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The extracted components were qualitatively and quantitatively analyzed by gas chromatography mass spectrometry.The results showed that 30,26 compounds were identified from the volatile components extracted by DSE,SDE methods resp.36 kinds of components were extracted by 2 methods in total,among them the content of hexadecanoic aci...

结果表明,从DSE、SDE法提取的挥发性成分中分别鉴定出30(总含量58.24μg/g)、26种化合物总含量(86.66μg/g,2种方法共提取出36种化合物,其中十六酸含量最高,其次为亚油酸、油酸、邻苯二甲酸二异丁酯、间甲苯甲醛、龙脑。

MIPC was photocatalytically transformed to 3,4-dihydroxyl hypnone, 2-iso-butyl phenol and acetic acid, and mineralized ultimately in oxygenated TiO2 slurries. The photocatalytic degradation processed according to first order kinetics with the apparent rate constant depending on initial concentration, light intensity and the amount of catalyst. The amount of catalyst had an optimum value (0.5g/L). The apparent rate was inversely proportional to square root of the initial concentration approximately.

MIPC能被光催化转化成3,4-二羟基苯乙酮、2-异丁基苯酚和乙酸等产物并最终被矿化,MIPC的光催化反应过程符合一级动力学规律,其表观速率常数与MIPC的起始浓度、TiO2量和光强等因素有关,MIPC降解的反应速率与入射光强成正比,与MIPC初始浓度的平方根成反比。

A new synthesis method of Taxane s was reported involving radicals generated from hypophosphorous acidn initiated by 2,2′-azobisisobutyronitrile.

由偶氮二异丁腈引发次磷酸产生次磷酸根自由基,以链式自由基反应机制脱除紫杉烷类化合物结构中的含氧基团,简单、高效地合成了紫杉烷。

A new synthesis method of Taxanes was reported involving radicals generated from hypophosphorous acid n initiated by 2,2′-azobisisobutyronitrile.

由偶氮二异丁腈引发次磷酸产生次磷酸根自由基,以链式自由基反应机制脱除紫杉烷类化合物结构中的含氧基团,简单、高效地合成了紫杉烷。

Methods:The subcutaneous adipose tissue was obtained from the fold inguen of four SD rats, then digested with collagenase type Ⅰ and cultured in endothelial medium for seven days.

获取4只雄性SD大鼠鼠蹊部皮下脂肪,通过机械分割和组织消化法获取脂肪基质细胞,在内皮细胞培养液中培养7d后,经免疫细胞化学及透射电镜鉴定证实95%以上细胞已具内皮细胞表型特征,再将这些细胞进行成脂(DMEM/F-12培养基内加入0.5mmol/L1-甲基-3-异丁基-黄嘌呤,1μmol/L地塞米松,10μmol/L胰岛素,200μmol/L吲哚美星)定向诱导7d,形态学观察和油红O特殊染色鉴定诱导后的细胞。

In the polymerization procedure,S--α-phenyl ethylamine was used as target template molecules,methacrylic acid was selected as functional monomers, ethylene glycol dimethacrylate or divinylbenzene as crosslinker, azobisisobutyronitrile or benzophenone was used as irritator.

以S--α-苯乙胺为模板,甲基丙烯酸为功能单体,分别以二甲基丙烯酸乙二醇酯、二乙烯基苯为交联剂,偶氮二异丁睛或二苯甲酮为引发剂,采用了本体聚合法、悬浮聚合法合成了一系列的S--α-苯乙胺印迹聚合物。

The reaction order of was found to be unity and that in isobutyl alcohol to be positive fractional.

结果表明反应对鈰离子为一级,对异丁醇的表观反应级数为正分数。

To improve the extraction of gold from electronic waste, statistical methods were used to analyze the impact of different factors affecting the extraction of Au using methyl isobutyl ketone as solvent.

以电子废料中的金为研究对象,用统计学方法对甲基异丁基甲酮萃取电子废料中金的影响因素进行了探讨和分析。

In order to investigate the effects of magnetic field on the liquid-liquid extraction,the extraction process of acetone-water-methyl isobutyl ketone system was studied under magnetic field with different magnetic induction intensities.

为探讨磁场对液-液萃取过程的影响,本研究在不同磁感应强度的磁场中,对丙酮-水-甲基异丁基酮物系的萃取过程进行了研究。

The kinetic mechanism of extraction reaction and the influence of isobutyl alcohol on the extraction rates of uranium with TOA are examined.

测定了三辛胺浓度、硫酸浓度、温度和异丁醇对萃取速率的影响。

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随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

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关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。