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No obvious difference was observed when 6′-OH of isonucleoside was free or was protected by allyl group.

异核苷6′-OH处于游离和烯丙基保护状态时的结果没有显著差异。

The course of reaction was monitored by estimating the amount of isopropanol liberated in benzene-isopropanol azeotrope in each case.

合成是在苯溶液中采用了金属/非金属的异丙氧基化合物和N-(2-甲基)苯基甘氨酸按1:1和1:2的配比完成的。

Compared with TEA,TiBA activated system produced more blocky copolymer,but the blockiness of its block fraction is lower.

与三乙基铝相比,三异丁基铝为助催化剂得到的不溶级份含量及丙烯含量都较高,但其嵌段性却较低。

These dendritic NOBIN derived Schiff base ligands have been applied to titanium catalyzed hetero-Diels-Alder reaction of Danishefshy's diene and aldehydes, affording the corresponding 2-substituted 2, 3-dihydro-4H-pyran-4-one in quantitative yields and excellent enantioselectivities (up to 97. 2%ee). Comparing the reactivities and enantioselectivities of reaction catalyzed by the titanium complexes of these Schiff base ligands, it was found that a series of ligands L〓 were superior to the other three series of ligands L〓, L〓 and L〓, a significant positive NLE and a dendrimer effect existed in the L〓 dendritic catalyst system. The disposition of the dendritic wedges and the dendron size in the ligands were observed to have a significant impact on the enantioselectivity of the reaction.

NOBIN衍生的树枝状大分子希夫碱手性配体与钛形成的配合物在催化不对称杂Diels-Alder反应中的应用将得到的四个系列NOBIN衍生的树枝状希夫碱三齿手性配体与四异丙氧基钛形成的配合物用于催化Danishefsky's diene与醛的不对称杂Diels-Alder反应,通过反应条件的优化,获得了定量的收率和最高达97.2%ee值的对映选择性;考察了这四个系列NOBIN衍生的树枝状希夫碱钛配合物的催化活性和对映选择性,结果发现它们的活性次序依次为L〓≈L〓>L〓>L〓,对映选择性次序依次为L〓>L〓>L〓>L〓。

In ChapterⅤ, the asymmetric reduction of prochiral ketones using borane as the reagent catalyzed by chiral dysprosium catalyst were described.

第五章主要研究了手性镝试剂催化下硼烷对潜手性酮的不对称还原反应,结果表明异丙氧基镝对硼烷还原酮有明显的催化作用。

The main compounds in the natural terpineol oil were eucalyptol, trans4thujanol, pisopropenyl toluene, cis4thujanol, linalool, camphor, borneol, 4terpineol,αterpineol and safrole.

天然松油醇粗油中主要成分是1,8桉叶素、反式4艹守醇、p异丙烯基甲苯、顺式4艹守醇、芳樟醇、樟脑、龙脑、4松油醇、α松油醇和黄樟素。

Objective: To establish a method for detection of mesityl oxide in the air of workplace by GC chromatography.

目的:建立工作场所空气中异亚丙基丙酮的采样和测定方法。

Objective: To establish a method for mesityl oxide in the air of workplace by GC -MS.

目的 建立工作场所空气中异亚丙基丙酮气质联用测定方法。

Ethoxyberberine and 9-isopropanoxyberberine bearing with different sterically hindered groups were synthesized from beberrubine material.

以小檗碱为原料,合成了小檗碱C-9位不同空间位阻取代的9-乙氧基小檗碱、9-异丙氧基小檗碱,通过MS、1H NMR确认其结构。

To improve the effect of CDCA on dissolving cholesterol gallstone, the water-soluble copolymers as polycarboxylic acid of comb-like copolymers and C_(60)-PCC were synthesized, which being used for modification of CDCA and strengthening effects of CDCA on dissolving the cholesterol gallstones by their entropy-repelled properties of comb-shaped side chains in buffers of phosphate and in model bile.The design theory of polymer was mainly employed to synthesis the conjugate of PCC-CDCA and C_(60)-PCC-CDCA by C_(60), polyoxyalkylene allylalkyldiether and maleic anhydride, which were copolymerized with AIBN as initiator, and then PCC or C_(60)-PCC were reacted with CDCA. The structures of the copolymers and the conjugates of PCC-CDCA and C_(60)-PCC-CDCA were confirmed with IR, TLC and TEM. The dissolving effects and the dissolution kinetics mechanism of cholesterol gallstone was inverstigated in PBS and in model bile of different cholesterol saturated index at pH7.4, including PCC-CDCA or C_(60)-PCC-CDCA.

利用高分子设计理论,以烯丙基聚氧乙烯基醚、顺丁烯二酸酐、C_(60)和CDCA为原料,以偶氮二异丁腈为引发剂,合成具有梳状侧链结构的梳状共聚物-CDCA结合物和C_(60)-梳状共聚物-CDCA结合物,以IR、TLC和TEM法表征共聚物的结构,并在pH7.4的PBS液和不同胆固醇饱和指数的模拟胆汁中进行溶石效果的研究,探讨在PBS液和不同CSI的模拟胆汁中结合物溶解胆固醇结石的效果和溶解动力学机制。

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Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化,但却比去年同期高8%。

However, to get a true quote, you will need to provide detailed personal and financial information.

然而,要让一个真正的引用,你需要提供详细的个人和财务信息。