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The studies segmented polyester polyurethaneurea elastomers based on 4,4'-diphenylmethane diisocyanate, ethylene diamine and polybutylene adipate (M. W. 1975 and M. W. 1228) were studied by means of IR spectrascopy.

用红外光谱法对基於4,4'-二苯基甲烷二异氰酸酯、乙二胺和聚己二酸丁二醇酯(分子量分别为1975和1228)的嵌段聚脲氨酯弹性体进行了研究。

Treatment of dials with N-tert-butanesulfinamide, all biaryl dials were successfully converted into the corresponding bis-imines which were then treated with samarium diiodide to afford diamine products. The absolute configurations of all the intramolecular coupling products were determined by X-ray crystallography.

轴手性二醛与N-叔丁基亚磺酰胺缩合得到相应的亚胺,其为一对非对映异构体。N-叔丁基亚磺酰亚胺在二碘化钐条件下得到的偶联产物,经X-衍射也确定了其立体构型。

The polyesters with terminal hydroxyl groups were prepared by condensation polymerization of adipic acid with 1,4-butanediol or ethylene glycol and, in some cases, a little amount of propylene glycol. The polyurethane thermoplastics were then prepared with the polyester, 4,4'-diphenylmethane diisocyanate and 1,4-butanediol.

采用己二酸、乙二醇(或加入少量1,2-丙二醇)和1,4-丁二醇制备了端羟基聚酯,并用该聚酯和4,4'-二苯基甲烷二异氰酸酯、1,4-丁二醇制备了聚酯型热塑性聚氨酯;考察了NCO/OH值、聚酯分子量等因素对热塑性聚氨酯的物理机械性能的影响。

Mixing and dilution heterotactic enthalpies of aqueous n-butanol solutions and aqueous amino acids (glycine, L-alanine, L-proline, L-valine) solutions were determined at 298.15 K by flow microcalorimetric system of 2277 Thermal Activity Monitor. The data were analyzed by using the McMillan-Mayer theory to obtain the enthalpic interaction coefficients.

利用2277热活性检测仪的流动测量系统获得了298.15K时甘氨酸、L-丙氨酸、L-缬氨酸和L-脯氨酸分别与n-丁醇在水溶液中混合过程的焓变以及各自的稀释焓,依据McMillan-Mayer理论关联得到异系焓相互作用系数,讨论了不同氨基酸与n-丁醇分子的作用机理。

Aminonocyclobutanecarboxylic acid is prepared according to above route, starting from 1-bromocyclobutanecarboxylic acid, which uses hexamethylenamine as catalyst in isopropyl alcohol.

再以1-溴代环丁甲酸为原料,以异丙醇作溶剂,乌洛托品为催化剂,与氨气反应,制备出1-氨基环丁甲酸,并优化了中间产物及最终产品的制备工艺。

In the synthesis of canthaxanthin by selective catalylitic oxidating of βcarotene,CO2 was used as acidifying or alkalizing agent,which controlled reacting system acidity and protected polyene.,producing less by-products and increasing catalylitic oxidation selectivity.In the addition reaction of isoprene with hypochloric acid,1-chloro-2-methyl-3-buten-2-ol and l-chloro-2-methyl-3-buten-4-ol were made by controlling of the acidity with carbon dioxide i...

CO2作为酸碱调节剂和惰性气体,在β-胡萝卜素催化氧化合成角黄素反应中,可以控制反应体系酸性,保护原料中的双键,减少副反应发生,提高催化氧化反应的选择性;异戊二烯氯醇化生成1-氯-2-甲基-3-丁烯-2-醇和1-氯-2-甲基-3-丁唏-4-醇反应中,CO2代替有机酸作酸碱调节剂,控制次氯酸的生成速度,达到调控反应的目的,反应条件温和,不副产固体。

A few days ago, 1500 tons when group of Henan day coronal builds / year ferment test-drive of mellow separate project succeeds, the purity of methylic Ding Chun all exceeds methylic Ding Chun of the alcohol of different the fifth of the ten Heavenly Stem that from inside miscellaneous mellow oil depart gives, 3-, 2- 99%, obtain line of business of person of the same trade banner level.

日前,河南天冠集团建设的1500吨/年发酵醇分离项目试车成功,从杂醇油中分离出的异戊醇、3-甲基丁醇、2-甲基丁醇的纯度均超过99%,达到同行业领先水平。

The results showed 3 types of aluminum compound prepared in this paper all had good poison protection effectiveness on such impurities as stannous chloride,lead oxide,sodium hydrogen sulfate,and so on.Moreover,the mechanism of the poison of catalyst was also discussed.

结果表明,合成的3种防中毒剂即防-1、防-2(主要成分为乙酰丙酮合铝)及防-3(主要成分为二乙酰丙酮基异丙氧基铝)对二月桂酸二丁基锡、氯化亚锡、二正丁胺、硫脲、氧化铅及硫酸氢钠等杂质均有较好的防中毒作用;不同防中毒剂对不同杂质的防中毒作用有一定的选择性。

Cases in the control group were treated with salbutamol based on the routine treatment.

将95例毛细支气管炎患儿随机分为两组,对照组95例在常规治疗基础上加用沙丁胺醇,治疗组95例在常规治疗基础上加用沙丁胺醇、异丙托溴铵、布地奈德,均2次/d空气压缩雾化泵吸入,观察两组临床症状、体征改善情况。

In this work, salbutamol and sulphuric acids were used as reactants and isopropanol was used as a solvent.

以沙丁胺醇和硫酸为反应物,在异丙醇溶液中采用反应结晶法制备超细硫酸沙丁胺醇颗粒。

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此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

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为了做成这笔生意,我建议我们在价格上大家各让一半。

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