定的数值分析方法上采用FORTRAN90语言编制了考虑粘结滑移影响的钢筋混凝土异形柱截面N-M-φ关系全曲线的计算机程序。

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

The separation of optical isomers of 2, 2'-dihydroxy-1, 1'-binaphthyl and 2, 2'-diamino-1, 1'-binaphthyl was studied by reversed-phase high performance liquid chromatography on a chiral stationary phase consisting of-hydroxypropyl-β-cyclodextrin (Cyclobond Ⅰ 2000 SP)using methanol/water as the mobile phase. The effects of mobile phase ratio, flow rate and column temperature on separation of optical isomers of DHBN and DABN were investigated.

在S-羟丙基－β-环糊精手性柱(CyclobondⅠ2000 SP)上用反相高效液相色谱法研究了2，2'-二氨基－1，1'-联萘和2，2'-二羟基－1，1'-联萘光学异构体的分离，考察了流动相组成、流速以及柱温等对联二萘胺和联二萘酚光学异构体分离的影响。

However in many projects about specially shaped R.C columns, arbitrarily inequiaxial special-shaped columns usually exist as a result of architectural and structural need.

然而在异形柱结构体系的许多实际工程中，由于建筑和结构上的需要，常出现不等肢异形柱。

C arbitrarily inequiaxial special-shaped columns subjected to biaxially eccentric loading is made, the failure character is clarified under different axial compression ratio, the strain distribution in the section under yielding state and limit state is presented, and the corresponding M -φ curves are drew.

接着又对不等肢异形柱在其最不利荷载方向上进行了双向压弯过程破坏机理分析，揭示了不等肢异形柱构件在不同轴压比下的破坏特征，并给出了截面达到屈服状态和极限状态时截面内钢筋和混凝土的应变分布，同时绘制了相应的M-φ关系曲线。

The purpose of this experimental program is to investigate the behavior of slab-column connection with nonrectangular columns and the differences between it and conventional connection.

因此，本文首先进行了柱截面形状为三种典型异形柱（十字形柱、T形柱和L形柱）的板柱冲切试验研究，并将其受冲切特性与相应的等面积方柱和等有效周长方柱试件进行了对比。

Based on the experimental behavior and results of nonrectangular column-slab connections in present thesis, the calculating formulas for flexural strengths of reinforced concrete slab-column connection with cross-shaped column, T-shaped column and L-shaped column are derived by yield-line theory.

4在研究考察三种典型异形柱－板柱连接的冲切试验现象和结果的基础上，应用屈服线理论，对十字形柱、T形柱和L形柱下的板柱连接抗弯承载力进行了研究，提出了上述三种柱型的板柱连接抗弯承载力计算公式。

In order to put this kind of structure into practic

为了能在实际工程中更好地运用这类结构，本文提出一种空间异形柱框架结构的非线性有限元分析方法，并结合单向及反复推覆分析方法对空间异形柱框架结构抗震性能进行分析，然后在推覆分析的基础上做一定的动力时程计算，另外还做了一些试

A micro-monolithic column was prepared by in-situ free radical polymerization of stearyl methacrylate with ethylene glycol dimethacrylate in the presence of the initiator AIBN and a mixture of porogens including iso-amyl alcohol and 1,4-butanediol.

以甲基丙烯酸碳酰十八酯为单体，乙叉二甲基丙烯酸酯为交联剂，异戊醇和1，4-丁二醇为二元致孔剂，偶氮二异丁腈为引发剂，原位制备了具有强疏水性的SMA整体微柱，并利用此整体微柱在普通高效液相色谱仪上测定滴眼液中氧氟沙星的含量。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。